JP5542146B2 - 酸素含有量を制御した非常に多孔質の活性炭 - Google Patents
酸素含有量を制御した非常に多孔質の活性炭 Download PDFInfo
- Publication number
- JP5542146B2 JP5542146B2 JP2011535635A JP2011535635A JP5542146B2 JP 5542146 B2 JP5542146 B2 JP 5542146B2 JP 2011535635 A JP2011535635 A JP 2011535635A JP 2011535635 A JP2011535635 A JP 2011535635A JP 5542146 B2 JP5542146 B2 JP 5542146B2
- Authority
- JP
- Japan
- Prior art keywords
- activated carbon
- temperature
- carbon
- heating
- carbon material
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims description 115
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 title claims description 54
- 239000001301 oxygen Substances 0.000 title claims description 52
- 229910052760 oxygen Inorganic materials 0.000 title claims description 52
- 239000007833 carbon precursor Substances 0.000 claims description 33
- 239000000463 material Substances 0.000 claims description 33
- 238000010438 heat treatment Methods 0.000 claims description 31
- 239000012190 activator Substances 0.000 claims description 22
- 239000000203 mixture Substances 0.000 claims description 19
- 238000000034 method Methods 0.000 claims description 15
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 9
- 239000007787 solid Substances 0.000 claims description 6
- 150000002484 inorganic compounds Chemical class 0.000 claims description 4
- 229910010272 inorganic material Inorganic materials 0.000 claims description 4
- 238000005406 washing Methods 0.000 claims description 3
- 230000004913 activation Effects 0.000 description 24
- 238000003763 carbonization Methods 0.000 description 19
- 239000000126 substance Substances 0.000 description 19
- 229910052799 carbon Inorganic materials 0.000 description 16
- 238000000746 purification Methods 0.000 description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 12
- 239000003575 carbonaceous material Substances 0.000 description 11
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 9
- 238000004146 energy storage Methods 0.000 description 6
- 239000000243 solution Substances 0.000 description 6
- 239000011148 porous material Substances 0.000 description 5
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 description 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 4
- 239000007864 aqueous solution Substances 0.000 description 4
- 238000001816 cooling Methods 0.000 description 4
- 239000003792 electrolyte Substances 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- 229920001568 phenolic resin Polymers 0.000 description 4
- 239000005011 phenolic resin Substances 0.000 description 4
- 239000002243 precursor Substances 0.000 description 4
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 description 4
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 3
- 230000015556 catabolic process Effects 0.000 description 3
- 238000006731 degradation reaction Methods 0.000 description 3
- 239000008367 deionised water Substances 0.000 description 3
- 229910021641 deionized water Inorganic materials 0.000 description 3
- 238000009826 distribution Methods 0.000 description 3
- 125000000524 functional group Chemical group 0.000 description 3
- 238000010348 incorporation Methods 0.000 description 3
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 3
- 229920005989 resin Polymers 0.000 description 3
- 239000011347 resin Substances 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 230000002411 adverse Effects 0.000 description 2
- 239000003570 air Substances 0.000 description 2
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 2
- 229910052786 argon Inorganic materials 0.000 description 2
- 239000012298 atmosphere Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 229910052734 helium Inorganic materials 0.000 description 2
- 230000007774 longterm Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 229920002239 polyacrylonitrile Polymers 0.000 description 2
- 229920002451 polyvinyl alcohol Polymers 0.000 description 2
- 238000010926 purge Methods 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- 239000011592 zinc chloride Substances 0.000 description 2
- 235000005074 zinc chloride Nutrition 0.000 description 2
- 239000002028 Biomass Substances 0.000 description 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000003213 activating effect Effects 0.000 description 1
- 239000012080 ambient air Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000005587 bubbling Effects 0.000 description 1
