JP3928813B2 - 溶融流量の値が高く分子量分布が狭い結晶質プロピレンポリマー - Google Patents
溶融流量の値が高く分子量分布が狭い結晶質プロピレンポリマー Download PDFInfo
- Publication number
- JP3928813B2 JP3928813B2 JP09320394A JP9320394A JP3928813B2 JP 3928813 B2 JP3928813 B2 JP 3928813B2 JP 09320394 A JP09320394 A JP 09320394A JP 9320394 A JP9320394 A JP 9320394A JP 3928813 B2 JP3928813 B2 JP 3928813B2
- Authority
- JP
- Japan
- Prior art keywords
- value
- polymer
- catalyst
- electron donor
- solid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/28—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from copolymers obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D01F6/30—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from copolymers obtained by reactions only involving carbon-to-carbon unsaturated bonds comprising olefins as the major constituent
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C33/00—Moulds or cores; Details thereof or accessories therefor
- B29C33/02—Moulds or cores; Details thereof or accessories therefor with incorporated heating or cooling means
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F10/00—Homopolymers and copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
- C08F10/04—Monomers containing three or four carbon atoms
- C08F10/06—Propene
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/02—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolymers obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D01F6/04—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolymers obtained by reactions only involving carbon-to-carbon unsaturated bonds from polyolefins
- D01F6/06—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolymers obtained by reactions only involving carbon-to-carbon unsaturated bonds from polyolefins from polypropylene
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/42—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
- D04H1/4282—Addition polymers
- D04H1/4291—Olefin series
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F110/00—Homopolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
- C08F110/04—Monomers containing three or four carbon atoms
- C08F110/06—Propene
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Textile Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Mechanical Engineering (AREA)
- Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Artificial Filaments (AREA)
- Nonwoven Fabrics (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US5470593A | 1993-04-29 | 1993-04-29 | |
US08/054705 | 1993-04-29 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPH072925A JPH072925A (ja) | 1995-01-06 |
JP3928813B2 true JP3928813B2 (ja) | 2007-06-13 |
Family
ID=21992959
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP09320394A Expired - Lifetime JP3928813B2 (ja) | 1993-04-29 | 1994-05-02 | 溶融流量の値が高く分子量分布が狭い結晶質プロピレンポリマー |
Country Status (11)
Families Citing this family (79)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
TW268072B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1993-12-09 | 1996-01-11 | Honda Motor Co Ltd | |
ES2107109T3 (es) * | 1993-12-16 | 1997-11-16 | Montell North America Inc | Resinas de homopolimeros de propileno que tienen un alto contenido de estereobloques. |
