JP5585995B2 - マルチトール強化生成物の製造方法 - Google Patents
マルチトール強化生成物の製造方法 Download PDFInfo
- Publication number
- JP5585995B2 JP5585995B2 JP2006519817A JP2006519817A JP5585995B2 JP 5585995 B2 JP5585995 B2 JP 5585995B2 JP 2006519817 A JP2006519817 A JP 2006519817A JP 2006519817 A JP2006519817 A JP 2006519817A JP 5585995 B2 JP5585995 B2 JP 5585995B2
- Authority
- JP
- Japan
- Prior art keywords
- maltitol
- product
- maltose
- fraction
- amylase
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 235000010449 maltitol Nutrition 0.000 title claims abstract description 131
- 239000000845 maltitol Substances 0.000 title claims abstract description 130
- VQHSOMBJVWLPSR-WUJBLJFYSA-N maltitol Chemical compound OC[C@H](O)[C@@H](O)[C@@H]([C@H](O)CO)O[C@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O VQHSOMBJVWLPSR-WUJBLJFYSA-N 0.000 title claims abstract description 125
- 229940035436 maltitol Drugs 0.000 title claims abstract description 125
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 20
- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 claims abstract description 64
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 claims abstract description 64
- 238000000034 method Methods 0.000 claims abstract description 57
- 235000020357 syrup Nutrition 0.000 claims abstract description 35
- 239000006188 syrup Substances 0.000 claims abstract description 35
- 239000007788 liquid Substances 0.000 claims abstract description 33
- 238000002425 crystallisation Methods 0.000 claims abstract description 14
- 230000008025 crystallization Effects 0.000 claims abstract description 14
- 239000000047 product Substances 0.000 claims description 67
- 229920002472 Starch Polymers 0.000 claims description 44
- 239000008107 starch Substances 0.000 claims description 44
- 235000019698 starch Nutrition 0.000 claims description 44
- 108090000637 alpha-Amylases Proteins 0.000 claims description 30
- 239000000126 substance Substances 0.000 claims description 30
- 235000013336 milk Nutrition 0.000 claims description 26
- 239000008267 milk Substances 0.000 claims description 26
- 210000004080 milk Anatomy 0.000 claims description 26
- 102000004139 alpha-Amylases Human genes 0.000 claims description 20
- 229940024171 alpha-amylase Drugs 0.000 claims description 20
- 239000006227 byproduct Substances 0.000 claims description 18
- 239000000203 mixture Substances 0.000 claims description 18
- 238000005194 fractionation Methods 0.000 claims description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
- 108010019077 beta-Amylase Proteins 0.000 claims description 12
- 238000011084 recovery Methods 0.000 claims description 10
- 238000004587 chromatography analysis Methods 0.000 claims description 9
- 230000001965 increasing effect Effects 0.000 claims description 8
- 229920002245 Dextrose equivalent Polymers 0.000 claims description 7
- 238000009903 catalytic hydrogenation reaction Methods 0.000 claims description 6
- 230000002787 reinforcement Effects 0.000 claims 3
- 239000007787 solid Substances 0.000 abstract description 12
- 238000007711 solidification Methods 0.000 abstract 1
- 230000008023 solidification Effects 0.000 abstract 1
- 102000004190 Enzymes Human genes 0.000 description 13
- 108090000790 Enzymes Proteins 0.000 description 13
- 229940088598 enzyme Drugs 0.000 description 13
- 238000005984 hydrogenation reaction Methods 0.000 description 13
- 239000013078 crystal Substances 0.000 description 12
- 229920000856 Amylose Polymers 0.000 description 6
