JP5089887B2 - 生理活性物質含有複合体 - Google Patents
生理活性物質含有複合体 Download PDFInfo
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- JP5089887B2 JP5089887B2 JP2006014231A JP2006014231A JP5089887B2 JP 5089887 B2 JP5089887 B2 JP 5089887B2 JP 2006014231 A JP2006014231 A JP 2006014231A JP 2006014231 A JP2006014231 A JP 2006014231A JP 5089887 B2 JP5089887 B2 JP 5089887B2
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- GBFLQPIIIRJQLU-UHFFFAOYSA-L zinc;tetradecanoate Chemical compound [Zn+2].CCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCC([O-])=O GBFLQPIIIRJQLU-UHFFFAOYSA-L 0.000 description 1
- 239000001243 zingiber officinale rosc. root absolute Substances 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
- RZFHLOLGZPDCHJ-XZXLULOTSA-N α-Tocotrienol Chemical compound OC1=C(C)C(C)=C2O[C@@](CC/C=C(C)/CC/C=C(C)/CCC=C(C)C)(C)CCC2=C1C RZFHLOLGZPDCHJ-XZXLULOTSA-N 0.000 description 1
- 235000004835 α-tocopherol Nutrition 0.000 description 1
- 239000002076 α-tocopherol Substances 0.000 description 1
- 235000019145 α-tocotrienol Nutrition 0.000 description 1
- 239000011730 α-tocotrienol Substances 0.000 description 1
- 229930007845 β-thujaplicin Natural products 0.000 description 1
- 235000007680 β-tocopherol Nutrition 0.000 description 1
- 239000011590 β-tocopherol Substances 0.000 description 1
- 235000019151 β-tocotrienol Nutrition 0.000 description 1
- 239000011723 β-tocotrienol Substances 0.000 description 1
- FGYKUFVNYVMTAM-WAZJVIJMSA-N β-tocotrienol Chemical compound OC1=CC(C)=C2O[C@@](CC/C=C(C)/CC/C=C(C)/CCC=C(C)C)(C)CCC2=C1C FGYKUFVNYVMTAM-WAZJVIJMSA-N 0.000 description 1
- 239000002478 γ-tocopherol Substances 0.000 description 1
- QUEDXNHFTDJVIY-DQCZWYHMSA-N γ-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1 QUEDXNHFTDJVIY-DQCZWYHMSA-N 0.000 description 1
- 235000019150 γ-tocotrienol Nutrition 0.000 description 1
- 239000011722 γ-tocotrienol Substances 0.000 description 1
- OTXNTMVVOOBZCV-WAZJVIJMSA-N γ-tocotrienol Chemical compound OC1=C(C)C(C)=C2O[C@@](CC/C=C(C)/CC/C=C(C)/CCC=C(C)C)(C)CCC2=C1 OTXNTMVVOOBZCV-WAZJVIJMSA-N 0.000 description 1
- 235000019144 δ-tocotrienol Nutrition 0.000 description 1
- 239000011729 δ-tocotrienol Substances 0.000 description 1
- ODADKLYLWWCHNB-LDYBVBFYSA-N δ-tocotrienol Chemical compound OC1=CC(C)=C2O[C@@](CC/C=C(C)/CC/C=C(C)/CCC=C(C)C)(C)CCC2=C1 ODADKLYLWWCHNB-LDYBVBFYSA-N 0.000 description 1
Landscapes
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Non-Alcoholic Beverages (AREA)
- Medicinal Preparation (AREA)
- Cosmetics (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Description
ン脂質、リゾレシチン、水素添加大豆リン脂質、部分水素添加大豆リン脂質、水素添加卵黄リン脂質、部分水素添加卵黄リン脂質、水酸化レシチン等のリン脂質類;シリコーン系両性界面活性剤等;高分子界面活性剤では、ポリビニルアルコール、アルギン酸ナトリウム、デンプン誘導体、トラガントガム、アクリル酸・メタアクリル酸アルキル共重合体、2−メタクロイルオキシエチルホスホリルコリン・ステアリルメタクリレート共重合体;シリコーン系各種界面活性剤が好ましいものとして挙げられる。
