JP4181958B2 - 粉体化粧料 - Google Patents
粉体化粧料 Download PDFInfo
- Publication number
- JP4181958B2 JP4181958B2 JP2003339873A JP2003339873A JP4181958B2 JP 4181958 B2 JP4181958 B2 JP 4181958B2 JP 2003339873 A JP2003339873 A JP 2003339873A JP 2003339873 A JP2003339873 A JP 2003339873A JP 4181958 B2 JP4181958 B2 JP 4181958B2
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- JP
- Japan
- Prior art keywords
- powder
- component
- content
- coated
- cosmetic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- 239000000843 powder Substances 0.000 title claims description 120
- 239000002537 cosmetic Substances 0.000 title claims description 74
- -1 2-ethylhexyl paramethoxycinnamate Chemical compound 0.000 claims description 56
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- 239000003795 chemical substances by application Substances 0.000 claims description 6
- IEKHISJGRIEHRE-UHFFFAOYSA-N 16-methylheptadecanoic acid;propan-2-ol;titanium Chemical compound [Ti].CC(C)O.CC(C)CCCCCCCCCCCCCCC(O)=O.CC(C)CCCCCCCCCCCCCCC(O)=O.CC(C)CCCCCCCCCCCCCCC(O)=O IEKHISJGRIEHRE-UHFFFAOYSA-N 0.000 claims description 5
- AVBJHQDHVYGQLS-UHFFFAOYSA-N 2-(dodecanoylamino)pentanedioic acid Chemical compound CCCCCCCCCCCC(=O)NC(C(O)=O)CCC(O)=O AVBJHQDHVYGQLS-UHFFFAOYSA-N 0.000 claims description 4
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- 235000014113 dietary fatty acids Nutrition 0.000 description 16
- 239000000194 fatty acid Substances 0.000 description 16
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- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 1
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- SLYCYWCVSGPDFR-UHFFFAOYSA-N octadecyltrimethoxysilane Chemical compound CCCCCCCCCCCCCCCCCC[Si](OC)(OC)OC SLYCYWCVSGPDFR-UHFFFAOYSA-N 0.000 description 1
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- 229920003217 poly(methylsilsesquioxane) Polymers 0.000 description 1
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Landscapes
- Cosmetics (AREA)
Description
(a)有機チタネート被覆粉体を5〜85質量%
(b)パラメトキシケイ皮酸2−エチルヘキシルを3〜10質量%
(c)油剤0.5〜23質量%
を含有し、且つ、〔成分(b)の含有量〕/〔成分(b)の含有量+成分(c)の含有量〕が0.3以上である粉体混合物を圧縮成形してなる固形状の粉体化粧料である。
イトステリル・ベヘニル・オクチルドデシル)エステル等が挙げられ、これらの一種又は二種以上を用いることができる。
また、本発明の粉体化粧料の形態は、粉末状、ケーキ状、スティック状、球状等が挙げられるが、本発明の効果が顕著に発揮されるのは、ケーキ状、スティック状、球状等の固形状の粉体化粧料である。
製造例1:有機チタネート5%被覆セリサイト
イソプロピルアルコール500gとイソプロピルトリイソステアロイルチタネート50gを混合し、ヘンシェルミキサー(三井鉱山社製)中でセリサイト〔サンシンセリサイトFSE(三信鉱工業社製)〕950gと混合する。その後、減圧下、60℃でイソプロピルアルコールを回収し、粉砕して、有機チタネート5%被覆セリサイトを得た。
セリサイトの代わりにタルク〔平均粒径5μm〕を用いて、前記製造例1と同様に操作し、有機チタネート5%被覆タルクを得た。
