JP4410934B2 - アクリル酸及びアクリル酸エステルの製造法 - Google Patents

アクリル酸及びアクリル酸エステルの製造法 Download PDF

Info

Publication number
JP4410934B2
JP4410934B2 JP2000541129A JP2000541129A JP4410934B2 JP 4410934 B2 JP4410934 B2 JP 4410934B2 JP 2000541129 A JP2000541129 A JP 2000541129A JP 2000541129 A JP2000541129 A JP 2000541129A JP 4410934 B2 JP4410934 B2 JP 4410934B2
Authority
JP
Japan
Prior art keywords
acrylic acid
oligomeric
mixture containing
cooling
column
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
JP2000541129A
Other languages
English (en)
Japanese (ja)
Other versions
JP2002509902A5 (enExample
JP2002509902A (ja
Inventor
ネストラー ゲアハルト
シュレーダー ユルゲン
マッハハマー オットー
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of JP2002509902A publication Critical patent/JP2002509902A/ja
Publication of JP2002509902A5 publication Critical patent/JP2002509902A5/ja
Application granted granted Critical
Publication of JP4410934B2 publication Critical patent/JP4410934B2/ja
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • C07C51/252—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP2000541129A 1998-03-31 1999-03-24 アクリル酸及びアクリル酸エステルの製造法 Expired - Lifetime JP4410934B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE19814387A DE19814387A1 (de) 1998-03-31 1998-03-31 Verfahren zur Herstellung von Acrylsäure und Acrylsäureestern
DE19814387.7 1998-03-31
PCT/EP1999/001995 WO1999050219A1 (de) 1998-03-31 1999-03-24 Verfahren zur herstellung von acrylsäure und acrylsäureestern

Publications (3)

Publication Number Publication Date
JP2002509902A JP2002509902A (ja) 2002-04-02
JP2002509902A5 JP2002509902A5 (enExample) 2006-05-18
JP4410934B2 true JP4410934B2 (ja) 2010-02-10

Family

ID=7863103

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2000541129A Expired - Lifetime JP4410934B2 (ja) 1998-03-31 1999-03-24 アクリル酸及びアクリル酸エステルの製造法

Country Status (8)

Country Link
US (1) US6727383B1 (enExample)
EP (1) EP1066239B1 (enExample)
JP (1) JP4410934B2 (enExample)
CN (1) CN1107046C (enExample)
BR (1) BR9909309B1 (enExample)
DE (2) DE19814387A1 (enExample)
MY (1) MY119537A (enExample)
WO (1) WO1999050219A1 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002539104A (ja) * 1999-03-06 2002-11-19 ビーエーエスエフ アクチェンゲゼルシャフト アクリル酸の製造法