アスタキサンチン20%油懸濁液(武田紙器製)1gとフィトステロール(タマ生化学製)0.3gと水添大豆レシチン(ホスホリピッド社製ホスホリポン90H)8.7gとをt−ブチルアルコール90gに溶解させた後、液体窒素にて瞬時に凍結し、凍結乾燥装置(東京理化器械製、FDU−2200型)にて凍結乾燥を行った。圧力は10Pa以下、トラップ温度は−80℃とした。このようにして得られた複合体は、均質な赤色の粉末であった。
20%ルテイン油懸濁液(光洋商会製)1gとフィトステロール(タマ生化学製)1gと水添大豆レシチン(ホスホリピッド社製ホスホリポン90H)8gとをt−ブチルアルコール90gに溶解させた後、液体窒素にて瞬時に凍結し、凍結乾燥装置(東京理化器械製、FDU−2200型)にて凍結乾燥を行った。圧力は10Pa以下、トラップ温度は−80℃とした。このようにして得られた複合体は、均質な橙色の粉末であった。
γ−オリザノール(築野食品製)1gと水添大豆レシチン(ホスホリピッド社製ホスホリポン90H)9gとをt−ブチルアルコール90gに溶解させた後、液体窒素にて瞬時に凍結し、凍結乾燥装置(東京理化器械製、FDU−2200型)にて凍結乾燥を行った。圧力は10Pa以下、トラップ温度は−80℃とした。このようにして得られた複合体は、均質な白色の粉末であった。
クエルセチン(和光純薬製)0.1gとフィトステロール(タマ生化学製)1gと水添大豆レシチン(ホスホリピッド社製ホスホリポン90H)8.8gとをt−ブチルアルコール90gに溶解させた後、液体窒素にて瞬時に凍結し、凍結乾燥装置(東京理化器械製、FDU−2200型)にて凍結乾燥を行った。圧力は10Pa以下、トラップ温度は−80℃とした。このようにして得られた複合体は、均質な黄色の粉末であった。
ヘスペリジン(和光純薬製)0.2gとフィトステロール(タマ生化学製)0.5gと水添大豆レシチン(ホスホリピッド社製ホスホリポン90H)9.3gとをt−ブチルアルコール90gに溶解させた後、液体窒素にて瞬時に凍結し、凍結乾燥装置(東京理化器械製、FDU−2200型)にて凍結乾燥を行った。圧力は10Pa以下、トラップ温度は−80℃とした。このようにして得られた複合体は、均質な白色の粉末であった。
ゲニステイン及びゲニスチンを主成分とするイソフラボンを40%、サポニンを10%含有する大豆抽出物(光洋商会製、ソルゲン40)1gと水添大豆レシチン(ツルーレシチン製SLPホワイトH)9gとをt−ブチルアルコール90gに溶解させた後、液体窒素にて瞬時に凍結し、凍結乾燥装置(東京理化器械製、FDU−2200型)にて凍結乾燥を行った。圧力は10Pa以下、トラップ温度は−80℃とした。このようにして得られた複合体は、均質な白色の粉末であった。
フェルラ酸(築野食品製)1gとフィトステロール(タマ生化学製)1gと水添大豆レシチン(ホスホリピッド社製ホスホリポン90H)8gとをt−ブチルアルコール90gに溶解させた後、液体窒素にて瞬時に凍結し、凍結乾燥装置(東京理化器械製、FDU−2200型)にて凍結乾燥を行った。圧力は10Pa以下、トラップ温度は−80℃とした。このようにして得られた複合体は、均質な白色の粉末であった。
β−カロテン(和光純薬製)0.2gとフィトステロール(タマ生化学製)1gと水添大豆レシチン(ホスホリピッド社製ホスホリポン90H)8.8gとをシクロヘキサン90gに溶解させた後、噴霧乾燥装置(東京理化機械(株)製、スプレードライヤーSD−1型)で噴霧乾燥した。噴霧空気圧力は1.5kg/cm2、送液速度は5g/分、チャンバー入口温度は65℃、出口温度は40℃とした。このようにして得られた複合体は、均質な橙色の粉末であった。
プロアントシアニジン(キッコーマン製)0.2gとフィトステロール(タマ生化学製)0.5gと水添大豆レシチン(ホスホリピッド社製ホスホリポン90H)9.3gとをシクロヘキサン90gに溶解させた後、噴霧乾燥装置(東京理化機械(株)製、スプレードライヤーSD−1型)で噴霧乾燥した。噴霧空気圧力は1.5kg/cm2、送液速度は5g/分、チャンバー入口温度は65℃、出口温度は40℃とした。このようにして得られた複合体は、均質な茶色の粉末であった。
9%レチノール油懸濁液(理研ビタミン製)1.0gとd−δ−トコフェロール(エーザイ製)0.1gとコレステロール(日本精化製)1gと水添大豆レシチン(ホスホリピッド社製ホスホリポン90H)7.9gとをシクロヘキサン90gに溶解させた後、噴霧乾燥装置(東京理化機械(株)製、スプレードライヤーSD−1型)で噴霧乾燥した。噴霧空気圧力は1.5kg/cm2、送液速度は5g/分、チャンバー入口温度は65℃、出口温度は40℃とした。このようにして得られた複合体は、均質な赤色の粉末であった。
硫酸シトステロール(アリスタライフサイエンス製)1gと水添大豆レシチン(ツルーレシチン製SLPホワイトH)9gとをシクロヘキサン90gに溶解させた後、噴霧乾燥装置(東京理化機械(株)製、スプレードライヤーSD−1型)で噴霧乾燥した。噴霧空気圧力は1.5kg/cm2、送液速度は5g/分、チャンバー入口温度は65℃、出口温度は40℃とした。このようにして得られた複合体は、均質な白色の粉末であった。
コエンザイムQ10(日清ファーマ製)100gと50%トコトリエノール(カロテック社製)10gとフィトステロール(日本精化製)50gと水添大豆レシチン(ホスホリピッド社製ホスホリポン90H)840gとをシクロヘキサン80Lに溶解させた後、瞬間真空乾燥機(ホソカワミクロン製、CRUX8B型)を用いて噴霧乾燥した。加熱管の温度を70℃、出口に設けられた真空室の真空度を60〜70mmHgとした。このようにして得られた複合体は均質な黄色の粉末であった。
α−リポ酸(立山化成製)50gとフィトステロール(タマ生化学製)30gと水添大豆レシチン(ホスホリピッド社製ホスホリポン90H)920gとをシクロヘキサン100Lに溶解させた後、瞬間真空乾燥機(ホソカワミクロン製、CRUX8B型)を用いて噴霧乾燥した。加熱管の温度を70℃、出口に設けられた真空室の真空度を60〜70mmHgとした。このようにして得られた複合体は均質な淡黄色の粉末であった。