- 239000003990 capacitor Substances 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 229910002091 carbon monoxide Inorganic materials 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000013626 chemical specie Substances 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 229910001882 dioxygen Inorganic materials 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000000921 elemental analysis Methods 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 238000004898 kneading Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000003607 modifier Substances 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 150000003112 potassium compounds Chemical class 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 238000006557 surface reaction Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- -1 tetraethylammonium tetrafluoroborate Chemical compound 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/20—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising free carbon; comprising carbon obtained by carbonising processes
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/30—Active carbon
- C01B32/312—Preparation
- C01B32/336—Preparation characterised by gaseous activating agents
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/30—Active carbon
- C01B32/312—Preparation
- C01B32/342—Preparation characterised by non-gaseous activating agents
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/22—Electrodes
- H01G11/30—Electrodes characterised by their material
- H01G11/32—Carbon-based
- H01G11/34—Carbon-based characterised by carbonisation or activation of carbon
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Power Engineering (AREA)
- Analytical Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Carbon And Carbon Compounds (AREA)
- Electric Double-Layer Capacitors Or The Like (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US12/264,568 | 2008-11-04 | ||
| US12/264,568 US8541338B2 (en) | 2008-11-04 | 2008-11-04 | Highly porous activated carbon with controlled oxygen content |
| PCT/US2009/063203 WO2010053939A1 (en) | 2008-11-04 | 2009-11-04 | Highly porous activated carbon with controlled oxygen content |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2012508155A JP2012508155A (ja) | 2012-04-05 |
| JP2012508155A5 JP2012508155A5 (enExample) | 2012-12-27 |
| JP5542146B2 true JP5542146B2 (ja) | 2014-07-09 |
Family
ID=41508765
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2011535635A Expired - Fee Related JP5542146B2 (ja) | 2008-11-04 | 2009-11-04 | 酸素含有量を制御した非常に多孔質の活性炭 |
Country Status (4)
| Country | Link |
|---|---|
| US (2) | US8541338B2 (enExample) |
| EP (1) | EP2362850A1 (enExample) |
| JP (1) | JP5542146B2 (enExample) |
| WO (1) | WO2010053939A1 (enExample) |
Families Citing this family (32)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8252716B2 (en) * | 2008-11-04 | 2012-08-28 | Corning Incorporated | Process for making porous activated carbon |
| JP5599186B2 (ja) * | 2009-12-28 | 2014-10-01 | Ｊｘ日鉱日石エネルギー株式会社 | 電気二重層キャパシタ電極用活性炭およびその製造方法 |
| US8198210B2 (en) * | 2010-05-27 | 2012-06-12 | Corning Incorporated | Halogenated activated carbon materials for high energy density ultracapacitors |
| EP2695176A4 (en) * | 2011-04-07 | 2015-04-29 | Retriev Technologies Inc | CARBON ELECTRODES AND ELECTROCHEMICAL CAPACITORS |
| US8842417B2 (en) * | 2011-09-23 | 2014-09-23 | Corning Incorporated | High voltage electro-chemical double layer capacitor |
| US8809231B2 (en) * | 2011-09-28 | 2014-08-19 | Corning Incorporated | Method for making alkali activated carbon |
| US20140017578A1 (en) * | 2012-07-11 | 2014-01-16 | Robert Bosch Gmbh | Reducing Oxygen and Electrolyte Transport Limitations in the Lithium/Oxygen Battery through Electrode Design and Wetting Control |
| US9640333B2 (en) * | 2012-10-03 | 2017-05-02 | Georgia Tech Research Corporation | High surface area carbon materials and methods for making same |
| US9552930B2 (en) | 2015-01-30 | 2017-01-24 | Corning Incorporated | Anode for lithium ion capacitor |
| WO2014134000A1 (en) * | 2013-02-28 | 2014-09-04 | Corning Incorporated | Chemical activation of carbon via an entrained stream method |
| US9464162B2 (en) * | 2013-03-13 | 2016-10-11 | Georgia-Pacific Chemicals Llc | Emulsion and suspension polymerization processes, and improved electrochemical performance for carbon derived from same |
| US9607775B2 (en) | 2013-08-30 | 2017-03-28 | Corning Incorporated | High-voltage and high-capacitance activated carbon and carbon-based electrodes |
| US9607776B2 (en) * | 2013-10-24 | 2017-03-28 | Corning Incorporated | Ultracapacitor with improved aging performance |