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10063161A1 (de) * 2000-12-18 2002-06-20 Basf Ag Verfahren zum Abschrecken eines heißen (Meth)acrylsäure enthaltenden Gasgemisches
WO2003095411A1 (de) * 2002-05-08 2003-11-20 Basf Aktiengesellschaft Verfahren zur herstellung von acrylsäure und/ oder deren ester sowie von propionsäure und/ oder deren ester im verbund
DE10300499A1 (de) * 2003-01-08 2003-10-23 Basf Ag Verfahren der rektifikativen Auftrennung von (Meth)acrylmonomere enthaltenden Fluiden
US8431743B2 (en) 2004-07-01 2013-04-30 Basf Aktiengesellschaft Preparation of acrylic acid by heterogeneously catalyzed partial gas phase oxidation of propylene
CN1930108B (zh) * 2004-08-02 2010-12-29 Lg化学株式会社 制备(甲基)丙烯酸的方法
TWI438187B (zh) * 2005-02-28 2014-05-21 Evonik Degussa Gmbh 丙烯酸和基於可再生原料之吸水聚合物結構及二者之製備方法
US7705181B2 (en) 2005-03-01 2010-04-27 Basf Akiengesellschaft Process for removing methacrylic acid from liquid phase comprising acrylic acid as a main constituent and target product, and methacrylic acid as a secondary component
US7601866B2 (en) 2005-03-01 2009-10-13 Basf Aktiengesellschaft Process for removing methacrolein from liquid phase comprising acrylic acid as a main constituent and target product, and methacrolein as a secondary component
KR100999428B1 (ko) * 2006-01-20 2010-12-09 니폰 쇼쿠바이 컴파니 리미티드 (메타)아크릴산의 제조 방법
JP5368673B2 (ja) * 2006-01-20 2013-12-18 株式会社日本触媒 （メタ）アクリル酸の製造方法
CN101516820B (zh) * 2006-09-15 2012-11-21 阿克马公司 制备丙烯酸的方法
DE102007043748A1 (de) 2007-09-13 2008-09-11 Basf Se Verfahren zur kontinuierlichen Abtrennung eines Zielproduktes X in Form von feinteiligem Kristallisat
DE102007043758A1 (de) 2007-09-13 2008-10-23 Basf Se Verfahren zum Betreiben einer kontinuierlichen Abtrennung eines Zielproduktes X in Form von feinteiligem Kristallisat des Zielproduktes X
BE1018537A3 (fr) 2007-09-13 2011-03-01 Basf Se Procede d'exploitation d'une separation en continu d'un produit cible x sous la forme d'un cristallisat finement divise.
KR101861855B1 (ko) 2008-07-28 2018-05-28 바스프 에스이 탄소원자 수가 ３개인 아크릴산의 전구체 화합물의 기체상 생성물 혼합물로부터 주성분으로서 함유된 아크릴산과 부산물로서 함유된 글리옥살을 분리시키는 방법
DE102008041573A1 (de) 2008-08-26 2010-03-04 Basf Se Verfahren zur Auftrennung von in einem Produktgasgemisch einer partiellen heterogen katalysierten Gasphasenoxidation einer C3-Vorläuferverbindung der Acrylsäure als Hauptbestandteil enhaltener Acrylsäure und als Nebenprodukt enthaltenem Glyoxal
DE102008040799A1 (de) 2008-07-28 2008-12-11 Basf Se Verfahren zur Auftrennung von in einem Produktgasgemisch einer partiellen heterogen katalysierten Gasphasenoxidation einer C3-Vorläuferverbindung der Acrylsäure als Hauptbestandteil enthaltener Acrylsäure und als Nebenprodukt enthaltenem Glyoxal
DE102010042216A1 (de) 2010-10-08 2011-06-09 Basf Se Verfahren zur Hemmung der unerwünschten radikalischen Polymerisation von in einer flüssigen Phase P befindlicher Acrylsäure
KR20160032994A (ko) * 2014-09-17 2016-03-25 주식회사 엘지화학 (메트)아크릴산의 회수 방법 및 회수 장치
CN104225942A (zh) * 2014-09-24 2014-12-24 南通中泰化工有限公司 丙烯酸异辛酯酯化反应中蒸发器冷凝水再利用系统装置
DE102014017815A1 (de) * 2014-12-03 2016-04-14 Basf Se Verfahren zur Gewinnung von Acrylsäure
KR102319305B1 (ko) * 2016-12-06 2021-10-28 주식회사 엘지화학 (메트)아크릴산의 회수 방법 및 장치
JP7384519B2 (ja) 2018-07-26 2023-11-21 ベーアーエスエフ・エスエー 液相ｐに存在するアクリル酸の望ましくないラジカル重合を抑制するための方法
CN115335354A (zh) 2020-03-26 2022-11-11 巴斯夫欧洲公司 抑制存在于液相p中的丙烯酸的不期望的自由基聚合的方法

