JP2526099B2 - 角質繊維染色組成物 - Google Patents
角質繊維染色組成物Info
- Publication number
- JP2526099B2 JP2526099B2 JP63169571A JP16957188A JP2526099B2 JP 2526099 B2 JP2526099 B2 JP 2526099B2 JP 63169571 A JP63169571 A JP 63169571A JP 16957188 A JP16957188 A JP 16957188A JP 2526099 B2 JP2526099 B2 JP 2526099B2
- Authority
- JP
- Japan
- Prior art keywords
- dyeing composition
- color
- present
- dyeing
- substance
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/10—Preparations for permanently dyeing the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/347—Phenols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4926—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having six membered rings
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4953—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom containing pyrimidine ring derivatives, e.g. minoxidil
Description
【発明の詳細な説明】 〔産業上の利用分野〕 本発明は染色組成物に関し、更に詳細には毛髪等の角
質繊維を高彩度に染色することができる角質繊維染色組
成物に関する。
質繊維を高彩度に染色することができる角質繊維染色組
成物に関する。
毛髪等の角質繊維の染色には、従来より顕色物質とカ
ツプリング物質を組み合せて用いる、いわゆる酸化染色
剤が広く使用されている。この酸化染色剤は顕色物質と
カツプリング物質の酸化カツプリングによつて生じる、
いわゆる酸化色素が毛髪等を強く染色することを利用し
たものである。そして顕色物質としては、一般にp−フ
エニレンジアミン誘導体、p−アミノフエノール誘導
体、ジアミノピリジン誘導体、4−アミノピラゾロン誘
導体、複素環状ヒドラゾン等が使用されている。
ツプリング物質を組み合せて用いる、いわゆる酸化染色
剤が広く使用されている。この酸化染色剤は顕色物質と
カツプリング物質の酸化カツプリングによつて生じる、
いわゆる酸化色素が毛髪等を強く染色することを利用し
たものである。そして顕色物質としては、一般にp−フ
エニレンジアミン誘導体、p−アミノフエノール誘導
体、ジアミノピリジン誘導体、4−アミノピラゾロン誘
導体、複素環状ヒドラゾン等が使用されている。
しかしながら、従来の酸化染色剤は、彩度、染着力お
よび堅ろう性において未だ満足すべきものではなかつ
た。
よび堅ろう性において未だ満足すべきものではなかつ
た。
そこで本発明者らは前記問題点を解決すべく種々検討
を重ねた結果、顕色物質として特定のトリアミノピリミ
ジン誘導体を使用することにより、角質繊維を高彩度で
強い色調に染色することが可能となり、かつその染色は
優れた堅ろう性を有することを見出し、本発明を完成し
た。
を重ねた結果、顕色物質として特定のトリアミノピリミ
ジン誘導体を使用することにより、角質繊維を高彩度で
強い色調に染色することが可能となり、かつその染色は
優れた堅ろう性を有することを見出し、本発明を完成し
た。
すなわち、本発明は、次式(I)または(I′) で表わされるトリアミノピリミジン誘導体〔以下化合物
(I)と称する〕またはその塩からなる顕色物質、およ
びレゾルシン、2−メチルレゾルシン、4−クロロレゾ
