JP3109838B2 - 抽出蒸留による熱分解ガソリンからのスチレンの回収 - Google Patents

抽出蒸留による熱分解ガソリンからのスチレンの回収

Info

Publication number
JP3109838B2
JP3109838B2 JP09540295A JP54029597A JP3109838B2 JP 3109838 B2 JP3109838 B2 JP 3109838B2 JP 09540295 A JP09540295 A JP 09540295A JP 54029597 A JP54029597 A JP 54029597A JP 3109838 B2 JP3109838 B2 JP 3109838B2
Authority
JP
Japan
Prior art keywords
styrene
distillation column
solvent
stream
aromatic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
JP09540295A
Other languages
English (en)
Japanese (ja)
Other versions
JPH11509868A (ja
Inventor
リー，フ―ミン
ジェントリイ，ジョセフ，シー．
ウィッチャーリィ，ランディ，ライト
Original Assignee
エイチエフエム インターナショナル，インコーポレイテッド
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by エイチエフエム インターナショナル，インコーポレイテッド filed Critical エイチエフエム インターナショナル，インコーポレイテッド
Publication of JPH11509868A publication Critical patent/JPH11509868A/ja
Application granted granted Critical
Publication of JP3109838B2 publication Critical patent/JP3109838B2/ja
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C5/00—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms
    • C07C5/32—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by dehydrogenation with formation of free hydrogen
    • C07C5/367—Formation of an aromatic six-membered ring from an existing six-membered ring, e.g. dehydrogenation of ethylcyclohexane to ethylbenzene
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G7/00—Distillation of hydrocarbon oils
    • C10G7/08—Azeotropic or extractive distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/32—Other features of fractionating columns ; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30
    • B01D3/322—Reboiler specifications
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C15/00—Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic parts
    • C07C15/40—Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic parts substituted by unsaturated carbon radicals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C15/00—Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic parts
    • C07C15/40—Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic parts substituted by unsaturated carbon radicals
    • C07C15/42—Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic parts substituted by unsaturated carbon radicals monocyclic
    • C07C15/44—Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic parts substituted by unsaturated carbon radicals monocyclic the hydrocarbon substituent containing a carbon-to-carbon double bond
    • C07C15/46—Styrene; Ring-alkylated styrenes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/005—Processes comprising at least two steps in series
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/04—Purification; Separation; Use of additives by distillation
    • C07C7/05—Purification; Separation; Use of additives by distillation with the aid of auxiliary compounds
    • C07C7/08—Purification; Separation; Use of additives by distillation with the aid of auxiliary compounds by extractive distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/10—Purification; Separation; Use of additives by extraction, i.e. purification or separation of liquid hydrocarbons with the aid of liquids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • Water Supply & Treatment (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
JP09540295A 1996-05-21 1997-05-07 抽出蒸留による熱分解ガソリンからのスチレンの回収 Expired - Lifetime JP3109838B2 (ja)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US65170796A 1996-05-21 1996-05-21
US651,707 1996-05-21
US08/651,707 1996-05-21
PCT/US1997/007888 WO1997044298A1 (en) 1996-05-21 1997-05-07 Recovery of styrene from pyrolysis gasoline by extractive distillation

Publications (2)

Publication Number Publication Date
JPH11509868A JPH11509868A (ja) 1999-08-31
JP3109838B2 true JP3109838B2 (ja) 2000-11-20

Family

ID=24613893

Family Applications (1)

Application Number Title Priority Date Filing Date
JP09540295A Expired - Lifetime JP3109838B2 (ja) 1996-05-21 1997-05-07 抽出蒸留による熱分解ガソリンからのスチレンの回収

Country Status (11)

Country Link
US (1) US5849982A (US06373033-20020416-M00035.png)
JP (1) JP3109838B2 (US06373033-20020416-M00035.png)
KR (1) KR100330488B1 (US06373033-20020416-M00035.png)
CN (1) CN1077560C (US06373033-20020416-M00035.png)
AR (1) AR007039A1 (US06373033-20020416-M00035.png)
AU (1) AU2937997A (US06373033-20020416-M00035.png)
ID (1) ID16811A (US06373033-20020416-M00035.png)
IN (1) IN191114B (US06373033-20020416-M00035.png)
TW (1) TW450993B (US06373033-20020416-M00035.png)
WO (1) WO1997044298A1 (US06373033-20020416-M00035.png)
ZA (1) ZA972966B (US06373033-20020416-M00035.png)