製造例1で得られた複合体0.2gを1,3−ブチレングリコール10gに分散後、この液を水90gに添加し、ホモミキサー(特殊機化製)にて攪拌(70℃、5000rpm、20分)した。得られた分散液はやや透明感のある赤色の液であった。
製造例2で得られた複合体を用いて、実施例1と同様にして水分散液を作製した。得られた分散液はやや透明感のある橙色の液であった。
製造例3で得られた複合体を用いて、実施例1と同様にして水分散液を作製した。得られた分散液はやや透明感のある白色の液であった。
製造例4で得られた複合体を用いて、実施例1と同様にして水分散液を作製した。得られた分散液はやや透明感のある黄色の液であった。
製造例5で得られた複合体を用いて、実施例1と同様にして水分散液を作製した。得られた分散液はやや透明感のある白色の液であった。
製造例6で得られた複合体を用いて、実施例1と同様にして水分散液を作製した。得られた分散液はやや透明感のある白色の液であった。
製造例7で得られた複合体を用いて、実施例1と同様にして水分散液を作製した。得られた分散液はやや透明感のある白色の液であった。
製造例8で得られた複合体を用いて、実施例1と同様にして水分散液を作製した。得られた分散液はやや透明感のある橙色の液であった。
製造例9で得られた複合体を用いて、実施例1と同様にして水分散液を作製した。得られた分散液はやや透明感のある薄茶色の液であった。
製造例10で得られた複合体を用いて、実施例1と同様にして水分散液を作製した。得られた分散液はやや透明感のある赤色の液であった。
製造例11で得られた複合体を用いて、実施例1と同様にして水分散液を作製した。得られた分散液はやや透明感のある白色の液であった。
製造例12で得られた複合体を用いて、実施例1と同様にして水分散液を作製した。得られた分散液はやや透明感のある橙色の液であった。
製造例13で得られた複合体を用いて、実施例1と同様にして水分散液を作製した。得られた分散液はやや透明感のある黄色の液であった。
製造例1の複合体と同じ組成の混合物(各成分を混ぜ合わせたのみ)0.2gを1,3−ブチレングリコール10gに分散後、この液を水90gに添加し、ホモミキサー(特殊機化製)にて攪拌(70℃、5000rpm、20分)した。得られた分散液はやや透明感のある赤色の液であったが、沈降物が存在した。
製造例2の複合体と同じ組成の混合物(各成分を混ぜ合わせたのみ)を比較例1と同様にして水分散液を作製した。得られた分散液はやや透明感のある橙色の液であったが、沈降物が存在した。
製造例12の複合体と同じ組成の混合物(各成分を混ぜ合わせたのみ)を比較例1と同様にして水分散液を作製した。得られた分散液はやや透明感のある橙色の液であったが、沈降物が存在した。
製造例13の複合体と同じ組成の混合物(各成分を混ぜ合わせたのみ)を比較例1と同様にして水分散液を作製した。得られた分散液はやや透明感のある黄色の液であったが、沈降物が存在した。
製造例1の複合体と同じ組成の混合物(各成分を混ぜ合わせたのみ)0.2gを1,3−ブチレングリコール10gに分散後、この液を水90gに添加し、ホモミキサー(特殊機化製)にて攪拌(70℃、5000rpm、20分)した後、さらに高圧乳化機(みずほ工業製マイクロフルイダイザー)にて分散させた。得られた分散液はやや透明感のある赤色の液であった。
製造例2の複合体と同じ組成の混合物(各成分を混ぜ合わせたのみ)を比較例5と同様にして水分散液を作製した。得られた分散液はやや透明感のある橙色の液であった。
製造例12の複合体と同じ組成の混合物(各成分を混ぜ合わせたのみ)を比較例5と同様にして水分散液を作製した。得られた分散液はやや透明感のある橙色の液であった。
製造例13の複合体と同じ組成の混合物(各成分を混ぜ合わせたのみ)を比較例5と同様にして水分散液を作製した。得られた分散液はやや透明感のある黄色の液であった。
フィトステロール0.3g(タマ生化学製)と水添大豆レシチン(ホスホリピッド社製ホスホリポン90H)8.7gとをt−ブチルアルコール90gに溶解させた後、液体窒素にて瞬時に凍結し、凍結乾燥装置(東京理化器械製、FDU−2200型)にて凍結乾燥を行い、フィトステロール−リン脂質複合体を作製した。この複合体0.18gと20%アスタキサンチン油懸濁液(武田紙器製)0.02gを1,3−ブチレングリコール10gに分散後、この液を水90gに添加し、ホモミキサー(特殊機化製)にて攪拌(70℃、5000rpm、20分)した。得られた分散液はやや透明感のある赤色の液であった。
フィトステロール1g(タマ生化学製)と水添大豆レシチン(ホスホリピッド社製ホスホリポン90H)8gとをt−ブチルアルコール90gに溶解させた後、液体窒素にて瞬時に凍結し、凍結乾燥装置(東京理化器械製、FDU−2200型)にて凍結乾燥を行い、フィトステロール−リン脂質複合体を作製した。この複合体0.18gと20%ルテイン油懸濁液(光洋商会製)0.02gを1,3−ブチレングリコール10gに分散後、この液を水90gに添加し、ホモミキサー(特殊機化製)にて攪拌(70℃、5000rpm、20分)した。得られた分散液はやや透明感のある赤色の液であった。
フィトステロール200g(タマ生化学製)と水添大豆レシチン(ホスホリピッド社製ホスホリポン90H)800gとをシクロヘキサン100Lに溶解させた後、瞬間真空乾燥機(ホソカワミクロン製、CRUX8B型)を用いて噴霧乾燥を行い、フィトステロール−リン脂質複合体を作製した。この複合体0.18gとコエンザイムQ10(日清ファーマ製)0.015g、50%トコトリエノール(カロテック社製)0.005gを1,3−ブチレングリコール10gに分散後、この液を水90gに添加し、ホモミキサー(特殊機化製)にて攪拌(70℃、5000rpm、20分)した。得られた分散液はやや透明感のある黄色の液であった。
フィトステロール200g(タマ生化学製)と水添大豆レシチン(ホスホリピッド社製ホスホリポン90H)800gとをシクロヘキサン100Lに溶解させた後、瞬間真空乾燥機(ホソカワミクロン製、CRUX8B型)を用いて噴霧乾燥を行い、フィトステロール−リン脂質複合体を作製した。この複合体0.18gとα−リポ酸(立山化成製)0.02gを1,3−ブチレングリコール10gに分散後、この液を水90gに添加し、ホモミキサー(特殊機化製)にて攪拌(70℃、5000rpm、20分)した。得られた分散液はやや透明感のある黄色の液であった。