セリサイトの代わりに酸化チタン〔タイペークCR−50(石原産業社製)〕を用いて、前記製造例1と同様に操作し、有機チタネート5%被覆酸化チタンを得た。
セリサイトを得た。
前記製造例4のトリエトキシオクチルシランをトリメトキシオクチルシランに代えて、同様の操作により、トリメトキシオクチルシラン2%被覆セリサイトを得た。
前記製造例4のセリサイトをタルク(平均粒径5μm)に代えて、同様の操作により、トリエトキシオクチルシラン2%被覆タルクを得た。
前記製造例4のセリサイトを酸化チタン〔タイペークCR−50(石原産業社製)〕に代えて、同様の操作により、トリエトキシオクチルシラン5%被覆酸化チタンを得た。
表1〜3に示す組成のファンデーションを下記製造方法により調製し、「化粧料塗布時の伸び広がり」、「しっとり感」、「肌への密着性」、「化粧持続性」の各項目について、以下に示す評価方法及び判定基準により評価判定し、結果を併せて表1〜3に示した。
A:成分15〜19を加熱し、混合する。
B:成分1〜14をヘンシェルミキサー(三井鉱山社製)で均一分散する。
C:BにAを添加し、混合する。
D:Cを粉砕する。
E:Dを金皿に充填し、圧縮成型して、ケーキ状サンカット(名称商標)ファンデーションを得た。
化粧品評価専門パネル20名に、前記実施例及び比較例のファンデーションを使用してもらい、「化粧料塗布時の伸び広がり」、「しっとり感」、「肌への密着性」、「化粧持続性」の其々の項目について、各自が以下の評価基準に従って5段階評価しファンデーション毎に評点を付し、更に全パネルの評点の平均点を以下の判定基準に従って判定した。尚、「化粧持続性」については、ファンデーション塗布後、日常生活を6時間した後に評価した。
評価基準:
[評価結果] :[評 点]
非常に良好 : 5点
良好 : 4点
普通 : 3点
やや不良 : 2点
不良 : 1点
判定基準:
[評点の平均点] :[判 定]
4.5以上 : ◎
3.5以上〜4.5未満 : ○
1.5以上〜3.5未満 : △
1.5未満 : ×
(成分) (%)
1.製造例1の有機チタネート5%被覆セリサイト 50
2.合成金雲母(平均粒径30μm、アスペクト比60) 10
3.ステアリン酸マグネシウム 3
4.ナイロンパウダー 3
5.タルク 残量
6.ベンガラ 2
7.黄色酸化鉄 2
8.黒色酸化鉄 1
9.パラオキシ安息香酸メチル 0.2
10.パラメトキシケイ皮酸2−エチルヘキシル 5
11.パーフルオロポリエーテル(注1) 1
12.ジペンタエリトリット(12−ヒドロキシステアリン酸・
ステアリン酸・ロジン)エステル(注2) 3
13.流動パラフィン 1
※注1:フォンブリンHC/04(アウジモント社製)
※注2:コスモール168AR(日清オイリオ社製)
A:成分10〜13を加熱し、混合する。
B:成分1〜9をヘンシェルミキサー(三井鉱山社製)で均一分散する。
C:BにAを添加し、混合する。
D:Cを粉砕する。
E:Dを金皿に充填し、圧縮成型して、ケーキ状頬紅を得た。
本発明の実施品である実施例9のケーキ状頬紅は、紫外線遮蔽効果に優れ、「化粧料塗布時の伸び広がり」、「しっとり感」、「肌への密着性」、「化粧持続性」の全ての項目に優れた粉体化粧料であった。
(成分) (%)
1.製造例2の有機チタネート5%被覆タルク 25
2.製造例6のトリエトキシオクチルシラン2%被覆タルク 25
3.窒化硼素(平均粒径6μm、アスペクト比40) 5
4.薄片状シリカ(平均粒径10μm、アスペクト比60) 5
5.球状多孔質シリカ(平均粒径10μm) 10
6.セリサイト 残量
7.黄色酸化鉄 1
8.ベンガラ 0.5
9.黒色酸化鉄 0.5
10.パラオキシ安息香酸メチル 0.2
11.パラメトキシケイ皮酸2−エチルヘキシル 8
12.ラウロイル−L−グルタミン酸ジ(コレステリル・ベヘニル・
オクチルドデシル)エステルスクワラン 2
13.ジメチルポリシロキサン 0.5
A:成分11〜13を加熱し、混合する。
B:成分1〜10をヘンシェルミキサー(三井鉱山社製)で均一分散する。
C:BにAを添加し、混合する。
D:Cを粉砕する。
E:Dを容器に充填し、粉末状頬紅を得た。
本発明の実施品である実施例10の粉末状白粉は、紫外線遮蔽効果に優れ、「化粧料塗布時の伸び広がり」、「しっとり感」、「肌への密着性」、「化粧持続性」の全ての項目に優れた粉体化粧料であった。
Claims (5)
- 次の成分(a)〜(c);
(a)有機チタネート被覆粉体を5〜85質量%
(b)パラメトキシケイ皮酸2−エチルヘキシルを3〜10質量%
(c)油剤0.5〜23質量%
を含有し、且つ、〔成分(b)の含有量〕/〔成分(b)の含有量+成分(c)の含有量〕が0.3以上である粉体混合物を圧縮成形してなる固形状の粉体化粧料。 - 成分(a)の有機チタネートがイソプロピルトリイソステアロイルチタネートであることを特徴とする請求項1記載の粉体化粧料。
- 更に、前記成分(c)中に、ペースト油を5〜20質量%含有することを特徴とする請求項1又は2記載の粉体化粧料。
- ペースト油が、N−ラウロイル−L−グルタミン酸ジ(コレステリル・ベヘニル・オクチルドデシル)エステル及び/又はN−ラウロイル−L−グルタミン酸ジ(フィトステリル・ベヘニル・オクチルドデシル)エステルであることを特徴とする請求項3記載の粉体化粧料。
- 更に、成分(d)としてトリアルコキシアルキルシラン被覆粉体を含有し、且つ、〔成分(a)の含有量〕/〔成分(d)の含有量〕が0.1以上10以下であることを特徴とする請求項1〜4の何れかの項記載の粉体化粧料。
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