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US6100439A (en) 1998-12-14 2000-08-08 Betzdearborn Inc. Styrene caustic wash extraction aid
US6555726B1 (en) 1999-11-10 2003-04-29 Gaylord Chemical Corporation Methods for enhanced extractive distillation employing extractive distillation compositions comprising sulfolane and compatibility agent
US6551502B1 (en) * 2000-02-11 2003-04-22 Gtc Technology Corporation Process of removing sulfur compounds from gasoline
US20010049462A1 (en) * 2000-04-28 2001-12-06 Fu-Ming Lee Aromatics purification from petroleum streams
US6660899B2 (en) 2001-02-14 2003-12-09 Gaylord Chemical Corporation Methods for enhanced aromatic extraction employing sulfone-sulfoxide compositions
US7014736B2 (en) 2003-03-18 2006-03-21 Nippon Shokubai Co., Ltd. Apparatus and process for purification of acrylic acid family
EP1650287B1 (en) * 2003-07-04 2012-03-28 Beijing Grand Golden-Bright Engineering & Technologies Co. Ltd. A method for recombining catalytic hydrocarbons
DE102005029643B3 (de) * 2005-06-23 2006-07-20 Uhde Gmbh Verfahren zur Gewinnung von Reinstyrol aus einer Pyrolysebenzinfraktion
EP2167210A2 (en) * 2006-08-09 2010-03-31 AMT International, Inc. Three phase extractive distillation with multiple columns connected in series
CN101121634B (zh) * 2006-08-11 2010-06-16 中国石油化工股份有限公司 裂解汽油中苯乙烯的回收方法
US7666299B2 (en) * 2007-08-10 2010-02-23 Amt International, Inc. Extractive distillation process for recovering aromatics from petroleum streams
CN101429091B (zh) * 2007-11-07 2011-07-20 中国石油化工股份有限公司 萃取精馏回收苯乙烯的脱色方法
CN101468938B (zh) * 2007-12-28 2012-09-05 中国石油化工股份有限公司 从烃类混合物中萃取精馏分离苯乙烯的复合溶剂及方法
CN102036726B (zh) 2008-03-25 2013-07-03 台湾中油股份有限公司 改进的使用水溶性萃取溶剂的萃取蒸馏方法
CN101759520B (zh) * 2008-12-25 2012-12-12 中国石油化工股份有限公司 从烃类混合物中萃取精馏分离苯乙烯的方法
CN101875592B (zh) * 2009-04-30 2013-07-31 中国石油化工股份有限公司 萃取精馏分离苯乙烯所用萃取溶剂的再生方法
US8696871B2 (en) * 2009-06-02 2014-04-15 Uop Llc Apparatus for removing a contaminant from a solvent separation process
US20100300939A1 (en) * 2009-06-02 2010-12-02 Uop Llc Process for Removing a Contaminant from an Aromatic Selective Solvent
US8771476B2 (en) * 2009-07-17 2014-07-08 Gtc Technology Lp Methods for inhibiting polymerization of vinyl aromatic compounds during extractive distillation
US8361312B2 (en) * 2009-07-17 2013-01-29 Gtc Technology, Lp Methods for removal of colored- and sulfur-containing impurities from hydrocarbon streams
US8460517B2 (en) * 2009-09-02 2013-06-11 Gtc Technology Us Llc Methods and apparatuses for steam addition to a reboiler coupled to an extractive distillation column for improved extractive distillation
CN102311304B (zh) * 2010-06-29 2014-10-01 中国石油化工股份有限公司 一种萃取精馏分离苯乙烯的复合溶剂及应用
EP2778158A1 (en) * 2013-03-14 2014-09-17 Advanced Technology Materials, Inc. Sulfolane mixtures as ambient aprotic polar solvents
KR101515816B1 (ko) * 2014-03-05 2015-05-04 주식회사 에젤 고비점, 중비점 및 저비점 성분을 포함하는 원료의 정제 장치 및 정제 방법
US10427994B2 (en) 2014-09-05 2019-10-01 Scg Chemicals Co., Ltd. Separation process for C8 aromatics mixture
EP2993163B1 (en) * 2014-09-05 2018-02-21 Scg Chemicals Co. Ltd. Process for the separation of ethylbenzene
WO2016036392A1 (en) * 2014-09-05 2016-03-10 Scg Chemicals Company Limited Process for the enhanced separation of ethylbenzene
US9221729B1 (en) * 2015-02-23 2015-12-29 Allnew Chemical Technology Company Extractive distillation for aromatics recovery
US10301235B1 (en) 2016-02-19 2019-05-28 Agilyx Corporation Systems and methods for recycling waste plastics, including waste polystyrene
WO2019137383A1 (zh) * 2018-01-12 2019-07-18 中国石油化工股份有限公司 萃取精馏分离苯乙烯所用溶剂的净化及苯乙烯分离方法
CN110627623B (zh) * 2019-09-06 2020-09-22 陕西煤业化工集团神木天元化工有限公司 酚类产品中碱性氮化物的分离系统及方法
EP3907211A1 (en) 2020-05-08 2021-11-10 Sulzer Management AG A process and apparatus for preparing a purified styrene composition from styrene containing feedstock
US11407947B2 (en) 2020-12-10 2022-08-09 Agilyx Corporation Systems and methods for recycling waste plastics

