JP4079898B2 - 有機無機ハイブリッドガラス状物質 - Google Patents
有機無機ハイブリッドガラス状物質 Download PDFInfo
- Publication number
- JP4079898B2 JP4079898B2 JP2004060550A JP2004060550A JP4079898B2 JP 4079898 B2 JP4079898 B2 JP 4079898B2 JP 2004060550 A JP2004060550 A JP 2004060550A JP 2004060550 A JP2004060550 A JP 2004060550A JP 4079898 B2 JP4079898 B2 JP 4079898B2
- Authority
- JP
- Japan
- Prior art keywords
- organic
- inorganic hybrid
- aging
- substance
- hybrid glassy
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- 239000000463 material Substances 0.000 title claims description 104
- 230000032683 aging Effects 0.000 claims description 77
- 238000002844 melting Methods 0.000 claims description 72
- 230000008018 melting Effects 0.000 claims description 59
- 229910052751 metal Inorganic materials 0.000 claims description 27
- 238000003980 solgel method Methods 0.000 claims description 27
- 125000000524 functional group Chemical group 0.000 claims description 26
- 239000002184 metal Substances 0.000 claims description 26
- 229910052791 calcium Inorganic materials 0.000 claims description 4
- 229910052749 magnesium Inorganic materials 0.000 claims description 4
- 229910052712 strontium Inorganic materials 0.000 claims description 4
- 229910052684 Cerium Inorganic materials 0.000 claims description 3
- 229910052692 Dysprosium Inorganic materials 0.000 claims description 3
- 229910052691 Erbium Inorganic materials 0.000 claims description 3
- 229910052693 Europium Inorganic materials 0.000 claims description 3
- 229910052688 Gadolinium Inorganic materials 0.000 claims description 3
- 229910052689 Holmium Inorganic materials 0.000 claims description 3
- 229910052779 Neodymium Inorganic materials 0.000 claims description 3
- 229910052777 Praseodymium Inorganic materials 0.000 claims description 3
- 229910052772 Samarium Inorganic materials 0.000 claims description 3
- 229910052771 Terbium Inorganic materials 0.000 claims description 3
- 229910052775 Thulium Inorganic materials 0.000 claims description 3
- 229910052804 chromium Inorganic materials 0.000 claims description 3
- 229910052802 copper Inorganic materials 0.000 claims description 3
- 229910052742 iron Inorganic materials 0.000 claims description 3
- 229910052748 manganese Inorganic materials 0.000 claims description 3
- 229910052759 nickel Inorganic materials 0.000 claims description 3
- 229910052758 niobium Inorganic materials 0.000 claims description 3
- 229910052761 rare earth metal Inorganic materials 0.000 claims description 3
- 229910052719 titanium Inorganic materials 0.000 claims description 3
- 229910001428 transition metal ion Inorganic materials 0.000 claims description 3
- 229910052720 vanadium Inorganic materials 0.000 claims description 3
- 229910052725 zinc Inorganic materials 0.000 claims description 3
- 229910052726 zirconium Inorganic materials 0.000 claims description 3
- 239000000126 substance Substances 0.000 description 118
- 239000011521 glass Substances 0.000 description 65
- 238000012360 testing method Methods 0.000 description 31
- 239000000499 gel Substances 0.000 description 30
- 238000000034 method Methods 0.000 description 28
- 239000002994 raw material Substances 0.000 description 28
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 21
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 20
- 239000012780 transparent material Substances 0.000 description 19
- JCVQKRGIASEUKR-UHFFFAOYSA-N triethoxy(phenyl)silane Chemical compound CCO[Si](OCC)(OCC)C1=CC=CC=C1 JCVQKRGIASEUKR-UHFFFAOYSA-N 0.000 description 14
- DENFJSAFJTVPJR-UHFFFAOYSA-N triethoxy(ethyl)silane Chemical compound CCO[Si](CC)(OCC)OCC DENFJSAFJTVPJR-UHFFFAOYSA-N 0.000 description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 13
- RBTBFTRPCNLSDE-UHFFFAOYSA-N 3,7-bis(dimethylamino)phenothiazin-5-ium Chemical compound C1=CC(N(C)C)=CC2=[S+]C3=CC(N(C)C)=CC=C3N=C21 RBTBFTRPCNLSDE-UHFFFAOYSA-N 0.000 description 11
- 230000001788 irregular Effects 0.000 description 11
