JP5348099B2

JP5348099B2 - ポリマーエマルジョンの製造方法およびそれを含んでなるインク組成物

ポリマーエマルジョンの製造方法およびそれを含んでなるインク組成物 Download PDF

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Publication number: JP5348099B2
Authority: JP; Japan
Prior art keywords: pigment; emulsion; ink composition; polymer; polymer emulsion
Prior art date: 2000-10-12
Legal status : Expired - Fee Related

Application number

JP2010198580A

Other languages

English (en)

Japanese (ja)

Other versions

JP2011038105A (ja

Inventor

利行宮林

正弘矢竹

Current Assignee

Seiko Epson Corp

Original Assignee

Seiko Epson Corp

Priority date

2000-10-12

Filing date

2010-09-06

Publication date

2013-11-20

2010-09-06 Application filed by Seiko Epson Corp filed Critical Seiko Epson Corp

2010-09-06 Priority to JP2010198580A priority Critical patent/JP5348099B2/ja

2011-02-24 Publication of JP2011038105A publication Critical patent/JP2011038105A/ja

2013-11-20 Application granted granted Critical

2013-11-20 Publication of JP5348099B2 publication Critical patent/JP5348099B2/ja

2021-10-12 Anticipated expiration legal-status Critical

Status Expired - Fee Related legal-status Critical Current

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229920000642 polymer Polymers 0.000 title claims abstract description 164
239000000839 emulsion Substances 0.000 title claims abstract description 140
239000000203 mixture Substances 0.000 title claims abstract description 92
238000004519 manufacturing process Methods 0.000 title claims abstract description 17
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 80
239000000178 monomer Substances 0.000 claims abstract description 45
239000003505 polymerization initiator Substances 0.000 claims abstract description 19
238000007720 emulsion polymerization reaction Methods 0.000 claims abstract description 11
239000003995 emulsifying agent Substances 0.000 claims abstract description 10
229910001853 inorganic hydroxide Inorganic materials 0.000 claims abstract description 10
238000002156 mixing Methods 0.000 claims abstract description 10
239000000049 pigment Substances 0.000 claims description 126
239000002245 particle Substances 0.000 claims description 58
238000000034 method Methods 0.000 claims description 45
239000003960 organic solvent Substances 0.000 claims description 20
125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims description 15
125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims description 14
230000007935 neutral effect Effects 0.000 claims description 5
239000000976 ink Substances 0.000 description 123
-1 glycol ethers Chemical class 0.000 description 63
239000010419 fine particle Substances 0.000 description 55
238000011156 evaluation Methods 0.000 description 53
238000006243 chemical reaction Methods 0.000 description 42
239000003795 chemical substances by application Substances 0.000 description 33
PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 28
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 27
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DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 description 22
235000019333 sodium laurylsulphate Nutrition 0.000 description 22
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239000002609 medium Substances 0.000 description 17
239000004094 surface-active agent Substances 0.000 description 17
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150000001875 compounds Chemical class 0.000 description 15
230000032683 aging Effects 0.000 description 14
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238000010992 reflux Methods 0.000 description 12
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239000003513 alkali Substances 0.000 description 11
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238000005259 measurement Methods 0.000 description 11
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239000000126 substance Substances 0.000 description 9
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238000006116 polymerization reaction Methods 0.000 description 8
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238000002834 transmittance Methods 0.000 description 7
