JP4750555B2 - ウール及びウール混合物のインジゴ染色方法 - Google Patents
ウール及びウール混合物のインジゴ染色方法 Download PDFInfo
- Publication number
- JP4750555B2 JP4750555B2 JP2005508890A JP2005508890A JP4750555B2 JP 4750555 B2 JP4750555 B2 JP 4750555B2 JP 2005508890 A JP2005508890 A JP 2005508890A JP 2005508890 A JP2005508890 A JP 2005508890A JP 4750555 B2 JP4750555 B2 JP 4750555B2
- Authority
- JP
- Japan
- Prior art keywords
- wool
- dyeing
- indigo
- seconds
- oxidation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
- D06P3/14—Wool
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/22—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using vat dyestuffs including indigo
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/22—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using vat dyestuffs including indigo
- D06P1/228—Indigo
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65168—Sulfur-containing compounds
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S8/00—Bleaching and dyeing; fluid treatment and chemical modification of textiles and fibers
- Y10S8/916—Natural fiber dyeing
- Y10S8/917—Wool or silk
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T442/00—Fabric [woven, knitted, or nonwoven textile or cloth, etc.]
- Y10T442/20—Coated or impregnated woven, knit, or nonwoven fabric which is not [a] associated with another preformed layer or fiber layer or, [b] with respect to woven and knit, characterized, respectively, by a particular or differential weave or knit, wherein the coating or impregnation is neither a foamed material nor a free metal or alloy layer
- Y10T442/2762—Coated or impregnated natural fiber fabric [e.g., cotton, wool, silk, linen, etc.]
Description
次の組成物を用いて浴を15℃に設定する。
酢酸 0.3-0.5 g/l
硫酸ナトリウム 1.5-3.0 g/l
バソラン(Basolan)DC(ジクロロイソシアヌル酸
ナトリウム無水物、収縮防止用化学物質) 3.0-5.0 g/l
pH 3.5-4.0
100%ウール
↓
経玉形成
長い成形(M/c.速度75−100mpm)
↓ クリール張力25−30g)
ロープ染色
インジゴ染色
↓
巻き返し(LCB上 M/C)(M/s.速度75−100mpm)
↓ ロープ張力5−10psi)
ノリ付け(sizing)
↓
製織
↓
織物硬化
↓
仕上げ
苛性ソーダ 1.5-3.0 g/l
ヒドロ亜硫酸ナトリウム 1.8-3.0 g/l
インジゴ 0.5-5.0 g/l
イオン性湿潤剤〔プリマゾール(Primasol)NF−
燐酸エステル塩〕 0.05-0.5 g/l
イオン性分散剤〔セタモール(Setamol)WS−
芳香族スルホン酸の縮合生成物〕 0.05-0.5 g/l
染料−浴温度 25℃- 35℃
pH 11.2-12.5
100%ウールヤーン
↓
直接整経
↓
インジゴ染色cumノリ付け
↓
織布
↓
仕上げ
苛性ソーダ 1.5-3.0 g/l
ヒドロ亜硫酸ナトリウム 1.8-3.0 g/l
インジゴ 0.5-5.0 g/l
イオン性湿潤剤(プリマゾールNF−燐酸エステル塩) 0.05-0.5 g/l
イオン性分散剤(セタモールWS−
芳香族スルホン酸の縮合生成物) 0.05-0.5 g/l
染料−浴温度 25℃- 35℃
pH 11.2-12.5
ウールトップのSR処理
↓
バッチ還元型でのトップ染色
↓
酸化
↓
洗浄
↓
乾燥
苛性ソーダ 1.5-3.0 g/l