実施例1〜13、及び、比較例1〜12で得られた水分散液について、50℃、1ヶ月の分散安定性試験を実施した(表1)。結果、本発明の複合体を用いた実施例1〜13の水分散液は50℃、1ヶ月後も沈降物はなく安定であった。それに対して複合化していない各成分をホモミキサーにて攪拌して作製した比較例1〜4の水分散液は作製直後から沈降物が存在し安定な分散液にはならなかった。また、複合化していない各成分をホモミキサーにて攪拌後、さらに高圧乳化機にて分散させた比較例5〜8の水分散液は、作製直後こそ沈降物は見られなかったが、50℃、1ヶ月後には沈降物が確認された。さらに、ステロールとリン脂質のみを複合体し、この複合体と難水溶性の生理活性物質をホモミキサーにて攪拌して作製した比較例9〜12の水分散液に関しても、50℃、1ヶ月後には沈降物が確認された。このことより、難水溶性の生理活性物質とリン脂質、あるいは、難水溶性の生理活性物質とステロールとリン脂質を複合化することにより、安定な水分散液が得られることが明らかとなった。また、その分散液の調製方法はホモミキサーで攪拌するだけの簡便なものであった。
――――――――――――――――――――――――――――
分散安定性(50℃/1ヶ月後)
――――――――――――――――――――――――――――
実施例1 ◎
実施例2 ◎
実施例3 ◎
実施例4 ◎
実施例5 ◎
実施例6 ◎
実施例7 ◎
実施例8 ◎
実施例9 ◎
実施例10 ◎
実施例11 ◎
実施例12 ◎
実施例13 ◎
比較例1 ×
比較例2 ×
比較例3 ×
比較例4 ×
比較例5 ○
比較例6 △
比較例7 ○
比較例8 ○
比較例9 △
比較例10 ○
比較例11 △
比較例12 ○
――――――――――――――――――――――――――
評価基準
◎:沈降物は見られない
○:わずかに沈降物が見られる
△:沈降物あり
×:作製直後から沈降物あり
実施例1〜13で得られた水分散液について、粒度分布計(マルバーン社製ゼータサイダー)を用いて平均粒子径を測定した(表2)。結果、いずれの分散液も100nm以下であった。さらに50℃、1ヶ月後の平均粒子径も測定したところ、平均粒子径はほとんど変化がないことが確認された。
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
平均粒子径(作成直後) 平均粒子径(50℃/1ヶ月後)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
製造例1の複合体 74 nm 77 nm
製造例2の複合体 68 70
製造例3の複合体 85 83
製造例4の複合体 69 72
製造例5の複合体 75 75
製造例6の複合体 72 75
製造例7の複合体 79 79
製造例8の複合体 68 70
製造例9の複合体 70 68
製造例10の複合体 77 77
製造例11の複合体 80 85
製造例12の複合体 82 83
製造例13の複合体 77 80
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
アスタキサンチンを水に分散させた実施例1、比較例1、比較例5、比較例9の分散液について、皮膚へ塗布した際の官能試験を実施した。7名のパネラーが皮膚上での伸び、すべり感、べたつきのなさの3項目について評価し、その結果を表3にまとめた。結果、実施例1の分散液がもっとも感触に優れることが分かった。このことより、複合化せずに水に分散液させるよりも、複合化した方が得られる分散液の感触が向上することが確認された。よって、本発明の複合体は化粧料または皮膚外用剤に使用した際に、良好な感触が得られるものと考えられた。
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
皮膚上での伸び すべり感 べたつきのなさ
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
実施例1 ◎ ◎ ◎
比較例1 △ × △
比較例5 ◎ ○ ○
比較例9 ◎ △ △
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
評価基準
◎:極めて良好
○:良好
△:やや不良
×:不良
レチノールとビタミンEを含有する実施例10の水分散液について、レチノールの安定性試験を実施した。レチノールの定量はHPLC法にて行った。比較として、界面活性剤(POE(20)セチルアルコールエーテル)を用いて実施例10と同じ濃度のレチノールとビタミンEを水に乳化させた組成物についても同様に試験した。表4に25℃で7日間保存した後のレチノールの残存率を示した。結果、比較とした乳化組成物に対して、実施例10の水分散液の方が、レチノールの残存率が高かった。よって、本発明の複合体を用いて水に分散させることにより、難水溶性の生理活性物質であるレチノールの水中での安定性が向上することが分かった。
−−−−−−−−−−−−−−−−−−−−−−−−−
残存率(25℃/7日後)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
実施例10の水分散液 89%
比較の乳化組成物 60%
−−−−−−−−−−−−−−−−−−−−−−−−−−
造例2の複合体を用いて下記処方の化粧水を作製した。得られた化粧水は安定性が高く、使用感も良好で効果の持続するものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 BG 2.0
2 グリセリン 3.0
3 クエン酸 0.01
4 クエン酸Na 0.1
5 キサンタンガム 0.05
6 製造例2の複合体 1.0
7 オレイン酸ソルビタン 0.1
8 テトラオレイン酸ソルベス−60 0.9
9 エタノール 7.0
10 防腐剤 適量
11 香料 微量
12 精製水 残余
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(製造方法)
各成分を70℃で均一に撹拌混合した。
製造例3の複合体を用いて下記処方のローションを作製した。得られたローションは安定性が高く、使用感に優れるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 BG 2.0