ルシン、4−プロピル−2,6−ジアミノピリジンまたは
3,4−ジメチル−2,6−ジアミノピリジンの1種または2
種以上からなるカップリング物質を含有することを特徴
とする角質繊維染色組成物を提供するものである。
(I)と称する〕またはその塩からなる顕色物質、およ
びレゾルシン、2−メチルレゾルシン、4−クロロレゾ
ルシン、4−プロピル−2,6−ジアミノピリジンまたは
3,4−ジメチル−2,6−ジアミノピリジンの1種または2
種以上からなるカップリング物質を含有することを特徴
とする角質繊維染色組成物を提供するものである。
本発明に使用される化合物(I)の塩としては、塩
酸、硫酸、リン酸等の無機酸または、炭素数1〜20の直
鎖もしくは分岐アルキル基を有するカルボン酸、ヒドロ
キシカルボン酸、ポリヒドロキシカルボン酸、スルホン
酸等の有機酸が挙げられ、塩酸、硫酸、リン酸、酢酸、
プロピオン酸、乳酸、クエン酸等が好ましい。
酸、硫酸、リン酸等の無機酸または、炭素数1〜20の直
鎖もしくは分岐アルキル基を有するカルボン酸、ヒドロ
キシカルボン酸、ポリヒドロキシカルボン酸、スルホン
酸等の有機酸が挙げられ、塩酸、硫酸、リン酸、酢酸、
プロピオン酸、乳酸、クエン酸等が好ましい。
本発明に使用される顕色物質は、レゾルシン系のカツ
プリング物質と組み合せることにより高彩度の赤系色調
が得られ、特にレゾルシン、2−メチルレゾルシン、4
−クロロレゾルシンをカツプリング物質とすると、高彩
度のオレンジ〜赤の色調が得られる。また、本発明に使
用される顕色物質を、ジアミノピリジン系のカツプリン
グ物質と組み合わせることによりあざやかな黄色が得ら
れ、特に4−プロピル−2,6−ジアミノピリジン、3,4−
ジメチル−2,6−ジアミノピリジンをカツプリング物質
として用いると高彩度の黄色が得られる。
プリング物質と組み合せることにより高彩度の赤系色調
が得られ、特にレゾルシン、2−メチルレゾルシン、4
−クロロレゾルシンをカツプリング物質とすると、高彩
度のオレンジ〜赤の色調が得られる。また、本発明に使
用される顕色物質を、ジアミノピリジン系のカツプリン
グ物質と組み合わせることによりあざやかな黄色が得ら
れ、特に4−プロピル−2,6−ジアミノピリジン、3,4−
ジメチル−2,6−ジアミノピリジンをカツプリング物質
として用いると高彩度の黄色が得られる。
本発明の染色組成物中の顕色物質とカツプリング物質
の配合割合は、一方の成分が他方に比べ過剰となつてい
てもさしつかえないが、モル比で1:0.5〜1:2程度である
ことが好ましい。また顕色物質およびカツプリング物質
は、ともに単独でも二種以上を組み合わせても使用する
ことができる。
の配合割合は、一方の成分が他方に比べ過剰となつてい
てもさしつかえないが、モル比で1:0.5〜1:2程度である
ことが好ましい。また顕色物質およびカツプリング物質
は、ともに単独でも二種以上を組み合わせても使用する
ことができる。
また本発明の染色組成物には所望の色調を得るため必
要であれば、更に公知の顕色物質、通常の直染性染料等
を配合することができる。
要であれば、更に公知の顕色物質、通常の直染性染料等
を配合することができる。
本発明染色組成物は、空気中の酸素によつても酸化カ
ツプリングを生起し、毛髪等を染色するが、化学的酸化
剤を添加することにより酸化カツプリングを生起させる
のが好ましい。特に好ましい酸化剤としては、過酸化水
素;過酸化水素が尿素、メラミン又は硼酸ナトリウムに
付加した生成物;このような過酸化水素付加物と過酸化
カリウム−二硫酸との混合物等が挙げられる。
ツプリングを生起し、毛髪等を染色するが、化学的酸化
剤を添加することにより酸化カツプリングを生起させる
のが好ましい。特に好ましい酸化剤としては、過酸化水
素;過酸化水素が尿素、メラミン又は硼酸ナトリウムに
付加した生成物;このような過酸化水素付加物と過酸化
カリウム−二硫酸との混合物等が挙げられる。
本発明の染色組成物は通常、クリーム、エマルジヨ
ン、ゲル、溶液等の剤型で提供されるのが好ましい。こ
のような剤型とするには、前記顕色物質およびカツプリ
ング物質に、通常化粧品分野において用いられる湿潤剤
(乳化剤)、可溶化剤、増粘剤、安定化剤、感触向上