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 6
- 239000012452 mother liquor Substances 0.000 description 6
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 5
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 5
- 239000003054 catalyst Substances 0.000 description 5
- 108010028688 Isoamylase Proteins 0.000 description 4
- 238000010828 elution Methods 0.000 description 4
- 239000012263 liquid product Substances 0.000 description 4
- 239000002002 slurry Substances 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- PKAUICCNAWQPAU-UHFFFAOYSA-N 2-(4-chloro-2-methylphenoxy)acetic acid;n-methylmethanamine Chemical compound CNC.CC1=CC(Cl)=CC=C1OCC(O)=O PKAUICCNAWQPAU-UHFFFAOYSA-N 0.000 description 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical group [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 238000005341 cation exchange Methods 0.000 description 3
- 239000003729 cation exchange resin Substances 0.000 description 3
- 238000013375 chromatographic separation Methods 0.000 description 3
- 238000010924 continuous production Methods 0.000 description 3
- 239000003480 eluent Substances 0.000 description 3
- 238000004128 high performance liquid chromatography Methods 0.000 description 3
- 238000002347 injection Methods 0.000 description 3
- 239000007924 injection Substances 0.000 description 3
- 239000008213 purified water Substances 0.000 description 3
- 239000011347 resin Substances 0.000 description 3
- 229920005989 resin Polymers 0.000 description 3
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- 101710117655 Maltogenic alpha-amylase Proteins 0.000 description 2
- KJTLSVCANCCWHF-UHFFFAOYSA-N Ruthenium Chemical compound [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 description 2
- 240000008042 Zea mays Species 0.000 description 2
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 2
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 230000032683 aging Effects 0.000 description 2
- 238000005119 centrifugation Methods 0.000 description 2
- 235000005822 corn Nutrition 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 238000011534 incubation Methods 0.000 description 2
- 239000003456 ion exchange resin Substances 0.000 description 2
- 229920003303 ion-exchange polymer Polymers 0.000 description 2
- 238000005086 pumping Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 229910052707 ruthenium Inorganic materials 0.000 description 2
- 238000007873 sieving Methods 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- 238000004448 titration Methods 0.000 description 2
- CHRJZRDFSQHIFI-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;styrene Chemical compound C=CC1=CC=CC=C1.C=CC1=CC=CC=C1C=C CHRJZRDFSQHIFI-UHFFFAOYSA-N 0.000 description 1
- 240000001592 Amaranthus caudatus Species 0.000 description 1
- 235000009328 Amaranthus caudatus Nutrition 0.000 description 1
- 229920001685 Amylomaize Polymers 0.000 description 1
- 229920000945 Amylopectin Polymers 0.000 description 1
- 235000005273 Canna coccinea Nutrition 0.000 description 1
- 240000008555 Canna flaccida Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 240000005979 Hordeum vulgare Species 0.000 description 1
- 235000007340 Hordeum vulgare Nutrition 0.000 description 1
- 244000017020 Ipomoea batatas Species 0.000 description 1
- 235000002678 Ipomoea batatas Nutrition 0.000 description 1
- 240000003183 Manihot esculenta Species 0.000 description 1
- 235000016735 Manihot esculenta subsp esculenta Nutrition 0.000 description 1
