JP5518329B2 - 水素貯蔵複合材料 - Google Patents
水素貯蔵複合材料 Download PDFInfo
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Description
仮出願ではないこの出願は、35 U.S.C. § 119(e)に則り、U.S. Provisional Patent Application Serial No. 60/673,859(2005年04月22日出願、この参照により本開示に含まれる)の優先権の利益を請求する。
本発明にかかる実施形態群は、水素貯蔵複合材料に関する。特に、本発明にかかる実施形態群は、水素の吸蔵と脱着を行うための水素貯蔵複合材料に関する。
本明細書では、「水素貯蔵複合材料」("composite hydrogen storage material")という語は、結合剤と混合した活性物質粒子のことを指し、ここでこの結合剤は、活性物質粒子間の空間的な相対位置関係を保持する上で充分な程度に活性物質粒子を固定化するものである。
5グラムのLaNi5粉末(粒径約1ミクロン以下)を、0.2グラムのAtofina's 2851 kynarflex(弗化ポリビニリデン 誘導体)熱可塑性樹脂粉末(粒径約0.1ミクロン以下)と混合する。この混合物を、所望の形状をした鋳型を使い、約100MPaおよび165℃で圧縮成形する。その後、圧力を100MPaに保ちつつ、鋳型を室温まで冷却する。鋳型から取り出した部分は、孔隙率約28%の多孔質固体材料であり、質量5.2グラム、比重約5.2、LaNi5充填係数は約60%である。
5グラムのLaNi5粉末(粒径約1ミクロン以下)を、0.2グラムの黒鉛フレーク(粒径約1〜10ミクロン)および0.2グラムのAtofina's 2851 kynarflex(弗化ポリビニリデン 誘導体)熱可塑性樹脂粉末(粒径約0.1ミクロン以下)と混合する。この混合物を、所望の形状をした鋳型を使い、約100MPaおよび165℃で圧縮成形する。その後、圧力を100MPaに保ちつつ、鋳型を室温まで冷却する。鋳型から取り出した部分は、孔隙率約28%の多孔質固体材料であり、質量5.4グラム、比重約5.0、LaNi5充填係数は約56%である。黒鉛フレークの添加により、固体材料の強度と熱伝導性が増大する。こうした特性の改善によって、(鋳型から取り出した)部分の水素注入速度と構造的な完全性が改良されることになるという効果が得られる。
5グラムのLaNi5粉末(粒径約1ミクロン以下)を、0.2グラムのポリパラフェニレン-テレフタルアミド(Kevlar)繊維(直径約10〜20ミクロン、長さ約1〜2mm)および0.2グラムのAtofina's 2851 kynarflex(弗化ポリビニリデン 誘導体)熱可塑性樹脂粉末(粒径約0.1ミクロン以下)と混合する。この混合物を、所望の形状をした鋳型を使い、約100MPaおよび165℃で圧縮成形する。その後、圧力を100MPaに保ちつつ、鋳型を室温まで冷却する。鋳型から取り出した部分は、孔隙率約28%の多孔質固体材料であり、質量5.4グラム、比重約4.9、LaNi5充填係数は約53%である。ポリパラフェニレン-テレフタルアミド繊維の添加により、材料の強度が増す。
5グラムのLaNi5粉末(粒径約1ミクロン以下)を、0.2グラムの活性炭(粒径約1〜10ミクロン)および0.2グラムのAtofina's 2851 kynarflex(弗化ポリビニリデン 誘導体)熱可塑性樹脂粉末(粒径約0.1ミクロン以下)と混合する。この混合物を、所望の形状をした鋳型を使い、約100MPaおよび165℃で圧縮成形する。その後、圧力を100MPaに保ちつつ、鋳型を室温まで冷却する。鋳型から取り出した部分は、孔隙率約28%の多孔質固体材料であり、質量5.4グラム、比重約4.8、LaNi5充填係数は約52%である。活性炭によって、注入時に金属水素化物を汚染しかねない有害な化合物を吸着できる。
Claims (1)
- 水素貯蔵複合材料であって、
水素を吸蔵及び脱着することの可能な活性物質粒子であって、1ミクロン以下のサイズの活性物質粒子と、
カーボンフレーク、カーボンナノチューブ、ファイバーガラス、カーボンファイバー、カーボンナノファイバー、およびそれらの組み合わせ、から成る群から選択された構造的添加剤と、
前記活性物質粒子と直接接触している弗化ポリビニリデン熱可塑性結合剤であって、少なくとも20%の破壊伸びを有する弗化ポリビニリデン熱可塑性結合剤と、
を含み、
前記水素貯蔵複合材料が、15%から40%の孔隙率を有し、また、前記活性物質粒子が、前記水素貯蔵複合材料の少なくとも40%となる充填密度を有し、また、前記水素貯蔵複合材料が、水素の吸蔵及び脱着のサイクルを繰り返した後に、元の長さの少なくとも80%であって且つ120%を超えない長さを維持することを特徴とする、水素貯蔵複合材料。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US67385905P | 2005-04-22 | 2005-04-22 | |
US60/673,859 | 2005-04-22 | ||
PCT/CA2006/000588 WO2006111005A1 (en) | 2005-04-22 | 2006-04-24 | Composite hydrogen storage material and methods related thereto |
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JP2013021236A Division JP5816205B2 (ja) | 2005-04-22 | 2013-02-06 | 水素貯蔵複合材料、それを使用する方法、及びそれを使用した水素貯蔵システム |