US5820981A (en) * | 1996-04-02 | 1998-10-13 | Montell North America Inc. | Radiation visbroken polypropylene and fibers made therefrom |
US6100351A (en) * | 1997-01-07 | 2000-08-08 | Huntsman Polymers Corporation | Olefin polymerization process and products thereof |
US5948720A (en) * | 1997-01-07 | 1999-09-07 | Huntsman Polymers Corporation | Catalyst for the production of flexible polyolefin compositions, methods for making and using same, and products thereof |
US6057407A (en) * | 1997-01-08 | 2000-05-02 | Bp Amoco Corporation | High melt flow propylene polymer produced by gas-phase polymerization |
US6080818A (en) * | 1997-03-24 | 2000-06-27 | Huntsman Polymers Corporation | Polyolefin blends used for non-woven applications |
US6423800B1 (en) | 1999-05-26 | 2002-07-23 | Fina Technology, Inc. | Pelletized polyolefin having ultra-high melt flow and its articles of manufacture |
US6413344B2 (en) | 1999-06-16 | 2002-07-02 | First Quality Nonwovens, Inc. | Method of making media of controlled porosity |
US6582762B2 (en) | 1999-12-22 | 2003-06-24 | Exxonmobil Chemical Patents Inc. | Sprayable hot melt adhesives |
FI111955B (fi) * | 1999-12-27 | 2003-10-15 | Borealis Tech Oy | Propeenipolymeerit, joilla on erittäin korkea sulavirta |
FR2804964B1 (fr) * | 2000-02-14 | 2006-09-29 | Omya Sa | Utilisation de polypropylenes isotactiques de tres grande fluidite pour la preparation de concentres de charges utilisables dans les thermoplastiques de type olefinique, concentres de charges et thermoplastiques ainsi obtenus |
US6476135B1 (en) * | 2000-06-07 | 2002-11-05 | Basell Poliolefine Italia S.P.A. | Polyolefin composition containing low viscosity propylene homopolymer, fiber and extensible non-woven fabric prepared therefrom |
US6900321B2 (en) | 2000-11-07 | 2005-05-31 | Symyx Technologies, Inc. | Substituted pyridyl amine complexes, and catalysts |
CN1367184A (zh) * | 2001-01-12 | 2002-09-04 | 弗纳技术股份有限公司 | 生产超高熔体流动聚丙烯树脂的方法 |
US7666805B1 (en) * | 2001-02-07 | 2010-02-23 | Fumin Lu | Spunbond fabrics and laminates from ultra low viscosity resins |
US20030022786A1 (en) * | 2001-05-03 | 2003-01-30 | Epstein Ronald A. | Catalyst for propylene polymerization |
JP2005505655A (ja) * | 2001-10-12 | 2005-02-24 | ハンツマン・ポリマーズ・コーポレーシヨン | 高弾性率、高延性のポリオレフィン |
ES2322047T3 (es) | 2002-03-08 | 2009-06-16 | Basell Poliolefine Italia S.R.L. | Proceso para obtener un componente catalizador basado en un dieter. |
US6992131B2 (en) | 2002-03-22 | 2006-01-31 | Exxonmobil Chemical Patents Inc. | Adhesives |
WO2003091262A1 (en) | 2002-04-24 | 2003-11-06 | Symyx Technologies, Inc. | Bridged bi-aromatic ligands, complexes, catalysts and processes for polymerizing and poymers therefrom |
US7091292B2 (en) | 2002-04-24 | 2006-08-15 | Symyx Technologies, Inc. | Bridged bi-aromatic catalysts, complexes, and methods of using the same |
US7060848B2 (en) | 2002-04-24 | 2006-06-13 | Symyx Technologies, Inc. | Bridged bi-aromatic catalysts, complexes, and methods of using the same |
US6780808B2 (en) * | 2002-07-15 | 2004-08-24 | Univation Technologies, Llc | Enhanced solubility of magnesium halides and catalysts and polymerization process using same |