剤、整髪基剤、香料等を添加し、常法に従つて製造すれ
ばよい。ここで用いられる湿潤剤(乳化剤)としては、
例えばアルキルベンゼンスルホネート、脂肪アルコール
サルフエート、アルキルスルホネート、脂肪酸アルカノ
ールアミド、エチレンオキシドと脂肪アルコールとの付
加生成物等が挙げられる。また増粘剤としては、例えば
メチルセルロース、デンプン、高級脂肪アルコール、パ
ラフイン油、脂肪酸等が挙げられ、安定化剤としては、
例えば亜硫酸塩等の還元剤、ヒドロキノン誘導体、キレ
ート剤等が挙げられ、感触向上剤、整髪基剤としては、
例えばシリコーン、高級アルコール、各種非イオン界面
活性剤等の油剤、各種のカチオンポリマー等が挙げられ
る。
ン、ゲル、溶液等の剤型で提供されるのが好ましい。こ
のような剤型とするには、前記顕色物質およびカツプリ
ング物質に、通常化粧品分野において用いられる湿潤剤
(乳化剤)、可溶化剤、増粘剤、安定化剤、感触向上
剤、整髪基剤、香料等を添加し、常法に従つて製造すれ
ばよい。ここで用いられる湿潤剤(乳化剤)としては、
例えばアルキルベンゼンスルホネート、脂肪アルコール
サルフエート、アルキルスルホネート、脂肪酸アルカノ
ールアミド、エチレンオキシドと脂肪アルコールとの付
加生成物等が挙げられる。また増粘剤としては、例えば
メチルセルロース、デンプン、高級脂肪アルコール、パ
ラフイン油、脂肪酸等が挙げられ、安定化剤としては、
例えば亜硫酸塩等の還元剤、ヒドロキノン誘導体、キレ
ート剤等が挙げられ、感触向上剤、整髪基剤としては、
例えばシリコーン、高級アルコール、各種非イオン界面
活性剤等の油剤、各種のカチオンポリマー等が挙げられ
る。
これらの剤型における顕色物質とカツプリング物質の
配合量は、合計で0.2〜5重量%(以下単に%で示
す)、特に1〜3%が好ましい。湿潤剤(乳化剤)は通
常0.5〜30%、増粘剤は0.1〜25%配合されるのが好まし
い。
配合量は、合計で0.2〜5重量%(以下単に%で示
す)、特に1〜3%が好ましい。湿潤剤(乳化剤)は通
常0.5〜30%、増粘剤は0.1〜25%配合されるのが好まし
い。
またこれらの剤型において、組成物全体のpHは8〜10
程度に調整されるのが好ましい。
程度に調整されるのが好ましい。
本発明染色組成物を用いて角質繊維の染色を実施する
には、例えば本発明染色組成物に酸化剤を添加して酸化
カツプリングを行い染色液を調製し、この染色液を角質
繊維に適用し、10〜50分、好ましくは25〜35分前後の作
用時間をおいて角質繊維を洗浄した後乾燥することによ
り行なわれる。ここで染色液の適用は15〜40℃で行なわ
れる。
には、例えば本発明染色組成物に酸化剤を添加して酸化
カツプリングを行い染色液を調製し、この染色液を角質
繊維に適用し、10〜50分、好ましくは25〜35分前後の作
用時間をおいて角質繊維を洗浄した後乾燥することによ
り行なわれる。ここで染色液の適用は15〜40℃で行なわ
れる。
本発明の染色組成物を用いて角質繊維を染色すれば、
顕色物質とカツプリング物質の組み合せにより黄〜赤〜
青さらに灰色〜黒褐色まで幅広い染色が可能であり、そ
の色調は高彩度である。特に、レゾルシン系のカツプリ
ング物質と組み合せることにより高彩度の赤系色調が、
またアミノピリジン系のカツプリング物質と組み合せる
ことにより高彩度の黄色が得られる。しかも得られた色
調は良好な耐光性、耐洗浄性及び耐摩耗性を有してい
る。
顕色物質とカツプリング物質の組み合せにより黄〜赤〜
青さらに灰色〜黒褐色まで幅広い染色が可能であり、そ
の色調は高彩度である。特に、レゾルシン系のカツプリ
ング物質と組み合せることにより高彩度の赤系色調が、
またアミノピリジン系のカツプリング物質と組み合せる
ことにより高彩度の黄色が得られる。しかも得られた色
調は良好な耐光性、耐洗浄性及び耐摩耗性を有してい
る。
次に実施例を挙げて本発明を詳細に説明するが、本発
明はこれによつて制限されるものではない。
明はこれによつて制限されるものではない。
実施例1 ベース組成: (%) オレイン酸 10 オレイン酸ジエタノールアミド 8 オレイルアルコール 2 ポリオキシエチレンオクチルドデシルエーテル 10 (平均EO20モル付加) エタノール 15 プロピレングリコール 10 塩化アンモニウム 3 25%アンモニア 7 水 35 上記組成からなるベース100g中に4,5,6−トリアミノ