ヒドロ亜硫酸ナトリウム 1.8-3.0 g/l
インジゴ 0.5-5.0 g/l
イオン性湿潤剤(プリマゾールNF−燐酸エステル塩) 0.05-0.5 g/l
イオン性分散剤(セタモールWS−
芳香族スルホン酸の縮合生成物) 0.05-0.5 g/l
染料−浴温度 25℃- 35℃
pH 11.2-12.5
臨界的処理パラメーター:
ロープ染色でウールヤーンのインジゴ染色のための臨界的処理パラメーター
処理工程図
クリール部分 M/C速度-23mpm (速度範囲16mpm-28mpm)
↓
洗浄箱−1 (繊維精錬:02g/l、プリマゾールNF(湿潤剤)、80℃)
↓
洗浄箱−1 (高温洗浄)50℃
↓
洗浄箱−3 (低温洗浄、室温)
↓ 16mpmの場合 28mpmの場合
染料箱−1(インジゴ染色) 浸漬時間−23.5秒 33.78秒 19.3秒
空気酸化 酸化時間−102 秒 146.6秒 83.78秒
↓
染料箱−2(インジゴ染色) 浸漬時間−23.5秒 33.78秒 19.3秒
空気酸化 酸化時間−102 秒 146.6秒 83.78秒
↓
染料箱−3(インジゴ染色) 浸漬時間−23.5秒 33.78秒 19.3秒
空気酸化 酸化時間−102 秒 146.6秒 83.78秒
↓
染料箱−4(インジゴ染色) 浸漬時間−23.5秒 33.78秒 19.3秒
空気酸化 酸化時間−102 秒 146.6秒 83.78秒
↓
染料箱−5(インジゴ染色) 浸漬時間−23.5秒 33.78秒 19.3秒
空気酸化 酸化時間−102 秒 146.6秒 83.78秒
↓
染料箱−6(インジゴ染色) 浸漬時間−23.5秒 33.78秒 19.3秒
空気酸化 酸化時間−102 秒 146.6秒 83.78秒
↓
染料箱−7(インジゴ染色) 浸漬時間−23.5秒 33.78秒 19.3秒
空気酸化 酸化時間−102 秒 146.6秒 83.78秒
↓
染料箱−8(インジゴ染色) 浸漬時間−23.5秒 33.78秒 19.3秒
空気酸化 酸化時間−102 秒 146.6秒 83.78秒
↓
洗浄箱−4 (高温洗浄)50℃
↓
洗浄箱−5 (高温洗浄)50℃
↓
洗浄箱−6 (酢酸 10g/l 、洗浄 60℃、pH 5-6)
↓
洗浄箱−7 (酢酸 10g/l 、洗浄 40℃、pH 5)
↓
乾燥(水蒸気加熱シリンダー、水蒸気圧 4.5バールまで)
Claims (7)
- 形状が安定なウール及びウール混合物を生成させるため前処理したウール及びウール混合物をインジゴで連続的に染色する方法において、前記前処理工程が、収縮防止剤を含浸させる工程を含み、前記前処理したウールを湿潤/洗浄工程にかけ、次にインジゴ染色/酸化及び洗浄工程にかけ、前記染色及び酸化工程が、前記洗浄したウール及びウール混合物をロイコインジゴ染料浴中で含浸させ、次に毎回酸化する工程を行う複数の工程を含み、更に洗浄、染色、及び酸化の工程を同じ機械で連続的に行う、連続的染色方法。
- 酸化工程を、空気に露出することにより行う、請求項1に記載の方法。
- 機械が16〜28mpmの速度を有する、請求項1に記載の方法。
- 各浴中での含浸時間及び酸化時間が、各段階で同じである、請求項1に記載の方法。
- 処理したウール及びウール混合物を、先ず湿潤剤で処理し、次に洗浄工程にかける、請求項1に記載の方法。
- ウールが、ばらばらの形態、トップ、かせ、パッケージ、コーン、チーズ、ビーム、ヤーンロープ/シート、及び織物の形態のウールから選択される、請求項1に記載の方法。
- 染料浴が、1.5〜3.0g/lの苛性ソーダ、1.8〜3.0g/lのヒドロ亜硫酸ナトリウム、0.5〜5.0g/lのインジゴ、0.05〜0.5g/lのイオン性湿潤剤(プリマゾールNF−燐酸エステルの塩)、0.05〜0.5g/lのイオン性分散剤(セタモールWS−芳香族スルホン酸の縮合生成物)の組成を有し、25℃〜35℃の染料浴温度、及び11.2〜12.5のpHを有する、請求項1に記載の方法。
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
PCT/IN2003/000318 WO2005026435A1 (en) | 2003-09-18 | 2003-09-18 | A process for indigo dyeing of wool and wool blends |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2007518884A JP2007518884A (ja) | 2007-07-12 |
JP4750555B2 true JP4750555B2 (ja) | 2011-08-17 |
Family
ID=34308038
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2005508890A Expired - Fee Related JP4750555B2 (ja) | 2003-09-18 | 2003-09-18 | ウール及びウール混合物のインジゴ染色方法 |
Country Status (5)
Country | Link |
---|---|
US (1) | US8187342B2 (ja) |
EP (1) | EP1668179B1 (ja) |
JP (1) | JP4750555B2 (ja) |
AU (1) | AU2003267813A1 (ja) |
