JP4824670B2 - 結合された高反応性硬質ポリウレタンフォーム - Google Patents

結合された高反応性硬質ポリウレタンフォーム Download PDF

Info

Publication number
JP4824670B2
JP4824670B2 JP2007502896A JP2007502896A JP4824670B2 JP 4824670 B2 JP4824670 B2 JP 4824670B2 JP 2007502896 A JP2007502896 A JP 2007502896A JP 2007502896 A JP2007502896 A JP 2007502896A JP 4824670 B2 JP4824670 B2 JP 4824670B2
Authority
JP
Japan
Prior art keywords
polyol
component
isocyanate
polyol component
polyisocyanate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP2007502896A
Other languages
English (en)
Japanese (ja)
Other versions
JP2007528434A (ja
JP2007528434A5 (cg-RX-API-DMAC7.html
Inventor
レコビック，フザイル
エル−カーティブ，アリ
ビンセント ビロット，フランク
オザサヒン，アリ
タバコビック，リファト
Original Assignee
ダウ グローバル テクノロジーズ エルエルシー
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=34961463&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=JP4824670(B2) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by ダウ グローバル テクノロジーズ エルエルシー filed Critical ダウ グローバル テクノロジーズ エルエルシー
Publication of JP2007528434A publication Critical patent/JP2007528434A/ja
Publication of JP2007528434A5 publication Critical patent/JP2007528434A5/ja
Application granted granted Critical
Publication of JP4824670B2 publication Critical patent/JP4824670B2/ja
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C08G18/4804—Two or more polyethers of different physical or chemical nature
    • C08G18/482—Mixtures of polyethers containing at least one polyether containing nitrogen
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/32—Polyhydroxy compounds; Polyamines; Hydroxyamines
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/10—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/67—Unsaturated compounds having active hydrogen
    • C08G18/671—Unsaturated compounds having only one group containing active hydrogen
    • C08G18/672—Esters of acrylic or alkyl acrylic acid having only one group containing active hydrogen
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C08J9/04—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent
    • C08J9/06—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent by a chemical blowing agent
    • C08J9/08—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent by a chemical blowing agent developing carbon dioxide
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00—Foam properties
    • C08G2110/0025—Foam properties rigid
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00—Foam properties
    • C08G2110/0041—Foam properties having specified density
    • C08G2110/0066—≥ 150kg/m3
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2350/00—Acoustic or vibration damping material
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2205/00—Foams characterised by their properties
    • C08J2205/10—Rigid foams
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2375/00—Characterised by the use of polyureas or polyurethanes; Derivatives of such polymers
    • C08J2375/04—Polyurethanes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • General Chemical & Material Sciences (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
JP2007502896A 2004-03-11 2005-03-07 結合された高反応性硬質ポリウレタンフォーム Expired - Fee Related JP4824670B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US55232104P 2004-03-11 2004-03-11
US60/552,321 2004-03-11
PCT/US2005/007323 WO2005090431A1 (en) 2004-03-11 2005-03-07 Attached, high reactivity rigid polyurethane foams

Publications (3)

Publication Number Publication Date
JP2007528434A JP2007528434A (ja) 2007-10-11
JP2007528434A5 JP2007528434A5 (cg-RX-API-DMAC7.html) 2008-04-24
JP4824670B2 true JP4824670B2 (ja) 2011-11-30

Family

ID=34961463

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2007502896A Expired - Fee Related JP4824670B2 (ja) 2004-03-11 2005-03-07 結合された高反応性硬質ポリウレタンフォーム

Country Status (11)

Country Link
US (1) US8372892B2 (cg-RX-API-DMAC7.html)
EP (1) EP1725600B2 (cg-RX-API-DMAC7.html)
JP (1) JP4824670B2 (cg-RX-API-DMAC7.html)
KR (1) KR101149662B1 (cg-RX-API-DMAC7.html)
CN (1) CN100519615C (cg-RX-API-DMAC7.html)
AT (1) ATE407161T1 (cg-RX-API-DMAC7.html)
BR (1) BRPI0508135A (cg-RX-API-DMAC7.html)
CA (1) CA2558634C (cg-RX-API-DMAC7.html)
DE (1) DE602005009505D1 (cg-RX-API-DMAC7.html)
ES (1) ES2309733T5 (cg-RX-API-DMAC7.html)
WO (1) WO2005090431A1 (cg-RX-API-DMAC7.html)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009508979A (ja) * 2005-09-15 2009-03-05 ダウ グローバル テクノロジーズ インコーポレイティド オキサゾリドン基を含む付着、高反応性硬質ポリウレタンフォーム