- 229960000907 methylthioninium chloride Drugs 0.000 description 11
- 239000000203 mixture Substances 0.000 description 11
- 230000003287 optical effect Effects 0.000 description 11
- 230000007704 transition Effects 0.000 description 11
- 239000003054 catalyst Substances 0.000 description 10
- 230000000740 bleeding effect Effects 0.000 description 9
- 238000004040 coloring Methods 0.000 description 8
- 230000000052 comparative effect Effects 0.000 description 8
- 238000010438 heat treatment Methods 0.000 description 8
- 238000004519 manufacturing process Methods 0.000 description 8
- 239000007858 starting material Substances 0.000 description 7
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical group [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 6
- 150000004703 alkoxides Chemical class 0.000 description 6
- 238000011161 development Methods 0.000 description 6
- 230000018109 developmental process Effects 0.000 description 6
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 6
- 230000000704 physical effect Effects 0.000 description 6
- HPGGPRDJHPYFRM-UHFFFAOYSA-J tin(iv) chloride Chemical compound Cl[Sn](Cl)(Cl)Cl HPGGPRDJHPYFRM-UHFFFAOYSA-J 0.000 description 6
- 239000010936 titanium Substances 0.000 description 6
- 238000006243 chemical reaction Methods 0.000 description 5
- 230000000694 effects Effects 0.000 description 5
- 238000001879 gelation Methods 0.000 description 5
- 239000002861 polymer material Substances 0.000 description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 4
- 125000000217 alkyl group Chemical group 0.000 description 4
- VYXSBFYARXAAKO-WTKGSRSZSA-N chembl402140 Chemical compound Cl.C1=2C=C(C)C(NCC)=CC=2OC2=C\C(=N/CC)C(C)=CC2=C1C1=CC=CC=C1C(=O)OCC VYXSBFYARXAAKO-WTKGSRSZSA-N 0.000 description 4
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 4
- 239000011240 wet gel Substances 0.000 description 4
- 125000003118 aryl group Chemical group 0.000 description 3
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- 230000005070 ripening Effects 0.000 description 3
- 238000007789 sealing Methods 0.000 description 3
- 238000001308 synthesis method Methods 0.000 description 3
- 239000010409 thin film Substances 0.000 description 3
- 229910052718 tin Inorganic materials 0.000 description 3
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 2
- 108010043121 Green Fluorescent Proteins Proteins 0.000 description 2
- 229910052788 barium Inorganic materials 0.000 description 2
- 239000002585 base Substances 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 229910052797 bismuth Inorganic materials 0.000 description 2
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 description 2
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 2
- 238000004891 communication Methods 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- YYLGKUPAFFKGRQ-UHFFFAOYSA-N dimethyldiethoxysilane Chemical compound CCO[Si](C)(C)OCC YYLGKUPAFFKGRQ-UHFFFAOYSA-N 0.000 description 2
- 239000012776 electronic material Substances 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 239000006060 molten glass Substances 0.000 description 2
- 125000000962 organic group Chemical group 0.000 description 2
- 239000011368 organic material Substances 0.000 description 2
- OGHBATFHNDZKSO-UHFFFAOYSA-N propan-2-olate Chemical compound CC(C)[O-] OGHBATFHNDZKSO-UHFFFAOYSA-N 0.000 description 2
- -1 rare earth metal ion Chemical group 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- POILWHVDKZOXJZ-ARJAWSKDSA-M (z)-4-oxopent-2-en-2-olate Chemical compound C\C([O-])=C\C(C)=O POILWHVDKZOXJZ-ARJAWSKDSA-M 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 239000004593 Epoxy Substances 0.000 description 1
- 229910004298 SiO 2 Inorganic materials 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 229910008449 SnF 2 Inorganic materials 0.000 description 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