US7700707B2 (en) | 2002-10-15 | 2010-04-20 | Exxonmobil Chemical Patents Inc. | Polyolefin adhesive compositions and articles made therefrom |
US7550528B2 (en) | 2002-10-15 | 2009-06-23 | Exxonmobil Chemical Patents Inc. | Functionalized olefin polymers |
CN101724110B (zh) | 2002-10-15 | 2013-03-27 | 埃克森美孚化学专利公司 | 用于烯烃聚合的多催化剂体系和由其生产的聚合物 |
US7101623B2 (en) | 2004-03-19 | 2006-09-05 | Dow Global Technologies Inc. | Extensible and elastic conjugate fibers and webs having a nontacky feel |
TW200610844A (en) | 2004-03-19 | 2006-04-01 | Dow Global Technologies Inc | Propylene-based copolymers, a method of making the fibers and articles made from the fibers |
US7256296B2 (en) | 2004-09-22 | 2007-08-14 | Symyx Technologies, Inc. | Heterocycle-amine ligands, compositions, complexes, and catalysts |
EP1794196A2 (en) | 2004-09-22 | 2007-06-13 | Symyx Technologies, Inc. | Heterocycle-amine ligands, compositions, complexes, and catalysts, and methods of making and using the same |
CN101056895B (zh) * | 2004-11-17 | 2016-03-02 | 三井化学株式会社 | 固体状钛催化剂成分、烯烃聚合用催化剂及烯烃系聚合物的制造方法 |
WO2006066126A2 (en) | 2004-12-16 | 2006-06-22 | Symyx Technologies, Inc. | Phenol-heterocyclic ligands, metal complexes, and their uses as catalysts |
JP4690131B2 (ja) * | 2005-07-13 | 2011-06-01 | 旭化成せんい株式会社 | 長繊維不織布用ポリプロピレン樹脂組成物 |
US8627993B2 (en) * | 2007-02-12 | 2014-01-14 | Ethicon Endo-Surgery, Inc. | Active braking electrical surgical instrument and method for braking such an instrument |
ES2329422T3 (es) * | 2006-04-24 | 2009-11-25 | Total Petrochemicals Research Feluy | Proceso para la produccion de polimeros de propileno que tienen un contenido bajo de cenizas. |
EP2529675B1 (en) * | 2006-05-19 | 2022-07-20 | Ethicon Endo-Surgery, Inc. | Surgical stapling instrument |
CN101472961A (zh) * | 2006-06-22 | 2009-07-01 | 巴塞尔聚烯烃意大利有限责任公司 | 基于1,3-二醚的用于烯烃聚合的催化剂组分 |
US20100240845A1 (en) * | 2006-06-22 | 2010-09-23 | Basell Poliolefine Italia S.R.L. | Catalyst component for the polymerization of olefins |
US8309659B2 (en) * | 2006-12-20 | 2012-11-13 | Basell Poliolefine Italia S.R.L. | Filled polyolefin compositions |
US8716394B2 (en) * | 2006-12-20 | 2014-05-06 | Basell Poliolefine Italia S.R.L. | Polypropylene compositions containing fillers and/or pigments |
EP2092015B1 (en) * | 2006-12-20 | 2012-11-14 | Basell Poliolefine Italia S.r.l. | Filled polyolefin compositions |
EP2070956A1 (en) * | 2007-12-14 | 2009-06-17 | Total Petrochemicals Research Feluy | Process for the production of a bimodal polypropylene having low ash content |
RU2471811C2 (ru) * | 2007-10-15 | 2013-01-10 | Базелль Полиолефин Италия С.Р.Л. | Способ получения полимеров пропилена с высокой текучестью |
EP2113541A1 (en) | 2008-04-28 | 2009-11-04 | Borealis AG | Adhesive propylene polymer composition suitable for extrusion coating of paper substrates |
US8557913B2 (en) | 2008-12-19 | 2013-10-15 | Basell Poliolefine Italia S.R.L. | Filled polyolefin compositions |
EP2251375A1 (en) | 2009-05-07 | 2010-11-17 | Borealis AG | Thermoplastic polyolefin compounds with decreased flaming sensitivity |
US20130102744A1 (en) | 2010-06-24 | 2013-04-25 | Basell Poliolefine Italia, s.r.l. | Catalyst Systems for the Polymerization of Olefins |
CN102958997B (zh) | 2010-06-29 | 2016-05-11 | 巴塞尔聚烯烃意大利有限责任公司 | 填充的聚烯烃组合物 |