2 マルチトール 1.0
3 クエン酸 0.1
4 クエン酸Na 0.05
5 フェノールスルホン酸亜鉛 0.1
6 製造例3の複合体 1.5
7 PEG−60水添ヒマシ油 0.5
8 エタノール 15.0
9 防腐剤 適量
10 香料 微量
11 精製水 残余
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(製造方法)
各成分を70℃で均一に撹拌混合した。
製造例1、12の複合体を用いて下記処方の化粧水を作製した。得られた化粧水は安定性が高く、使用感も良好で効果の持続するものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 乳酸 0.01
2 乳酸ナトリウム 0.1
3 ピロリドンカルボン酸ナトリウム 1.0
4 1,3−ブチレングリコール 3.0
5 ジプロピレングリコール 1.0
6 精製水 残余
7 製造例12の複合体 1.5
8 製造例1の複合体 0.5
9 ポリオキシエチレン硬化ヒマシ油 0.2
10 防腐剤 適量
11 セラミド3 0.01
12 セラミド2 0.01
13 フィトスフィンゴシン 1.0
14 エタノール 10.0
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(製造方法)
No.1〜6を50℃で攪拌混合した(A部)。No.7〜14を50℃で攪拌混合した(B部)。BをAに撹拌しながら徐々に加え可溶化した。撹拌しながら冷却し,30℃で攪拌を留め、放置した。
製造例4の複合体を用いて下記処方のエモリエントミルクを作製した。得られたエモリエントミルクは安定性が高く、伸びが良くてしっとり感を付与するものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 製造例4の複合体 1.5
2 YOFCO MAS(日本精化) 2.0
3 イソオクタン酸セチル 2.0
4 トリオクタン酸トリメチロールプロパン 3.0
5 パルミチン酸イソステアリル 4.0
6 トリオクタノイン 4.0
7 スクワラン 2.0
8 ミリスチルアルコール 1.0
9 水添パーム油 3.5
10 ステアリン酸グリセリル(SE) 1.5
11 ステアリン酸グリセリル 3.0
12 ステアリン酸ソルビタン 1.0
13 ポリソルベート65 0.5
14 ステアリン酸PEG−40 0.5
15 ジメチコン 1.5
16 水添レシチン 0.05
17 プロピルパラベン 0.15
18 BG 5.0
19 グリセリン 3.0
20 フェノキシエタノール 0.2
21 メチルパラベン 0.1
22 精製水 残余
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(製造方法)
No.2〜17を約80℃に加温し、溶解させた(A部)。No.1、No.18〜22を約80℃に加温し溶解させた(B部)。A部にB部を加えホモミキサーにて乳化させた後、40℃まで冷却した。
製造例5の複合体を用いて下記処方の乳液を作製した。得られた乳液は安定性が高く、伸びが良くてしっとり感を付与するものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 Phytopresome Cera−2 1.0
(日本精化)
2 製造例5の複合体 0.5
3 ステアリン酸 2.0
4 ワセリン 3.0
5 セチルアルコール 1.0
6 ベヘニルアルコール 0.5
7 ソルビタンモノオレイン酸エステル 2.0
8 ポリエチレングリコール1500 3.0
9 1,3−ブチレングリコール 5.0
10 トリエタノールアミン 1.0
11 キサンタンガム 0.1
12 香料 適量
13 防腐剤 適量
14 精製水 残余
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(製造方法)
No.1、2、8、9、10、11、14を加え70℃に加熱混合した(水相)。その他の成分を混合し70℃に加熱溶解した(油相)。水相にかき混ぜながら油相を徐々に加え予備乳化した。更に乳化機にて均一に乳化して室温まで冷却した。
製造例13の複合体を用いて下記処方の乳液を作製した。得られた乳液は安定性が高く、使用感に優れるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 製造例13の複合体 1.5
2 セバシン酸ジエチル 1.0
3 グリセリン 10.0
4 キサンタンガム 0.05
5 Tremoist−TP(日本精化) 0.05
6 ヒドロキシプロピルセルロース 0.1
7 1,2−ペンタンジオール 0.1
8 アルブチン 3.0
9 精製水 残余
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(調製方法)
No.1〜3を約70℃に加温混合した(A部)。別容器でNo.7〜9を70℃で混合溶解させた(B部)。B部にA部を加え、ホモミキサーにて乳化させた。さらにNo.4〜6を加えホモミキサーにて攪拌した後、40℃まで冷却した。
製造例9の複合体を用いて下記処方の乳液を作製した。得られた乳液は安定性が高く、使用感に優れるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 スクワラン 2.0
2 YOFCO MAC(日本精化) 1.0
3 製造例9の複合体 1.0
4 Presome R−3(日本精化) 1.0
5 Lipidure PMB(日本油脂) 0.01
6 ステアリン酸 2.0
7 ワセリン 3.0
8 セチルアルコール 1.0
9 ソルビタンモノオレイン酸エステル 2.0
10 ポリエチレングリコール1500 3.0
11 1,3−ブチレングリコール 5.0
12 トリエタノールアミン 1.0
13 香料、防腐剤 適量
14 精製水 残余
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(製造方法)
No.3、4、5、10〜14を混合し80℃で加熱溶解した(水相)。その他の成分を混合し80℃で加熱溶解した(油相)。水相に油相をかき混ぜながら徐々に加え予備乳化した。更に乳化機にて均一に乳化して室温まで冷却した。