Family Cites Families (25)

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US2380019A (en) * 1942-02-09 1945-07-10 Lummus Co Azeotropic distillation
US2385235A (en) * 1942-10-26 1945-09-18 Lummus Co Styrene distillation
US2467197A (en) * 1945-09-06 1949-04-12 Allied Chem & Dye Corp Azeotropic distillation of styrene
US2480919A (en) * 1946-03-13 1949-09-06 Allied Chem & Dye Corp Recovery of styrene by azeotropic distillation
US2753381A (en) * 1953-12-18 1956-07-03 Phillips Petroleum Co Nu-acyl pyrrolidines as selective solvents
US2831039A (en) * 1955-04-04 1958-04-15 Standard Oil Co Solvent extraction
US2943122A (en) * 1957-06-19 1960-06-28 Ohio Oil Company Fractionation of mixtures of aromatic compounds utilizing gamma lactum solvents
US3018228A (en) * 1958-08-04 1962-01-23 Monsanto Chemicals Extractive distillation process
US3210259A (en) * 1961-06-26 1965-10-05 Monsanto Co Extractive separation process
US3272723A (en) * 1962-10-24 1966-09-13 Monsanto Co Purification of xylenes from styrene by distillation in the presence of combined azeotroping agent and solvent additive
DE1188075B (de) * 1963-03-12 1965-03-04 Erdoelchemie Gmbh Verfahren zur Trennung von o-Xylol und Styrol
BE745743A (fr) * 1969-02-17 1970-07-16 Toray Industries Procedes de recuperation de styrene et de xylenes a partir d'huile craquee et nouveaux produits ainsi obtenus (
JPS5021B1 (US06373033-20020416-M00035.png) * 1970-07-18 1975-01-06
JPS5516330B2 (US06373033-20020416-M00035.png) * 1972-05-20 1980-05-01
US3953300A (en) * 1972-11-29 1976-04-27 Snam Progetti, S.P.A. Process for separating a high purity vinyl aromatic hydrocarbon from hydrocarbon mixtures containing the same
US4031153A (en) * 1975-09-25 1977-06-21 Phillips Petroleum Company Separation of styrene from xylenes
US4371427A (en) * 1981-06-16 1983-02-01 Phillips Petroleum Company Extractive distillation
US4401517A (en) * 1981-11-20 1983-08-30 Phillips Petroleum Company Vapor-liquid extractive distillation with dialkyl sulfone/water combination
US4514261A (en) * 1984-08-31 1985-04-30 El Paso Products Company Refining of tertiary butylstyrene
US4543437A (en) * 1984-12-24 1985-09-24 El Paso Products Company Refining of tertiary butylstyrene
US4543438A (en) * 1984-12-24 1985-09-24 El Paso Products Company Tertiary-butylstyrene recovery
US4959128A (en) * 1990-02-26 1990-09-25 Lloyd Berg Separation of styrene from ethyl benzene by extractive distillation
US4966656A (en) * 1990-06-04 1990-10-30 Lloyd Berg Separation of styrene from ethyl benzene or o-xylene by azeotropic or extractive distillation with esters
US5100514A (en) * 1991-03-01 1992-03-31 Lloyd Berg Separation of pyridine from water by extractive distillation
US5399244A (en) * 1993-12-06 1995-03-21 Glitsch, Inc. Process to recover benzene from mixed hydrocarbons by extractive distillation

Also Published As

Publication number Publication date
TW450993B (en) 2001-08-21
CN1077560C (zh) 2002-01-09
KR20000015878A (ko) 2000-03-15
CN1225081A (zh) 1999-08-04
ID16811A (id) 1997-11-13
WO1997044298A1 (en) 1997-11-27
AU2937997A (en) 1997-12-09
US5849982A (en) 1998-12-15
IN191114B (US06373033-20020416-M00035.png) 2003-09-20
AR007039A1 (es) 1999-10-13
ZA972966B (en) 1997-11-21
JPH11509868A (ja) 1999-08-31
KR100330488B1 (ko) 2002-06-20

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