| CN104709905A (zh) * | 2013-12-16 | 2015-06-17 | 中国科学院兰州化学物理研究所 | 一种利用混合熔盐为活化剂制备超级电容器用活性炭的方法 |
| US9613760B2 (en) * | 2014-06-12 | 2017-04-04 | Corning Incorporated | Energy storage device and methods for making and use |
| US9679704B2 (en) | 2015-01-30 | 2017-06-13 | Corning Incorporated | Cathode for a lithium ion capacitor |
| US9911545B2 (en) | 2015-01-30 | 2018-03-06 | Corning Incorporated | Phenolic resin sourced carbon anode in a lithium ion capacitor |
| US9607778B2 (en) | 2015-01-30 | 2017-03-28 | Corning Incorporated | Poly-vinylidene difluoride anode binder in a lithium ion capacitor |
| US9672992B2 (en) | 2015-01-30 | 2017-06-06 | Corning Incorporated | Coke sourced anode for lithium ion capacitor |
| CN105642228B (zh) * | 2016-01-08 | 2017-11-07 | 桂林理工大学 | 一种用于吸附烟气中co2的活性炭的制备方法 |
| CN109155204B (zh) | 2016-05-20 | 2020-12-22 | 阿维科斯公司 | 用于超级电容器的电极构造体 |
| KR102635455B1 (ko) | 2016-05-20 | 2024-02-13 | 교세라 에이브이엑스 컴포넌츠 코포레이션 | 고온용 울트라커패시터 |
| EP3459097A4 (en) | 2016-05-20 | 2020-05-06 | AVX Corporation | NON-AQUEOUS ELECTROLYTE FOR SUPERCAPACITOR |
| KR102506938B1 (ko) * | 2018-02-02 | 2023-03-07 | 현대자동차 주식회사 | 활성탄소의 제조방법 |
| CN108389728B (zh) * | 2018-02-07 | 2020-10-30 | 中国地质大学（武汉） | 一种氮/磷/氧异质元素共掺杂碳电极材料的制备方法 |
| CN108910881A (zh) * | 2018-08-27 | 2018-11-30 | 天津市职业大学 | 一种制备高性能活性炭的复合活化剂及其应用 |
| CN110143592A (zh) * | 2019-07-05 | 2019-08-20 | 咖法科技(上海)有限公司 | 一种咖啡渣活性炭的制备方法 |
| CN113120904B (zh) * | 2019-12-31 | 2022-11-11 | 中国石油化工股份有限公司 | 一种活性炭处理方法 |
| CN111994905A (zh) * | 2020-08-14 | 2020-11-27 | 五邑大学 | 一种高性能碳材料的制备方法 |
| US12110456B2 (en) | 2020-08-28 | 2024-10-08 | Florrent, Inc. | Biomass-based method and composition |
| CN114713193B (zh) * | 2022-04-21 | 2023-11-14 | 华南师范大学 | 一种氮掺杂磁性多孔碳复合材料及其制备方法及应用 |
| CN118790992B (zh) * | 2024-09-13 | 2024-12-24 | 成都达奇科技股份有限公司 | 氮磷掺杂活性炭的制备方法 |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4656153A (en) * | 1983-02-28 | 1987-04-07 | Standard Oil Company (Indiana) | Active carbon containing a dispersion of a metal component and method for making same |
| US5776385A (en) * | 1994-04-15 | 1998-07-07 | Corning Incorporated | Method of making activated carbon composites from supported crosslinkable resins |
| JPH11297580A (ja) * | 1998-04-16 | 1999-10-29 | Mitsubishi Chemical Corp | 電気二重層キャパシター |
| US6156697A (en) * | 1997-11-04 | 2000-12-05 | Corning Incorporated | Method of producing high surface area carbon structures |
| US6248691B1 (en) * | 1998-02-10 | 2001-06-19 | Corning Incorporated | Method of making mesoporous carbon |
| JPH11250910A (ja) * | 1998-03-02 | 1999-09-17 | Toshiba Corp | リチウム二次電池 |
| DE60121705T2 (de) | 2000-05-09 | 2007-08-02 | Mitsubishi Chemical Corp. | Aktivierter kohlenstoff für elektrischen doppelschichtkondensator |
| JP2002083748A (ja) * | 2000-06-27 | 2002-03-22 | Asahi Glass Co Ltd | 活性炭およびその製造方法およびこれを用いた電気二重層キャパシタ |
| KR100777951B1 (ko) * | 2001-08-23 | 2007-11-28 | 더 프록터 앤드 갬블 캄파니 | 정수 필터 재료, 대응하는 정수 필터 및 그의 사용 방법 |
| JP2004067498A (ja) * | 2002-06-13 | 2004-03-04 | Kashima Oil Co Ltd | 活性炭およびそれを用いた電気二重層キャパシタ |
| JP2004221332A (ja) * | 2003-01-15 | 2004-08-05 | Gun Ei Chem Ind Co Ltd | 電気二重層キャパシタの電極用活性炭組成物及びその製造方法 |
| JP2005047788A (ja) * | 2003-02-12 | 2005-02-24 | Naoki Komatsu | フラーレンの製造方法 |
| JP2004273520A (ja) * | 2003-03-05 | 2004-09-30 | Petroleum Energy Center | キャパシタ電極用活性炭素繊維および電気二重層キャパシタ |
| JP2006024747A (ja) * | 2004-07-08 | 2006-01-26 | Mitsubishi Gas Chem Co Inc | 電気二重層キャパシタ電極用炭素材料およびその製造方法 |
| JP4560477B2 (ja) * | 2005-11-15 | 2010-10-13 | 日立オートモティブシステムズ株式会社 | 電子制御装置および防水ケース |
| FR2909483B1 (fr) * | 2006-11-30 | 2009-02-27 | Centre Nat Rech Scient | Un condensateur electrochimique avec deux electrodes en carbone de nature differente en milieu aqueux |
-
2008
- 2008-11-04 US US12/264,568 patent/US8541338B2/en not_active Expired - Fee Related
-
2009
- 2009-11-04 EP EP09748661A patent/EP2362850A1/en not_active Withdrawn
- 2009-11-04 WO PCT/US2009/063203 patent/WO2010053939A1/en not_active Ceased
- 2009-11-04 JP JP2011535635A patent/JP5542146B2/ja not_active Expired - Fee Related
-
2013
- 2013-08-22 US US13/973,392 patent/US9006136B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| US20100110611A1 (en) | 2010-05-06 |
| US20130342964A1 (en) | 2013-12-26 |
| US8541338B2 (en) | 2013-09-24 |
| WO2010053939A1 (en) | 2010-05-14 |
| EP2362850A1 (en) | 2011-09-07 |
| US9006136B2 (en) | 2015-04-14 |
| JP2012508155A (ja) | 2012-04-05 |
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