Families Citing this family (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7125461B2 (en) 2003-05-07 2006-10-24 L & L Products, Inc. Activatable material for sealing, baffling or reinforcing and method of forming same
US7199165B2 (en) 2003-06-26 2007-04-03 L & L Products, Inc. Expandable material
US8475694B2 (en) 2005-10-25 2013-07-02 Zephyros, Inc. Shaped expandable material
CN100372880C (zh) * 2006-06-08 2008-03-05 北京科聚化工新材料有限公司 一种储存稳定的聚氨酯预聚体及其制备方法
FR2919295B1 (fr) * 2007-07-25 2009-11-06 Rhodia Operations Sas Synthese d'urethanes et de polyurethanes catalysees par des carbenes.
DE102008008391A1 (de) * 2008-02-09 2009-08-13 Bayer Materialscience Ag Geschäumte, lichtechte Polyurethanformteile
GB0806434D0 (en) 2008-04-09 2008-05-14 Zephyros Inc Improvements in or relating to structural adhesives
GB0916205D0 (en) 2009-09-15 2009-10-28 Zephyros Inc Improvements in or relating to cavity filling
BR112012022319B1 (pt) 2010-03-04 2020-01-28 Zephyros Inc laminado estrutural compósito
GB201016530D0 (en) 2010-09-30 2010-11-17 Zephyros Inc Improvements in or relating to adhesives
DE102011078768A1 (de) 2011-07-07 2013-01-10 Bayer Materialscience Aktiengesellschaft Verfahren zum Ausfüllen von Hohl- und Zwischenräumen mit duroplastischen Polyurethanschaumstoffen
EP2736694B1 (en) 2011-07-26 2019-07-10 Dow Global Technologies LLC Method for filling hollow cavities with polymer foam
KR101351432B1 (ko) * 2011-12-27 2014-01-15 에스케이씨 주식회사 초미세 발포 폴리우레탄 탄성체의 제조방법
WO2014091500A1 (en) * 2012-12-13 2014-06-19 Varroc Polymers Pvt. Ltd. Polyurethane composite for automotive seat base.
EP3024871B1 (en) 2013-07-26 2022-12-07 Zephyros Inc. Thermosetting adhesive films including a fibrous carrier
JP6240959B2 (ja) * 2014-01-09 2017-12-06 株式会社アイ・イー・ジェー 硬質ウレタンフォームおよび軽石
EP3154929B1 (en) 2014-04-21 2020-09-16 Firestone Building Products Company, LLC Method of preparing a foam
GB201417985D0 (en) 2014-10-10 2014-11-26 Zephyros Inc Improvements in or relating to structural adhesives
US9464170B2 (en) * 2014-12-15 2016-10-11 The United States Of America, As Represented By The Secretary Of The Navy Controlling crosslinking density and processing parameters of phthalonitriles
PL415002A1 (pl) * 2015-12-01 2017-06-05 Selena Labs Spółka Z Ograniczoną Odpowiedzialnością Pianka montażowa oraz jej zastosowanie jako kleju, szczeliwa, do wytwarzania powłok albo do wypełniania wewnątrz pustych struktur
CN107522892B (zh) * 2016-06-02 2020-08-18 山东理工大学 碳酸氢有机胺盐类化合物及其作为发泡剂的用途
CN107089910B (zh) * 2016-06-02 2017-11-14 山东理工大学 碳酸有机胺盐类化合物及其作为发泡剂的用途
CN106279607A (zh) * 2016-08-08 2017-01-04 常州大学 一种以二氧化碳为环境友好型潜伏性发泡剂的聚氨酯泡沫材料及其制备方法
CN109422904B (zh) * 2017-08-24 2021-03-19 山东理工大学 包含仲胺和醇胺盐的发泡剂及用于聚氨酯连续板泡沫体材料中的用途
CN109679130B (zh) * 2017-10-19 2021-09-07 山东理工大学 包含六氟丁烯和有机醇胺盐化合物的复合发泡剂
MX2020009421A (es) * 2018-03-13 2020-11-06 Dow Global Technologies Llc Espuma viscoelastica.
JP7327904B2 (ja) * 2018-03-30 2023-08-16 マツダ株式会社 ２液反応型ウレタン樹脂組成物を用いたポリウレタンフォームの形成方法
CN114829436A (zh) * 2019-12-24 2022-07-29 科思创知识产权两合公司 用于形成具有空气渗透率的硬质聚氨酯泡沫的组合物和硬质聚氨酯泡沫
JP7685502B2 (ja) * 2020-02-04 2025-05-29 コベストロ、ドイチュラント、アクチエンゲゼルシャフト 通気性を有する硬質ポリウレタンフォーム形成用組成物及び硬質ポリウレタンフォーム
WO2025025200A1 (en) * 2023-08-03 2025-02-06 Ddp Specialty Electronic Materials Us, Llc Low density and flame retardant two-component polyurethane potting formulation

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH05287046A (ja) * 1992-04-06 1993-11-02 Mitsui Toatsu Chem Inc 発泡成形性の良い半硬質ポリウレタンフォームの製造法
JP2000169442A (ja) * 1998-11-16 2000-06-20 Basf Ag カルバメ―ト溶液
JP2000515893A (ja) * 1996-07-29 2000-11-28 ザ ダウ ケミカル カンパニー アルカノールアミン／二酸化炭素付加物及びポリウレタンフォーム
JP2001524995A (ja) * 1997-02-20 2001-12-04 住化バイエルウレタン株式会社 硬質ポリウレタンフォームの製造方法
JP2005506397A (ja) * 2001-04-01 2005-03-03 ダウ グローバル テクノロジーズ インコーポレイティド 硬質ポリウレタン発泡体
JP2005507964A (ja) * 2001-10-29 2005-03-24 ダウ グローバル テクノロジーズ インコーポレイティド 硬質ハイブリッド型ウレタンフォーム