製造例6の複合体を用いて下記処方のエモリエントクリームを作製した。得られたエモリエントクリームは安定性が高く、塗布した際の伸びが良く保湿効果に優れるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 製造例6の複合体 1.5
2 YOFCO MAS(日本精化) 1.0
3 Phytocompo−PP(日本精化)1.0
4 ステアリン酸 3.0
5 ワセリン 6.0
6 セチルアルコール 5.0
7 L−カルノシン 0.05
8 POE(20)セチルアルコールエーテル 2.0
9 PPGモノステアリン酸エステル 3.0
10 ジプロピレングリコール 3.0
11 グリセリン 3.0
12 アルブチン(日本精化) 0.5
13 DES(日本精化) 1.0
14 トリエタノールアミン 1.0
15 防腐剤、酸化防止剤 適量
16 精製水 残余
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(製造方法)
No.1、7、10、11、12、14、15.16を混合し70℃で加温溶解した(水相)。その他の成分を混合し70℃で加温溶解した(油相)。水相にかき混ぜながら油相を徐々に加え攪拌した後、乳化機で均一に乳化し室温まで冷却した。
製造例9の複合体を用いて下記処方のエモリエントクリームを作製した。得られたエモリエントクリームは安定性が高く、塗布した際の伸びが良く保湿効果に優れるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 製造例9の複合体 1.5
2 IOTG(日本精化) 3.0
3 Composite−PC (日本精化) 1.0
4 ベヘニルアルコール 6.0
5 BG 5.0
6 メチルパラベン 0.1
7 フェノキシエタノール 0.4
8. スクワラン 25.0
9 ジステアリン酸Al 1.6
10 ステアリン酸Mg 1.6
11 マイクロクリスタリンワックス 3.0
12 硫酸マグネシウム 0.5
13 精製水 残余
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(製造方法)
No.8〜11を一旦約150℃に加温し、均一に溶解させた(A部)。No.2、4〜7を約80℃に加温し、溶解させた(B部)。No.1、3、12、13を約80℃に加温した(C部)。約80℃でA部にB部を加えて混合した。攪拌しながらC部を徐々に加え、1分間攪拌後急冷した。
製造例1、8の複合体を用いて下記処方のエモリエントクリームを作製した。得られたエモリエントクリームは安定性が高く、塗布した際の伸びが良く保湿効果に優れるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 スクワラン 10.0
2 IOTG(日本精化) 7.0
3 製造例8の複合体 1.5
4 製造例1の複合体 1.0
5 セチルアルコール 5.0
6 ステアリン酸 3.0
7 POE(20)セチルアルコールエーテル 3.0
8 PPGモノステアリン酸エステル 3.0
9 ジプロピレングリコール 5.0
10 α−リポ酸 1.0
11 セバシン酸ジエチル 1.0
12 アスコルビン酸−2−グルコシド 0.5
13 グリセリン 5.0
14 トリエタノールアミン 1.0
15 防腐剤、酸化防止剤 適量
16 精製水 残余
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(製造方法)
No.3、4、9、12、13、14、16を混合し70℃で加温溶解した(水相)。その他の成分を混合し70℃で加温溶解した(油相)。水相にかき混ぜながら油相を徐々に加え攪拌した後、乳化機で均一に乳化し室温まで冷却した。
製造例2の複合体を用いて下記処方のサンスクリーンを作製した。得られたサンスクリーンは安定性が高く、使用感に優れるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 製造例2の複合体 10.0
2 スクワラン 22.5
3 IOTG(日本精化) 2.7
4 ジステアリン酸Al 1.6
5 ステアリン酸Mg 1.6
6 マイクロクリスタリンワックス 2.7
7 ベヘニルアルコール 4.8
8 酸化チタン 9.0
9 BG 5.0
10 メチルパラベン 0.2
11 Neosolue−DE(日本精化) 1.0
12 コレステロール(日本精化) 0.8
13 プロピルパラベン 0.2
14 硫酸Mg 0.5
15 精製水 残余
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(製造方法)
No.8にNo.2の一部、No.3を秤りとり、ミルで混練した(A部)。No.2の残り、NO.4〜6を約150℃に加温して溶解した(B部)。No.7、11、12、13を秤りとり、約80℃に加温して溶解した(C部)。No.1、9、10、14、15を約80℃に加温して溶解すした(D部)。B部にC部を加えて混合した後、A部加えて均一にした(E部)。E部にD部を加えて攪拌し、乳化後40℃まで冷却した。
製造例7の複合体を用いて下記処方のサンスクリーンを作製した。得られたサンスクリーンは安定性が高く、使用感に優れるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 微粒子酸化チタン 5.0
2 イオン交換水 54.95
3 1,3−ブチレングリコール 7.0
4 エデト酸二ナトリウム 0.05
5 トリエタノールアミン 1.0
6 製造例7の複合体 1.5
7 パラメトキシ桂皮酸オクチル 5.0
8 スクワラン 10.0
9 オキシベンゾン 2.0
10 Neosolue−MP(日本精化) 3.0
11 ステアリン酸 3.0
12 グリセリルモノステアレート 3.0
13 ポリアクリル酸エチル 1.0
14 酸化防止剤 適量
15 防腐剤 適量
16 香料 適量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(製造方法)