- 240000008790 Musa x paradisiaca Species 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 244000046052 Phaseolus vulgaris Species 0.000 description 1
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 1
- NPXOKRUENSOPAO-UHFFFAOYSA-N Raney nickel Chemical compound [Al].[Ni] NPXOKRUENSOPAO-UHFFFAOYSA-N 0.000 description 1
- 229910000564 Raney nickel Inorganic materials 0.000 description 1
- 244000061456 Solanum tuberosum Species 0.000 description 1
- 235000002595 Solanum tuberosum Nutrition 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
- 235000021307 Triticum Nutrition 0.000 description 1
- 244000098338 Triticum aestivum Species 0.000 description 1
- 206010046865 Vaccinia virus infection Diseases 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 235000012735 amaranth Nutrition 0.000 description 1
- 239000004178 amaranth Substances 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 235000021015 bananas Nutrition 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 235000014633 carbohydrates Nutrition 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000011210 chromatographic step Methods 0.000 description 1
- 235000008504 concentrate Nutrition 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 229920006037 cross link polymer Polymers 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000003795 desorption Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 235000021374 legumes Nutrition 0.000 description 1
- 150000002692 maltoses Chemical class 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229910000510 noble metal Inorganic materials 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 235000012015 potatoes Nutrition 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 230000005070 ripening Effects 0.000 description 1
- 239000012265 solid product Substances 0.000 description 1
- 229960002920 sorbitol Drugs 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000012607 strong cation exchange resin Substances 0.000 description 1
- 125000001174 sulfone group Chemical group 0.000 description 1
- 208000007089 vaccinia Diseases 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H15/00—Compounds containing hydrocarbon or substituted hydrocarbon radicals directly attached to hetero atoms of saccharide radicals
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H15/00—Compounds containing hydrocarbon or substituted hydrocarbon radicals directly attached to hetero atoms of saccharide radicals
- C07H15/02—Acyclic radicals, not substituted by cyclic structures
- C07H15/04—Acyclic radicals, not substituted by cyclic structures attached to an oxygen atom of the saccharide radical
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Biotechnology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
- Crystallography & Structural Chemistry (AREA)
- Saccharide Compounds (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP03254528.7 | 2003-07-18 | ||
| EP03254528 | 2003-07-18 | ||
| PCT/EP2004/007372 WO2005014608A2 (en) | 2003-07-18 | 2004-07-06 | Process for preparing maltitol enriched products |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012230490A Division JP2013028641A (ja) | 2003-07-18 | 2012-10-18 | マルチトール強化生成物の製造方法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2008538739A JP2008538739A (ja) | 2008-11-06 |
| JP2008538739A5 JP2008538739A5 (cg-RX-API-DMAC7.html) | 2011-12-08 |
| JP5585995B2 true JP5585995B2 (ja) | 2014-09-10 |
Family
ID=34130331