US9815918B2 (en) | 2012-03-19 | 2017-11-14 | Formosa Plastics Corporation, U.S.A. | Catalyst component for high activity and high stereoselectivity in olefin polymerization |
CN103788260B (zh) * | 2012-10-30 | 2019-05-31 | 中国石油化工股份有限公司 | 一种丙烯均聚物的制备方法 |
CN103788259B (zh) | 2012-10-30 | 2017-05-31 | 中国石油化工股份有限公司 | 一种分子量窄分布聚丙烯 |
US9522968B2 (en) * | 2012-11-26 | 2016-12-20 | Lummus Novolen Technology Gmbh | High performance Ziegler-Natta catalyst systems, process for producing such MgCl2 based catalysts and use thereof |
KR101820613B1 (ko) | 2013-08-14 | 2018-01-19 | 보레알리스 아게 | 저온에서 개선된 충격 저항성을 갖는 프로필렌 조성물 |
JP6190961B2 (ja) | 2013-08-21 | 2017-08-30 | ボレアリス・アクチェンゲゼルシャフトBorealis Ag | 高い剛性および靭性を有する高流動ポリオレフィン組成物 |
JP2016528368A (ja) | 2013-08-21 | 2016-09-15 | ボレアリス・アクチェンゲゼルシャフトBorealis Ag | 高い剛性および靭性を有する高流動ポリオレフィン組成物 |
EP2853563B1 (en) | 2013-09-27 | 2016-06-15 | Borealis AG | Films suitable for BOPP processing from polymers with high XS and high Tm |
EP2860031B1 (en) | 2013-10-11 | 2016-03-30 | Borealis AG | Machine direction oriented film for labels |
EP2865713B1 (en) | 2013-10-24 | 2016-04-20 | Borealis AG | Blow molded article based on bimodal random copolymer |
WO2015059229A1 (en) | 2013-10-24 | 2015-04-30 | Borealis Ag | Low melting pp homopolymer with high content of regioerrors and high molecular weight |
US9670293B2 (en) | 2013-10-29 | 2017-06-06 | Borealis Ag | Solid single site catalysts with high polymerisation activity |
CA2927448C (en) * | 2013-11-22 | 2017-01-17 | Borealis Ag | Low emission propylene homopolymer with high melt flow |
EP3071607B1 (en) | 2013-11-22 | 2018-05-09 | Borealis AG | Low emission propylene homopolymer |
CN105793298B (zh) * | 2013-12-04 | 2019-06-28 | 博里利斯股份公司 | 用于熔喷纤维的不含邻苯二甲酸酯的pp均聚物 |
CN105980457B (zh) | 2013-12-18 | 2019-03-22 | 博里利斯股份公司 | 具有改善的刚性/韧性平衡的bopp膜 |
CN105829364B (zh) | 2014-01-17 | 2017-11-10 | 博里利斯股份公司 | 用于制备丙烯/1‑丁烯共聚物的方法 |
ES2827285T3 (es) | 2014-02-06 | 2021-05-20 | Borealis Ag | Copolímeros blandos con alta resistencia al impacto |
JP6474417B2 (ja) | 2014-02-06 | 2019-02-27 | ボレアリス エージー | 軟質及び透明衝撃コポリマー |
US10696765B2 (en) | 2014-02-07 | 2020-06-30 | Eastman Chemical Company | Adhesive composition comprising amorphous propylene-ethylene copolymer and propylene polymer |
US9611341B2 (en) | 2014-02-07 | 2017-04-04 | Eastman Chemical Company | Amorphous propylene-ethylene copolymers |
US10723824B2 (en) | 2014-02-07 | 2020-07-28 | Eastman Chemical Company | Adhesives comprising amorphous propylene-ethylene copolymers |
US11267916B2 (en) | 2014-02-07 | 2022-03-08 | Eastman Chemical Company | Adhesive composition comprising amorphous propylene-ethylene copolymer and polyolefins |
US10647795B2 (en) | 2014-02-07 | 2020-05-12 | Eastman Chemical Company | Adhesive composition comprising amorphous propylene-ethylene copolymer and polyolefins |
US10308740B2 (en) | 2014-02-07 | 2019-06-04 | Eastman Chemical Company | Amorphous propylene-ethylene copolymers |
EP2907841A1 (en) | 2014-02-14 | 2015-08-19 | Borealis AG | Polypropylene composite |
EP2947118B1 (en) | 2014-05-20 | 2017-11-29 | Borealis AG | Polypropylene composition for automotive interior applications |
PL3118249T3 (pl) | 2015-07-14 | 2018-04-30 | Borealis Ag | Kompozyt wzmocniony włóknem |