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DBCAQXHNJOFNGC-UHFFFAOYSA-N 4-bromo-1,1,1-trifluorobutane Chemical compound FC(F)(F)CCCBr DBCAQXHNJOFNGC-UHFFFAOYSA-N 0.000 description 6
SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 description 6
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SMWDFEZZVXVKRB-UHFFFAOYSA-N Quinoline Chemical compound N1=CC=CC2=CC=CC=C21 SMWDFEZZVXVKRB-UHFFFAOYSA-N 0.000 description 6
239000002253 acid Substances 0.000 description 6
ROOXNKNUYICQNP-UHFFFAOYSA-N ammonium persulfate Chemical compound [NH4+].[NH4+].[O-]S(=O)(=O)OOS([O-])(=O)=O ROOXNKNUYICQNP-UHFFFAOYSA-N 0.000 description 6
230000008859 change Effects 0.000 description 6
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239000003002 pH adjusting agent Substances 0.000 description 6
IEQIEDJGQAUEQZ-UHFFFAOYSA-N phthalocyanine Chemical compound N1C(N=C2C3=CC=CC=C3C(N=C3C4=CC=CC=C4C(=N4)N3)=N2)=C(C=CC=C2)C2=C1N=C1C2=CC=CC=C2C4=N1 IEQIEDJGQAUEQZ-UHFFFAOYSA-N 0.000 description 6
239000002002 slurry Substances 0.000 description 6
235000000346 sugar Nutrition 0.000 description 6
229920002554 vinyl polymer Polymers 0.000 description 6
229920002126 Acrylic acid copolymer Polymers 0.000 description 5
KWIUHFFTVRNATP-UHFFFAOYSA-N Betaine Natural products C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 description 5
KWIUHFFTVRNATP-UHFFFAOYSA-O N,N,N-trimethylglycinium Chemical compound C[N+](C)(C)CC(O)=O KWIUHFFTVRNATP-UHFFFAOYSA-O 0.000 description 5
GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 description 5
125000000217 alkyl group Chemical group 0.000 description 5
239000012736 aqueous medium Substances 0.000 description 5
DMSMPAJRVJJAGA-UHFFFAOYSA-N benzo[d]isothiazol-3-one Chemical compound C1=CC=C2C(=O)NSC2=C1 DMSMPAJRVJJAGA-UHFFFAOYSA-N 0.000 description 5
229960003237 betaine Drugs 0.000 description 5
230000021523 carboxylation Effects 0.000 description 5
238000006473 carboxylation reaction Methods 0.000 description 5
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238000005342 ion exchange Methods 0.000 description 5
229920001223 polyethylene glycol Polymers 0.000 description 5
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150000008163 sugars Chemical class 0.000 description 5
AOPDRZXCEAKHHW-UHFFFAOYSA-N 1-pentoxypentane Chemical compound CCCCCOCCCCC AOPDRZXCEAKHHW-UHFFFAOYSA-N 0.000 description 4
POAOYUHQDCAZBD-UHFFFAOYSA-N 2-butoxyethanol Chemical compound CCCCOCCO POAOYUHQDCAZBD-UHFFFAOYSA-N 0.000 description 4
SVTBMSDMJJWYQN-UHFFFAOYSA-N 2-methylpentane-2,4-diol Chemical compound CC(O)CC(C)(C)O SVTBMSDMJJWYQN-UHFFFAOYSA-N 0.000 description 4
JFGQHAHJWJBOPD-UHFFFAOYSA-N 3-hydroxy-n-phenylnaphthalene-2-carboxamide Chemical compound OC1=CC2=CC=CC=C2C=C1C(=O)NC1=CC=CC=C1 JFGQHAHJWJBOPD-UHFFFAOYSA-N 0.000 description 4
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 4
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229910019142 PO4 Inorganic materials 0.000 description 4
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 4
235000010443 alginic acid Nutrition 0.000 description 4
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239000011324 bead Substances 0.000 description 4
238000005452 bending Methods 0.000 description 4
XCJYREBRNVKWGJ-UHFFFAOYSA-N copper(II) phthalocyanine Chemical compound [Cu+2].C12=CC=CC=C2C(N=C2[N-]C(C3=CC=CC=C32)=N2)=NC1=NC([C]1C=CC=CC1=1)=NC=1N=C1[C]3C=CC=CC3=C2[N-]1 XCJYREBRNVKWGJ-UHFFFAOYSA-N 0.000 description 4
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VOZRXNHHFUQHIL-UHFFFAOYSA-N glycidyl methacrylate Chemical compound CC(=C)C(=O)OCC1CO1 VOZRXNHHFUQHIL-UHFFFAOYSA-N 0.000 description 4
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PXZQEOJJUGGUIB-UHFFFAOYSA-N isoindolin-1-one Chemical compound C1=CC=C2C(=O)NCC2=C1 PXZQEOJJUGGUIB-UHFFFAOYSA-N 0.000 description 4
229910021645 metal ion Inorganic materials 0.000 description 4
239000012860 organic pigment Substances 0.000 description 4
239000010452 phosphate Substances 0.000 description 4
YPFDHNVEDLHUCE-UHFFFAOYSA-N propane-1,3-diol Chemical compound OCCCO YPFDHNVEDLHUCE-UHFFFAOYSA-N 0.000 description 4
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230000002940 repellent Effects 0.000 description 4
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