No.2〜6を70℃に加熱し溶解させた。これにNo.1を加え十分分散させた。この中にNo.7〜16を加熱溶解させたものを加え、ホモジナイザーを用いて乳化分散し、室温まで撹拌冷却した。
製造例5、10の複合体を用いて下記処方の口紅を作製した。得られた口紅は安定性が高く、艶があり塗布感に優れるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 LUSPLAN DD−DHR(日本精化)10.0
2 Plandool−H(日本精化) 38.5
3 製造例10の複合体 0.5
4 製造例5の複合体 1.0
5 LUSPLAN PI−DA(日本精化) 20.0
6 カルナウバロウ 3.0
7 キャンデリラロウ 6.0
8 セレシン 5.0
9 マキシリップ 1.0
10 α―リポ酸 0.1
11 二酸化チタン 6.0
12 赤色201号 1.0
13 赤色202号 2.0
14 酸化鉄黒 1.0
15 香料、酸化防止剤 適量
16 精製水 残量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(製造方法)
No.11〜14をNo.2の一部に加えローラーで練り、均一に混合した(A部)。No.1、2、5、6、7、8、9、10、15を混合し加熱溶解した(B部)。更にNo.16に溶解したNo.3、4を加え、ホモミキサーで均一に分散した(C部)。B部にA部を加え、さらにC部を加えて分散、脱気後、型に流し込み急冷し、スティック状とした。
製造例10の複合体を用いて下記処方のリップグロスを作製した。得られたリップグロスは安定性が高く、艶があり塗布感に優れるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 ポリエチレンワックス (m.p.88℃) 0.2
2 12−ヒドロキシステアリン酸 1.5
3 Plandool−S(日本精化) 35.0
4 LUSPLAN DD−DA7(日本精化) 35.0
5 製造例10の複合体 1.0
6 流動パラフィン 13.3
7 煙霧状シリカ 2.0
アエロジルR972(日本アエロジル)
8 雲母チタン 12.0
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
( 製造方法 )
No.1〜6を均一に加熱混合した後、No.7〜8を加え、均一に混合する。これを容器に充填した。
製造例4の複合体を用いて下記処方のファンデーションを作製した。得られたファンデーションは安定性が高く、使用感に優れるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 製造例4の複合体 2.0
2 タルク 24.0
3 酸化鉄 1.9
4 酸化チタン 20.0
5 シクロメチコン 3.5
6 トリメチルシロキシケイ酸 1.5
7 ジメチコン 2.0
8 トコフェロール 0.1
9 メトキシケイヒ酸オクチル 1.0
10 フェノキシエタノール 0.4
11 マイカ 残余
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(製造方法)
No.1〜No.11を高速攪拌し、均一に混合した。
製造例6の複合体を用いて下記処方の乳化ファンデーションを作製した。得られた乳化ファンデーションは安定性が高く、使用感に優れるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 イオン交換水 57.4
2 分散剤 0.1
3 ジプロピレングリコール 5.0
4 防腐剤 適量
5 製造例6の複合体 1.5
6 デカメチルシクロペンタシロキサン 12.0
7 POE変性ジメチルポリシロキサン 4.0
8 亜鉛華 10.0
9 セリサイト 0.36
10 二酸化チタン 8.32
11 酸化鉄黄 0.8
12.酸化鉄赤 0.36
13 酸化鉄黒 0.16
14 香料 適量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(製造方法)
No.1〜5を70℃に加熱撹拌後、No.9〜13を添加し分散処理した。これをあらかじめ70℃に加熱しておいたNo.6〜8に添加して乳化分散した。その後室温まで冷却してNo.14を加えた。
製造例11の複合体を用いて下記処方のクレンジングジェルを作製した。得られたクレンジングジェルは安定性が高く、使用後もつっぱり感がなく、良好な使用感を有するものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 製造例11の複合体 2.0
2 IOTG(日本精化) 15.0
3 ベルポールDC−30(日本精化) 2.0
4 LUSPLAN DD−IS(日本精化) 15.0
5 PEG−25水添ヒマシ油 20.0
6 グリセリン 16.0
7 BG 5.0
8 ネオペンタン酸イソデシル 1.0
9 精製水 残余
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(製造方法)
No.2〜No.8を秤りとり、約80℃に加温して溶解した(A部)。No.1、No.9を秤りとり、約80℃に加温した(B部)。攪拌しながらA部にB部を徐々に加え、乳化後40℃まで冷却した。
製造例7の複合体を用いて下記処方の洗顔フォームを作製した。得られた洗顔フォームは安定性が高く、使用後の皮膚につるっとすべり感、しっとり感を与えるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 (ヤシ脂肪酸/水添牛脂脂肪酸) 20.0
グルタミン酸Na
2 1,3−ブチレングリコール 14.0
3 製造例7の複合体 1.0
4 ポリエチレングリコール400 5.0
5 ポリエチレングリコール1500 10.0
6 ラウリン酸ジエタノールアミド 2.0
7 1,2−ペンタンジオール 0.1
8 1,2−ヘキサンジオール 0.2
9 Lipidure A(日本油脂) 1.0
10 結晶セルロース 10.0
11 ステアリン酸ブチル 1.0
12 トコフェロール 0.2
13 精製水 残余
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(製造方法)