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2006519817A Expired - Fee Related JP5585995B2 (ja) | 2003-07-18 | 2004-07-06 | マルチトール強化生成物の製造方法 |
| JP2012230490A Withdrawn JP2013028641A (ja) | 2003-07-18 | 2012-10-18 | マルチトール強化生成物の製造方法 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012230490A Withdrawn JP2013028641A (ja) | 2003-07-18 | 2012-10-18 | マルチトール強化生成物の製造方法 |
Country Status (16)
| Country | Link |
|---|---|
| US (1) | US7935190B2 (cg-RX-API-DMAC7.html) |
| EP (1) | EP1656388B1 (cg-RX-API-DMAC7.html) |
| JP (2) | JP5585995B2 (cg-RX-API-DMAC7.html) |
| KR (1) | KR101148615B1 (cg-RX-API-DMAC7.html) |
| CN (2) | CN1823082A (cg-RX-API-DMAC7.html) |
| AT (1) | ATE541852T1 (cg-RX-API-DMAC7.html) |
| AU (1) | AU2004263221B2 (cg-RX-API-DMAC7.html) |
| BR (1) | BRPI0412698A (cg-RX-API-DMAC7.html) |
| CA (1) | CA2529508C (cg-RX-API-DMAC7.html) |
| DK (1) | DK1656388T3 (cg-RX-API-DMAC7.html) |
| ES (1) | ES2379352T3 (cg-RX-API-DMAC7.html) |
| MY (1) | MY140844A (cg-RX-API-DMAC7.html) |
| PL (1) | PL1656388T3 (cg-RX-API-DMAC7.html) |
| SI (1) | SI1656388T1 (cg-RX-API-DMAC7.html) |
| WO (1) | WO2005014608A2 (cg-RX-API-DMAC7.html) |
| ZA (1) | ZA200600012B (cg-RX-API-DMAC7.html) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106798312A (zh) * | 2015-11-26 | 2017-06-06 | 山东福田药业有限公司 | 一种氢化淀粉水解物及其制备方法 |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040224058A1 (en) * | 2003-03-20 | 2004-11-11 | Spi Polyols, Inc. | Maltitol solutions with high maltitol content and methods of making same |
| CN100424088C (zh) * | 2005-05-19 | 2008-10-08 | 禹城福田药业有限公司 | 利用纯度为45%-50%的麦芽糖制取晶体麦芽糖醇的方法 |
| WO2008025809A1 (en) * | 2006-09-01 | 2008-03-06 | Cargill, Incorporated | Polyol syrups useful in the manufacture of sugar-free chewable confectionery |
| FR2905705B1 (fr) | 2006-09-08 | 2011-11-04 | Syral | Procede d'obtention d'un sirop a haute teneur en maltitol et sirop ainsi obtenu |
| KR20080049924A (ko) * | 2006-12-01 | 2008-06-05 | 주식회사 신동방씨피 | 고순도 결정 분말 말티톨의 제조방법 |
| FR2922890B1 (fr) | 2007-10-30 | 2009-12-18 | Roquette Freres | Procede d'evapocristallisation du maltitol. |
| CN101486741B (zh) * | 2008-12-15 | 2011-12-14 | 山东福田投资有限公司 | 一种连续生产结晶麦芽糖醇的工艺 |
| EP2809791B1 (en) * | 2012-01-31 | 2019-10-30 | Cargill, Incorporated | Process for producing solid maltitol from starch |
| US20150024437A1 (en) * | 2012-01-31 | 2015-01-22 | Cargill, Incorporated | Maltitol enriched products |
| CN102743897B (zh) * | 2012-07-23 | 2015-06-10 | 中粮生物化学(安徽)股份有限公司 | 一种淀粉糖液的精制方法 |
| AU2015292799B2 (en) * | 2014-07-21 | 2019-06-13 | Xyleco, Inc. | Processing biomass |
| CN106539056A (zh) * | 2016-10-24 | 2017-03-29 | 山东福田药业有限公司 | 一种具高保湿活性的还原水饴及其糖化工艺 |
| CN112480190A (zh) * | 2020-12-29 | 2021-03-12 | 山东福田药业有限公司 | 一种细粒度麦芽糖醇晶体及其制备方法 |
Family Cites Families (23)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS57134498A (en) * | 1981-02-12 | 1982-08-19 | Hayashibara Biochem Lab Inc | Anhydrous crystalline maltitol and its preparation and use |
| JPS57209000A (en) * | 1981-06-17 | 1982-12-22 | Organo Kk | Decomposition of maltose |
| JPS5823799A (ja) | 1981-08-03 | 1983-02-12 | 株式会社林原生物化学研究所 | 高純度マルト−スの製造方法 |
| JPS6067000A (ja) | 1983-09-19 | 1985-04-17 | 三菱化学株式会社 | マルト−スの分離法 |
| FR2575180B1 (fr) * | 1984-12-20 | 1987-02-06 | Roquette Freres | Produit a haute teneur en maltitol, ses applications et son procede de fabrication |
| FR2575179B1 (fr) * | 1984-12-20 | 1987-02-06 | Roquette Freres | Procede de preparation de maltitol cristallise |