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JP2008538321A JP2008538321A (ja) | 2008-10-23 |
JP5518329B2 true JP5518329B2 (ja) | 2014-06-11 |
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JP2008506893A Expired - Fee Related JP5518329B2 (ja) | 2005-04-22 | 2006-04-24 | 水素貯蔵複合材料 |
JP2013021236A Expired - Fee Related JP5816205B2 (ja) | 2005-04-22 | 2013-02-06 | 水素貯蔵複合材料、それを使用する方法、及びそれを使用した水素貯蔵システム |
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JP2013021236A Expired - Fee Related JP5816205B2 (ja) | 2005-04-22 | 2013-02-06 | 水素貯蔵複合材料、それを使用する方法、及びそれを使用した水素貯蔵システム |
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US (1) | US7708815B2 (ja) |
EP (1) | EP1874679A4 (ja) |
JP (2) | JP5518329B2 (ja) |
KR (2) | KR101160552B1 (ja) |
CN (1) | CN101203454B (ja) |
CA (1) | CA2605695C (ja) |
HK (1) | HK1122545A1 (ja) |
WO (1) | WO2006111005A1 (ja) |
Families Citing this family (70)
Publication number | Priority date | Publication date | Assignee | Title |
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US8518856B2 (en) * | 2003-05-30 | 2013-08-27 | Indiana University Research And Technology Corporation | Solid-state hydrogen storage media and catalytic hydrogen recharging thereof |
US20060283864A1 (en) * | 2005-02-10 | 2006-12-21 | Angstrom Power | Shipping container and method of use |
CA2605695C (en) * | 2005-04-22 | 2014-06-17 | Angstrom Power Incorporated | Composite hydrogen storage material and methods related thereto |
US8372184B2 (en) | 2005-04-22 | 2013-02-12 | Societe Bic | Composite hydrogen storage material and methods related thereto |
CN101395735B (zh) * | 2006-01-09 | 2013-05-01 | 法商Bic公司 | 便携式燃料电池及其方法 |
JP4957007B2 (ja) * | 2006-02-03 | 2012-06-20 | 日産自動車株式会社 | 水素発生システム、燃料電池システム及び燃料電池車両 |
US7563305B2 (en) * | 2006-06-23 | 2009-07-21 | Angstrom Power Incorporated | Fluid enclosure and methods related thereto |
US7891637B2 (en) * | 2006-11-07 | 2011-02-22 | Angstrom Power Incorporated | Magnetic fluid coupling assemblies and methods |
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KR101160552B1 (ko) | 2012-06-27 |
WO2006111005A1 (en) | 2006-10-26 |
CA2605695C (en) | 2014-06-17 |
EP1874679A4 (en) | 2011-11-16 |
CN101203454A (zh) | 2008-06-18 |
HK1122545A1 (en) | 2009-05-22 |
US20060237688A1 (en) | 2006-10-26 |
EP1874679A1 (en) | 2008-01-09 |
JP5816205B2 (ja) | 2015-11-18 |
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US7708815B2 (en) | 2010-05-04 |
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