US20230257494A1 (en) * | 2020-09-08 | 2023-08-17 | Lg Chem, Ltd. | Powder type polypropylene resin and method for preparing the same |
EP4506410A1 (en) | 2023-08-09 | 2025-02-12 | Borealis AG | Flame retardant polypropylene composition |
Family Cites Families (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2720701C2 (de) * | 1977-05-07 | 1985-05-02 | Hughes Aircraft Co., Culver City, Calif. | Verfahren zur Herstellung von Kunststoff-Fasern aus einem nichtkristallinen Polymeren |
US4665118A (en) * | 1985-05-22 | 1987-05-12 | Atlantic Richfield Company | Processing additive for vinyl compounds |
BR8806195A (pt) * | 1987-11-25 | 1989-08-15 | Shell Oil Co | Processo para a producao de um polimero de propileno com taxa de escoamento de fusao ultra-alta na ausencia de qualquer tratamento pos-reator |
IT1227259B (it) * | 1988-09-30 | 1991-03-28 | Himont Inc | Catalizzatori per la polimerizzazione di olefine. |
IT1227258B (it) * | 1988-09-30 | 1991-03-28 | Himont Inc | Componenti e catalizzatori per la polimerizzazione di olefine |
DE69127220T2 (de) * | 1990-04-13 | 1998-01-02 | Mitsui Petrochemical Ind | Festes Titan enthaltendes Katalysatorbestandteil und Katalysator für Olefinpolymerisation, vorpolymerisierte Olefinpolymerisationskatalysator und Verfahren für Olefinpolymerisation |
DE4030379A1 (de) * | 1990-09-26 | 1992-04-02 | Basf Ag | Polymerwachse des propylens mit hoher haerte und kristallinitaet |
TW275076B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) † | 1992-12-02 | 1996-05-01 | Hoechst Ag |
-
1994
- 1994-04-20 CA CA002121721A patent/CA2121721C/en not_active Expired - Fee Related
- 1994-04-22 EP EP94106280A patent/EP0622380B2/en not_active Expired - Lifetime
- 1994-04-22 DE DE69413107T patent/DE69413107T3/de not_active Expired - Lifetime
- 1994-04-26 AU AU60673/94A patent/AU672881B2/en not_active Ceased
- 1994-04-27 NO NO941543A patent/NO303125B1/no not_active IP Right Cessation
- 1994-04-28 BR BR9401640A patent/BR9401640A/pt not_active IP Right Cessation
- 1994-04-28 KR KR1019940009088A patent/KR100329447B1/ko not_active Expired - Fee Related
- 1994-04-29 FI FI942004A patent/FI942004L/fi unknown
- 1994-04-29 CN CN94104908A patent/CN1041098C/zh not_active Expired - Fee Related
- 1994-05-02 JP JP09320394A patent/JP3928813B2/ja not_active Expired - Lifetime
- 1994-07-05 US US08/270,806 patent/US5476911A/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
EP0622380A1 (en) | 1994-11-02 |
AU6067394A (en) | 1994-11-03 |
JPH072925A (ja) | 1995-01-06 |
FI942004A0 (fi) | 1994-04-29 |
NO941543L (no) | 1994-10-31 |
US5476911A (en) | 1995-12-19 |
KR100329447B1 (ko) | 2002-08-14 |
NO941543D0 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1994-04-27 |
CA2121721A1 (en) | 1994-10-30 |
NO303125B1 (no) | 1998-06-02 |
CN1041098C (zh) | 1998-12-09 |
CA2121721C (en) | 2004-11-23 |
EP0622380B2 (en) | 2006-03-15 |
DE69413107D1 (de) | 1998-10-15 |
AU672881B2 (en) | 1996-10-17 |
CN1097770A (zh) | 1995-01-25 |
FI942004A7 (fi) | 1994-10-30 |
BR9401640A (pt) | 1994-12-13 |
DE69413107T2 (de) | 1999-03-11 |
EP0622380B1 (en) | 1998-09-09 |
FI942004L (fi) | 1994-10-30 |
DE69413107T3 (de) | 2007-04-19 |
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