- 150000008065 acid anhydrides Chemical class 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 238000009529 body temperature measurement Methods 0.000 description 1
- 239000002419 bulk glass Substances 0.000 description 1
- 239000013590 bulk material Substances 0.000 description 1
- 238000012769 bulk production Methods 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 238000000280 densification Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000010408 film Substances 0.000 description 1
- 230000002431 foraging effect Effects 0.000 description 1
- 239000003365 glass fiber Substances 0.000 description 1
- 230000009477 glass transition Effects 0.000 description 1
- 125000004051 hexyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 238000010309 melting process Methods 0.000 description 1
- 229910001507 metal halide Inorganic materials 0.000 description 1
- 150000005309 metal halides Chemical class 0.000 description 1
- 229910000000 metal hydroxide Inorganic materials 0.000 description 1
- 150000004692 metal hydroxides Chemical class 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 239000012860 organic pigment Substances 0.000 description 1
- 239000011236 particulate material Substances 0.000 description 1
- 238000002161 passivation Methods 0.000 description 1
- 125000001147 pentyl group Chemical group C(CCCC)* 0.000 description 1
- 238000006068 polycondensation reaction Methods 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 125000004076 pyridyl group Chemical group 0.000 description 1
- 239000003566 sealing material Substances 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- 125000003944 tolyl group Chemical group 0.000 description 1
- 125000005023 xylyl group Chemical group 0.000 description 1
Landscapes
- Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)
- Silicon Polymers (AREA)
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2004060550A JP4079898B2 (ja) | 2003-03-14 | 2004-03-04 | 有機無機ハイブリッドガラス状物質 |
| US10/800,010 US7802450B2 (en) | 2003-03-14 | 2004-03-15 | Organic-inorganic hybrid glassy materials and their production processes |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2003069342 | 2003-03-14 | ||
| JP2003069336 | 2003-03-14 | ||
| JP2004060550A JP4079898B2 (ja) | 2003-03-14 | 2004-03-04 | 有機無機ハイブリッドガラス状物質 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2004300417A JP2004300417A (ja) | 2004-10-28 |
| JP2004300417A5 JP2004300417A5 (https=) | 2005-07-28 |
| JP4079898B2 true JP4079898B2 (ja) | 2008-04-23 |
Family
ID=33424766
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2004060550A Expired - Fee Related JP4079898B2 (ja) | 2003-03-14 | 2004-03-04 | 有機無機ハイブリッドガラス状物質 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP4079898B2 (https=) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4375982B2 (ja) * | 2003-03-14 | 2009-12-02 | セントラル硝子株式会社 | 有機無機ハイブリッドガラス状物質及びその製造方法 |
| JP4512936B2 (ja) * | 2003-03-14 | 2010-07-28 | セントラル硝子株式会社 | 有機無機ハイブリッドガラス状物質 |
| JP4516776B2 (ja) * | 2004-03-31 | 2010-08-04 | セントラル硝子株式会社 | 有機無機ハイブリッドガラス状物質とその製造方法 |
| JP4516728B2 (ja) * | 2003-07-31 | 2010-08-04 | セントラル硝子株式会社 | 有機無機ハイブリッドガラス状物質及びその製造方法 |
| JP4516727B2 (ja) * | 2003-07-31 | 2010-08-04 | セントラル硝子株式会社 | 有機無機ハイブリッドガラス状物質とその製造方法 |
| JP4516736B2 (ja) * | 2003-11-19 | 2010-08-04 | セントラル硝子株式会社 | 膜状有機無機ハイブリッドガラス状物質及びその製造方法 |
| JP4736388B2 (ja) * | 2004-09-29 | 2011-07-27 | セントラル硝子株式会社 | 有機無機ハイブリッドガラス状物質とその製造方法 |
| JP5109387B2 (ja) * | 2007-02-02 | 2012-12-26 | セントラル硝子株式会社 | 有機無機ハイブリッド透明封止材とその製造方法 |
| JP2010111749A (ja) * | 2008-11-05 | 2010-05-20 | Central Glass Co Ltd | 機能性微粒子封止用熱硬化性有機無機ハイブリッド透明材料 |
| CN102844382B (zh) | 2010-02-03 | 2015-09-09 | 住友大阪水泥股份有限公司 | 有机无机复合物、有机无机复合物形成用组合物以及油墨 |
| JP2020076057A (ja) * | 2018-09-21 | 2020-05-21 | 公立大学法人首都大学東京 | ポリシルセスキオキサンガラス |
-
2004
- 2004-03-04 JP JP2004060550A patent/JP4079898B2/ja not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| JP2004300417A (ja) | 2004-10-28 |
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