| FR2581999B1 (fr) * | 1985-05-15 | 1988-08-12 | Roquette Freres | Procede et installation de production de maltitol cristallise |
| JPH0675648B2 (ja) | 1985-07-16 | 1994-09-28 | 三菱化成株式会社 | 成分分離方法 |
| JPS62126993A (ja) * | 1985-11-26 | 1987-06-09 | Agency Of Ind Science & Technol | マルト−スの製法 |
| JP2622695B2 (ja) * | 1987-10-05 | 1997-06-18 | 東和化成工業株式会社 | マルチトールの製造方法 |
| JP2696534B2 (ja) | 1988-09-29 | 1998-01-14 | 東和化成工業株式会社 | 高純度マルトース及びその還元物の製造方法 |
| JP2696537B2 (ja) * | 1988-10-28 | 1998-01-14 | 東和化成工業株式会社 | 高純度マルトースの製造方法 |
| JP3070890B2 (ja) | 1993-02-12 | 2000-07-31 | オルガノ株式会社 | 澱粉糖の製造方法 |
| JP3089146B2 (ja) * | 1993-10-01 | 2000-09-18 | オルガノ株式会社 | 澱粉糖の製造方法 |
| JP3602903B2 (ja) * | 1995-05-02 | 2004-12-15 | 東和化成工業株式会社 | 結晶マルチトール及びそれを含有する含蜜結晶の製造方法 |
| JP4106078B2 (ja) | 1995-11-08 | 2008-06-25 | 三菱商事フードテック株式会社 | 結晶マルチトールの製造方法 |
| JP4711471B2 (ja) * | 1996-07-05 | 2011-06-29 | 三菱商事フードテック株式会社 | 結晶マルチトール及びそれを含有する含蜜結晶の製造方法 |
| FR2769023B1 (fr) * | 1997-09-26 | 2000-08-25 | Roquette Freres | Procede de fabrication d'un sirop riche en maltose |
| FR2769025B1 (fr) * | 1997-09-26 | 1999-12-03 | Roquette Freres | Cristaux de maltitol de formes particulieres, compositions cristallines les contenant et procedes pour leur preparation |
| JP3624672B2 (ja) | 1998-01-27 | 2005-03-02 | 株式会社林原生物化学研究所 | 無水結晶マルチトールの連続的製造方法及び製造装置 |
| FR2787809B1 (fr) * | 1998-12-29 | 2002-01-18 | Roquette Freres | Procede de fabrication d'un sirop riche en maltose |
| FR2787807B1 (fr) * | 1998-12-29 | 2002-01-18 | Roquette Freres | Alpha-amylase maltogenique immobilisee et son utilisation dans la fabrication d'un sirop riche en maltose |
| JP3822465B2 (ja) * | 2000-07-25 | 2006-09-20 | 株式会社ニッシ | マルトース液の製造方法 |
-
2004
- 2004-07-06 CA CA2529508A patent/CA2529508C/en not_active Expired - Lifetime
- 2004-07-06 ES ES04740697T patent/ES2379352T3/es not_active Expired - Lifetime
- 2004-07-06 BR BRPI0412698-0A patent/BRPI0412698A/pt not_active Application Discontinuation
- 2004-07-06 PL PL04740697T patent/PL1656388T3/pl unknown
- 2004-07-06 DK DK04740697.0T patent/DK1656388T3/da active
- 2004-07-06 JP JP2006519817A patent/JP5585995B2/ja not_active Expired - Fee Related
- 2004-07-06 US US10/564,652 patent/US7935190B2/en not_active Expired - Fee Related
- 2004-07-06 AT AT04740697T patent/ATE541852T1/de active
- 2004-07-06 SI SI200431844T patent/SI1656388T1/sl unknown
- 2004-07-06 AU AU2004263221A patent/AU2004263221B2/en not_active Ceased
- 2004-07-06 CN CNA2004800205716A patent/CN1823082A/zh active Pending
- 2004-07-06 KR KR1020067001130A patent/KR101148615B1/ko not_active Expired - Fee Related
- 2004-07-06 WO PCT/EP2004/007372 patent/WO2005014608A2/en not_active Ceased
- 2004-07-06 EP EP04740697A patent/EP1656388B1/en not_active Revoked
- 2004-07-06 CN CN201410364987.5A patent/CN104961780A/zh active Pending
- 2004-07-14 MY MYPI20042812A patent/MY140844A/en unknown
-
2006
- 2006-01-03 ZA ZA200600012A patent/ZA200600012B/xx unknown
-
2012
- 2012-10-18 JP JP2012230490A patent/JP2013028641A/ja not_active Withdrawn
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106798312A (zh) * | 2015-11-26 | 2017-06-06 | 山东福田药业有限公司 | 一种氢化淀粉水解物及其制备方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1823082A (zh) | 2006-08-23 |
| KR101148615B1 (ko) | 2012-05-21 |
| ZA200600012B (en) | 2007-03-28 |
| JP2008538739A (ja) | 2008-11-06 |
| CA2529508A1 (en) | 2005-02-17 |
| EP1656388B1 (en) | 2012-01-18 |
| DK1656388T3 (da) | 2012-05-14 |
| BRPI0412698A (pt) | 2006-10-03 |
| ATE541852T1 (de) | 2012-02-15 |
| US7935190B2 (en) | 2011-05-03 |