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3312215A1 (de) * 1983-04-05 1984-10-11 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung eines zelligen polyurethans
DE3333464A1 (de) * 1983-09-16 1985-04-11 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung von mikrozellularen oder geschaeumten formkoerpern und zur durchfuehrung dieses verfahrens geeignete verbindungen mit gegenueber isocyanatgruppen reaktionsfaehigen gruppen
DE3607964A1 (de) * 1986-03-11 1987-09-17 Bayer Ag Verfahren zur herstellung eines zelligen polyurethans
CZ287435B6 (en) * 1993-11-04 2000-11-15 Bayer Ag Process for preparing foam polyurethane shaped parts without use of fluorochlorinated hydrocarbons
DE4405061A1 (de) * 1994-02-17 1995-08-24 Bayer Ag Verfahren zur Isolierung von Rohren mit Polyurethan-Hartschaumstoffen nach dem Rotationsgußverfahren
US5735970A (en) * 1996-05-30 1998-04-07 Air Liquide America Corporation Apparatus and process for the production of a neutral atmosphere
DE19742012A1 (de) * 1997-09-24 1999-03-25 Basf Ag Temperaturstabile Hartschaumstoffe auf Isocyanatbasis mit geringer Sprödigkeit und niedriger Wärmeleitfähigkeit
WO2007040617A1 (en) * 2005-09-15 2007-04-12 Dow Global Technologies, Inc. Attached, high reactivity rigid polyurethane foams containing oxazolidone groups

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH05287046A (ja) * 1992-04-06 1993-11-02 Mitsui Toatsu Chem Inc 発泡成形性の良い半硬質ポリウレタンフォームの製造法
JP2000515893A (ja) * 1996-07-29 2000-11-28 ザ ダウ ケミカル カンパニー アルカノールアミン／二酸化炭素付加物及びポリウレタンフォーム
JP2001524995A (ja) * 1997-02-20 2001-12-04 住化バイエルウレタン株式会社 硬質ポリウレタンフォームの製造方法
JP2000169442A (ja) * 1998-11-16 2000-06-20 Basf Ag カルバメ―ト溶液
JP2005506397A (ja) * 2001-04-01 2005-03-03 ダウ グローバル テクノロジーズ インコーポレイティド 硬質ポリウレタン発泡体
JP2005507964A (ja) * 2001-10-29 2005-03-24 ダウ グローバル テクノロジーズ インコーポレイティド 硬質ハイブリッド型ウレタンフォーム

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009508979A (ja) * 2005-09-15 2009-03-05 ダウ グローバル テクノロジーズ インコーポレイティド オキサゾリドン基を含む付着、高反応性硬質ポリウレタンフォーム

Also Published As

Publication number Publication date
ES2309733T3 (es) 2008-12-16
DE602005009505D1 (de) 2008-10-16
US8372892B2 (en) 2013-02-12
EP1725600B2 (en) 2012-10-03
CA2558634A1 (en) 2005-09-29
JP2007528434A (ja) 2007-10-11
WO2005090431A1 (en) 2005-09-29
KR20060129086A (ko) 2006-12-14
ATE407161T1 (de) 2008-09-15
EP1725600A1 (en) 2006-11-29
CA2558634C (en) 2013-02-26
CN100519615C (zh) 2009-07-29
KR101149662B1 (ko) 2012-07-05
US20080038461A1 (en) 2008-02-14
CN1930202A (zh) 2007-03-14
BRPI0508135A (pt) 2007-07-24
EP1725600B1 (en) 2008-09-03
ES2309733T5 (es) 2013-02-11

Similar Documents

Publication Publication Date Title
EP1725600B1 (en) Attached, high reactivity rigid polyurethane foams
US6803390B2 (en) Rigid polyurethane foams
CN1332994C (zh) 刚性复合聚氨酯泡沫体
CN101268110B (zh) 包含噁唑烷酮基团的、附着的高反应性硬聚氨酯泡沫
JP2007522325A (ja) バイオポリマー系低密度吸音発泡体
KR20070015920A (ko) 생체고분자에 기초한 저밀도 흡음 발포체
JP2004210880A (ja) インテグラルスキン付きポリウレタンフォームおよびその製造方法

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20080306

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20080306

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20110113

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20110118

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20110415

A602 Written permission of extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A602

Effective date: 20110422

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20110715

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20110809

A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20110908

R150 Certificate of patent or registration of utility model

Free format text: JAPANESE INTERMEDIATE CODE: R150

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20140916

Year of fee payment: 3

LAPS Cancellation because of no payment of annual fees