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1127127A (en) 1966-04-26 1968-09-11 Bp Chem Int Ltd Stabilization of acrylic acid
US3555082A (en) * 1966-12-15 1971-01-12 Knapsack Ag Process for isolating acrylic acid from the reaction gases obtained by oxidation of propylene or acrolein
DE2121123C3 (de) 1971-04-29 1980-06-12 Basf Ag, 6700 Ludwigshafen Verfahren zum Abtrennen von Wasser aus wäßrigen Lösungen von Acrylsäure durch azeotrope Destillation
BE786398A (fr) 1971-07-21 1973-01-18 Basf Ag Procede de preparation de l'acide acrylique anhydre
IN151108B (enExample) * 1978-09-13 1983-02-19 Standard Oil Co
GB2146636B (en) 1983-08-11 1987-02-04 Nippon Catalytic Chem Ind Process for producing acrylic acid
US5154800A (en) 1992-01-31 1992-10-13 Lloyd Berg Dehydration of acrylic acid by extractive distillation
DE4308087C2 (de) 1993-03-13 1997-02-06 Basf Ag Verfahren zur Abtrennung von Acrylsäure aus den Reaktionsgasen der katalytischen Oxidation von Propylen und/oder Acrolein
DE19547485A1 (de) * 1995-12-19 1996-05-09 Basf Ag Verfahren zum Verestern von (Meth)acrylsäure mit einem Alkanol
DE19600955A1 (de) * 1996-01-12 1997-07-17 Basf Ag Verfahren zur Herstellung von Acrylsäure und deren Ester
DE19740253A1 (de) * 1997-09-12 1999-03-18 Basf Ag Verfahren zur fraktionierten Kondensation eines heißen Gasgemisches mit einem hohen Anteil nicht kondensierbarer Komponenten

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002539104A (ja) * 1999-03-06 2002-11-19 ビーエーエスエフ アクチェンゲゼルシャフト アクリル酸の製造法

Also Published As

Publication number Publication date
US6727383B1 (en) 2004-04-27
DE19814387A1 (de) 1999-10-07
JP2002509902A (ja) 2002-04-02
EP1066239A1 (de) 2001-01-10
WO1999050219A1 (de) 1999-10-07
EP1066239B1 (de) 2003-05-28
DE59905749D1 (de) 2003-07-03
CN1107046C (zh) 2003-04-30
BR9909309B1 (pt) 2011-11-01
CN1295552A (zh) 2001-05-16
BR9909309A (pt) 2000-11-21
MY119537A (en) 2005-06-30

Similar Documents

Publication Publication Date Title
JP4410934B2 (ja) アクリル酸及びアクリル酸エステルの製造法
JP5199260B2 (ja) アクリル酸の生成方法
JP4243016B2 (ja) アクリル酸およびメタクリル酸の製造方法
US10112885B2 (en) Process and system for producing acrylic acid
US6555707B1 (en) Method for producing acrylic acid and acrylic acids esters
CA2303373A1 (en) Method for the fractional condensation of a hot gas mixture containing acrylic acid or methacrylic acid and having a high proportion of non-condensable constituents
KR102263549B1 (ko) 개선된 (메트)아크릴산 제조 방법
CN1318378C (zh) (甲基)丙烯酸酯的制备方法
JP2012232996A (ja) （メタ）アクリル酸の製造方法
JP5021116B2 (ja) アクリル酸およびアクリル酸エステルの製造方法
JP2004529129A (ja) （メタ）アクリル酸を連続的に抽出する方法
KR100530967B1 (ko) 프로필렌 및/또는 아크롤레인의 산화로 수득한 아크릴산의정제 방법
KR101052710B1 (ko) 기체 기재의 산화에 의해 얻어진 (메트)아크릴산의정제방법
US8044237B2 (en) Method for production of aqueous (meth)acrylic acid
JP5368673B2 (ja) （メタ）アクリル酸の製造方法
JP4192465B2 (ja) （メタ）アクリル酸類製造時の副生物の分解方法
JP2001520213A (ja) （メタ）アクリル酸の製造方法
KR101092275B1 (ko) 기체 기질의 산화에 의해 발생한 (메트) 아크릴 산의 정제방법
CN115397801A (zh) 纯化(甲基)丙烯酸的方法

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20060322

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20060322

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20090206

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20090414

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20091016

A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20091116

R150 Certificate of patent or registration of utility model

Free format text: JAPANESE INTERMEDIATE CODE: R150

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20121120

Year of fee payment: 3

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20121120

Year of fee payment: 3

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20131120

Year of fee payment: 4

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

EXPY Cancellation because of completion of term