| JP2013028641A (ja) | 2013-02-07 |
| WO2005014608A2 (en) | 2005-02-17 |
| MY140844A (en) | 2010-01-29 |
| AU2004263221B2 (en) | 2008-06-26 |
| CN104961780A (zh) | 2015-10-07 |
| EP1656388A2 (en) | 2006-05-17 |
| ES2379352T3 (es) | 2012-04-25 |
| KR20060038447A (ko) | 2006-05-03 |
| AU2004263221A1 (en) | 2005-02-17 |
| WO2005014608A3 (en) | 2005-08-11 |
| PL1656388T3 (pl) | 2012-06-29 |
| SI1656388T1 (sl) | 2012-04-30 |
| CA2529508C (en) | 2013-08-27 |
| US20060188626A1 (en) | 2006-08-24 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP2013028641A (ja) | マルチトール強化生成物の製造方法 | |
| KR100411636B1 (ko) | 결정성말티톨및이를함유하는함밀결정의제조방법 | |
| US6346400B1 (en) | Process for the preparation of a maltose-rich syrup | |
| US5462864A (en) | Manufacturing method of high purity maltose and its reduced product | |
| AU758436B2 (en) | Method of manufacturing a maltose-rich syrup | |
| JP6177803B2 (ja) | デンプンからの固体マルチトール製造方法 | |
| WO1997021718A1 (en) | Crystalline 1-kestose and process for preparing the same | |
| JP6177804B2 (ja) | デンプンからのマルチトール製造方法 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20091006 |
|
| A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20100105 |
|
| A602 | Written permission of extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A602 Effective date: 20100113 |
|
| A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20100203 |
|
| A602 | Written permission of extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A602 Effective date: 20100210 |
|
| A524 | Written submission of copy of amendment under article 19 pct |
Free format text: JAPANESE INTERMEDIATE CODE: A524 Effective date: 20100301 |
|
| RD04 | Notification of resignation of power of attorney |
Free format text: JAPANESE INTERMEDIATE CODE: A7424 Effective date: 20100525 |
|
| A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20110419 |
|
| A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20110715 |
|
| A602 | Written permission of extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A602 Effective date: 20110725 |
|
| A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20110818 |
|
| A602 | Written permission of extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A602 Effective date: 20110825 |
|
| A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20110916 |
|
| A602 | Written permission of extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A602 Effective date: 20110927 |
|
| A524 | Written submission of copy of amendment under article 19 pct |
Free format text: JAPANESE INTERMEDIATE CODE: A524 Effective date: 20111018 |
|
| A02 | Decision of refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A02 Effective date: 20120619 |
|
| A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20140225 |
|
| A602 | Written permission of extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A602 Effective date: 20140305 |
|
| A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20140325 |
|
| A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20140407 |
|
| A602 | Written permission of extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A602 Effective date: 20140411 |
|
| A61 | First payment of annual fees (during grant procedure) |
Free format text: JAPANESE INTERMEDIATE CODE: A61 Effective date: 20140716 |
|
| R150 | Certificate of patent or registration of utility model |
Ref document number: 5585995 Country of ref document: JP Free format text: JAPANESE INTERMEDIATE CODE: R150 |
|
| LAPS | Cancellation because of no payment of annual fees |