WO (1) | WO2005026435A1 (ja) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2008544111A (ja) * | 2005-06-28 | 2008-12-04 | マルワ インダストリーズ リミテッド | 羊毛又は絹及びそれらの混合物(繊維/糸/編織物)をインジゴで染色する方法 |
JP5260856B2 (ja) * | 2006-11-10 | 2013-08-14 | 有限会社藍布屋 | 天然藍による木綿藍染め物品の染色方法 |
CN102453992B (zh) * | 2010-10-20 | 2014-03-26 | 上海中纺物产发展有限公司 | Esta纱线的生产方法 |
TR201817298A2 (tr) * | 2018-11-16 | 2019-02-21 | Denge Kimya Ve Tekstil Sanayi Ticaret Anonim Sirketi | Kapali si̇stem i̇ndi̇go parça boyama yöntemi̇ |
US11591748B2 (en) | 2020-01-14 | 2023-02-28 | Shadow Works, Llc | Heat treated multilayer knitted textile of liquid crystal polymer fibers and modified polyacrylonitrile fibers, and process for making same |
Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2450773A (en) * | 1944-03-30 | 1948-10-05 | Allied Chem & Dye Corp | Dyeing of wool with indigo dyestuffs |
GB1006893A (en) * | 1963-04-19 | 1965-10-06 | Basf Ag | Uniform dyeing of wool and fibre mixtures containing wool |
US3457022A (en) * | 1964-12-02 | 1969-07-22 | Cone Mills Corp | Process of dyeing cotton fibers with indigo vat dyes |
JPS49110998A (ja) * | 1973-03-07 | 1974-10-22 | ||
JPS5042198A (ja) * | 1973-08-20 | 1975-04-17 | ||
GB1488722A (en) * | 1974-04-09 | 1977-10-12 | South African Wool Board | Oxidation of wool and like keratin fibres |
JPH03287883A (ja) * | 1990-03-30 | 1991-12-18 | Kurabo Ind Ltd | 多色羊毛繊維製品の製法 |
JPH06184960A (ja) * | 1992-12-16 | 1994-07-05 | Kanebo Ltd | 羊毛繊維の染色方法 |
JPH0921077A (ja) * | 1995-07-06 | 1997-01-21 | Nara Pref Gov | 獣皮、動物性の、糸および織物の藍色染方法 |
Family Cites Families (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB372325A (en) | 1930-11-27 | 1932-04-27 | Ig Farbenindustrie Ag | Improvements in the treatment of fibrous materials |
US2254965A (en) * | 1933-09-22 | 1941-09-02 | Patcheni Ag Zur Beteiligung An | Process for the dyeing of fibrous materials |
GB448272A (en) | 1933-12-09 | 1936-06-05 | Ig Farbenindustrie Ag | Improvements in dyeing with vat dyestuffs |
US2367273A (en) * | 1939-10-30 | 1945-01-16 | Tootal Broadhurst Lee Co Ltd | Treatment of wool |
US3120480A (en) | 1961-08-02 | 1964-02-04 | Ledin Eric | Control rod for nuclear reactors |
UST100201I4 (en) * | 1980-02-07 | 1981-01-06 | E. I. Du Pont De Nemours And Company | Indigo dyeing of polyester fibers |
JPS60134080A (ja) * | 1983-12-16 | 1985-07-17 | 一方社油脂工業株式会社 | 繊維材料の染色性改良方法、カチオン性の繊維反応性化合物及びその製造方法 |
GB9014192D0 (en) * | 1990-06-26 | 1990-08-15 | Precision Proc Textiles Ltd | A method for the treatment of wool |