No.1〜8、11を約80℃に加温し溶解させた。溶解後No.12、13を加え、溶解させた。約60℃で攪拌しながら、No.9、10を加え約40℃まで冷却した。
製造例5の複合体を用いて下記処方のボディシャンプーを作製した。得られたボディシャンプーは安定性が高く、使用後の皮膚につるっとすべり感、しっとり感を与えるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 ラウリル硫酸TEA(40%) 40.0
2 ラウレス硫酸Na(30%) 20.0
3 ラウラミドDEA 5.0
4 パルミチン酸グリセリル 1.0
5 製造例5の複合体 1.0
6 Lipidure NR(日本油脂) 1.0
7 PG 5.0
8 香料 0.2
9 メチルパラベン 0.1
10 プロピルパラベン 0.2
11 Plandool−G(日本精化) 1.0
12 精製水 25.5
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(製造方法)
No.1〜13を約80℃に加温し均一に溶解させ、攪拌しながら冷却した。
製造例3の複合体を用いて下記処方のヘアコンディショナーを作製した。得られたヘアコンディショナーは安定性が高く、毛髪にさらっとしたすべり感を与えるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 製造例3の複合体 2.0
2 ベヘニルアルコール 8.0
3 ラノリン 1.0
4 2−オクチルドデカノール 6.0
5 イソオクタン酸セチル 4.0
6 POE(7)オレイルエーテル 2.0
7 1,3−ブチレングリコール 12.0
8 防腐・殺菌剤 適量
9 香料・色素 適量
10 精製水 残量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(製造方法)
No.1〜6を混合し70℃で加温溶解した(A部)。No.7〜10を混合し70℃で加温溶解した(B部)。A部にB成分を加え混合し、撹拌しながら30℃まで冷却した。
製造例12の複合体を用いて下記処方の乳化型皮膚外用剤を作製した。得られた乳化型皮膚外用剤は安定性が高く、使用感に優れるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 製造例12の複合体 1.0
2 ヘキシレングリコール 10.0
3 植物性スクワラン 1.0
4 精製水 残量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(製造方法)
No.1〜3を混合し70℃に加温後、同じく70℃に加温した精製水を加えホモジナイザーで分散させた。
製造例6の複合体を用いて下記処方の乳飲料を作製した。得られた乳飲料は安定性が高く、嗜好性に優れるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 製造例6の複合体 2.0
2 大豆たんぱく質 10.0
3 果糖・ブドウ糖液糖 5.0
4 デキストリン 10.0
5 精製大豆油 4.0
6 ショ糖脂肪酸エステル 0.2
7 香料 適量
8 精製水 残量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(製造方法)
全成分を混ぜ合わせてホモミキサーにて攪拌し、1次乳化した。この液を80℃まで加温し、高圧乳化機にて2次乳化を行った。
製造例13の複合体を用いて下記処方のヨーグルト飲料を作製した。得られたヨーグルト飲料は安定性が高く、嗜好性に優れるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 製造例13の複合体 0.5
2 ヨーグルト 45.0
3 果糖・ブドウ糖液糖 5.0
4 MHペクチン 10.0
5 オレンジ果汁(12%) 30.0
6 香料 適量
7 精製水 残量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(製造方法)
全成分を混ぜ合わせてホモミキサーにて攪拌し、1次乳化した。この液を80℃まで加温し、高圧乳化機にて2次乳化を行った。
製造例12の複合体を用いて下記処方の清涼飲料を作製した。得られた清涼飲料は安定性が高く、嗜好性に優れるものであった。
成 分 配合量(重量%)
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
1 製造例12の複合体 0.2
2 オレンジ透明果汁 0.2
3 果糖・ブドウ糖液糖 15.0
4 L−アスコルビン酸 0.1
5 クエン酸 0.2
6 クエン酸ナトリウム 0.05
7 香料 適量
8 精製水 残量
−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−−
(製造方法)
全成分を混合後、約70℃まで加温しホモミキサーにて攪拌混合した。
Claims (3)
- 以下の(A)〜(C);
(A)α−カロテン、β−カロテン、γ−カロテン、リコピン、β−クリプトキサンチン、ルテイン、ゼアキサンチン、カンタキサンチン、アスタキサンチンから選ばれる1種又は2種以上のカロテノイド類
(B)ステロール
(C)リン脂質
が有機溶媒中に均一に溶解している溶液から有機溶媒を除去して、(A)〜(C)を同時に析出せしめて得られる乳化又は可溶化組成物の調製に使用される化粧料用のカロテノイド類−ステロール−リン脂質複合体において、(A):(B):(C)の重量比率が0.5〜50:0.5〜50:50〜99であることを特徴とする複合体 - カロテノイド類がアスタキサンチンであることを特徴とする請求項1に記載の複合体
- 請求項1又は2に記載の複合体を含有することを特徴とする化粧料
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WO2020137017A1 (ja) | 2018-12-26 | 2020-07-02 | 日本精化株式会社 | 美白剤、ヒアルロン酸産生促進剤、コラーゲン産生促進剤、細胞内活性酸素消去剤、刺激緩和剤、シワ改善剤、複合体、化粧料、及び皮膚外用剤 |
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