JPH04281079A (ja) | 1991-03-06 | 1992-10-06 | Takao Kimura | 糸と織物の染色方法 |
IT1255221B (it) * | 1992-07-14 | 1995-10-20 | Procedimento per la tintura in indaco di filati in matassa | |
US5611822A (en) * | 1993-05-10 | 1997-03-18 | Allegro Natural Dyes Llc | Indigo dye process |
DE10060048A1 (de) * | 2000-12-01 | 2002-06-06 | Bayer Ag | Filzfrei ausgerüstete Wolle und Verfahren zur Filzfreiausrüstung |
JP2004036037A (ja) | 2002-07-03 | 2004-02-05 | Nippon Sanmou Senshoku Kk | 絹・獣毛混紡繊維の染色方法及び染色された絹・獣毛混紡繊維 |
KR100477470B1 (ko) | 2002-11-20 | 2005-03-21 | 에스케이케미칼주식회사 | 산성염료 가염성 아세테이트 섬유의 제조방법 |
JP4067400B2 (ja) | 2002-12-27 | 2008-03-26 | 日本食品化工株式会社 | 澱粉組成物 |
US7235110B2 (en) * | 2004-02-18 | 2007-06-26 | Melvin Alpert | Method for dyeing fabric materials with indigo, other vat dyes, and sulfur dyes |
-
2003
- 2003-09-18 AU AU2003267813A patent/AU2003267813A1/en not_active Abandoned
- 2003-09-18 JP JP2005508890A patent/JP4750555B2/ja not_active Expired - Fee Related
- 2003-09-18 EP EP03748508.3A patent/EP1668179B1/en not_active Expired - Lifetime
- 2003-09-18 US US10/572,436 patent/US8187342B2/en not_active Expired - Fee Related
- 2003-09-18 WO PCT/IN2003/000318 patent/WO2005026435A1/en active Application Filing
Patent Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2450773A (en) * | 1944-03-30 | 1948-10-05 | Allied Chem & Dye Corp | Dyeing of wool with indigo dyestuffs |
GB1006893A (en) * | 1963-04-19 | 1965-10-06 | Basf Ag | Uniform dyeing of wool and fibre mixtures containing wool |
US3457022A (en) * | 1964-12-02 | 1969-07-22 | Cone Mills Corp | Process of dyeing cotton fibers with indigo vat dyes |
JPS49110998A (ja) * | 1973-03-07 | 1974-10-22 | ||
JPS5042198A (ja) * | 1973-08-20 | 1975-04-17 | ||
GB1488722A (en) * | 1974-04-09 | 1977-10-12 | South African Wool Board | Oxidation of wool and like keratin fibres |
JPH03287883A (ja) * | 1990-03-30 | 1991-12-18 | Kurabo Ind Ltd | 多色羊毛繊維製品の製法 |
JPH06184960A (ja) * | 1992-12-16 | 1994-07-05 | Kanebo Ltd | 羊毛繊維の染色方法 |
JPH0921077A (ja) * | 1995-07-06 | 1997-01-21 | Nara Pref Gov | 獣皮、動物性の、糸および織物の藍色染方法 |
Also Published As
Publication number | Publication date |
---|---|
EP1668179B1 (en) | 2016-03-30 |
EP1668179A1 (en) | 2006-06-14 |
WO2005026435A1 (en) | 2005-03-24 |
US8187342B2 (en) | 2012-05-29 |
JP2007518884A (ja) | 2007-07-12 |
AU2003267813A1 (en) | 2005-04-06 |
US20070107144A1 (en) | 2007-05-17 |
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