−2(1H)−ピリミジンチオン0.01モル及び表1に示す
カツプリング物質0.01モルを混入した。次いで組成物の
pHをアンモニアにて9.5に調整することにより、本発明
染色組成物を製造した。
−2(1H)−ピリミジンチオン0.01モル及び表1に示す
カツプリング物質0.01モルを混入した。次いで組成物の
pHをアンモニアにて9.5に調整することにより、本発明
染色組成物を製造した。
本発明染色組成物100gに対し、等重量の6%過酸化水
素水溶液を加えて染色液を調製した。この染色液を白毛
混じりの人毛に塗布し、30℃で30分間放置した。次いで
毛髪を通常のシヤンプーで洗浄し、乾燥した。得られた
染色の色調を観察した結果を表1に示す。
素水溶液を加えて染色液を調製した。この染色液を白毛
混じりの人毛に塗布し、30℃で30分間放置した。次いで
毛髪を通常のシヤンプーで洗浄し、乾燥した。得られた
染色の色調を観察した結果を表1に示す。
───────────────────────────────────────────────────── フロントページの続き (56)参考文献 特開 昭51−123838(JP,A) 特開 昭53−6440(JP,A) 特開 平2−172909(JP,A) 西独国特許2714831(DE,A)
Claims (1)
- 【請求項1】次式(I)または(I′) で表わされるトリアミノピリミジン誘導体またはその塩
からなる顕色物質、およびレゾルシン、2−メチルレゾ
ルシン、4−クロロレゾルシン、4−プロピル−2,6−
ジアミノピリジンまたは3,4−ジメチル−2,6−ジアミノ
ピリジンの1種または2種以上からなるカップリング物
質を含有することを特徴とする角質繊維染色組成物。
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP63169571A JP2526099B2 (ja) | 1988-07-07 | 1988-07-07 | 角質繊維染色組成物 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP63169571A JP2526099B2 (ja) | 1988-07-07 | 1988-07-07 | 角質繊維染色組成物 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPH0219576A JPH0219576A (ja) | 1990-01-23 |
JP2526099B2 true JP2526099B2 (ja) | 1996-08-21 |
Family
ID=15888943
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP63169571A Expired - Fee Related JP2526099B2 (ja) | 1988-07-07 | 1988-07-07 | 角質繊維染色組成物 |
Country Status (1)
Country | Link |
---|---|
JP (1) | JP2526099B2 (ja) |
Cited By (13)
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US7288639B2 (en) | 2004-12-15 | 2007-10-30 | L'oreal S.A. | Dyssymmetrical diazo compounds having at least one 4-pyridinium unit and a cationic or non-cationic linker, compositions comprising them, method of coloring, and device |
US7326259B2 (en) | 2004-06-23 | 2008-02-05 | L'oreal S.A. | Use of polycationic compounds in the dyeing of keratinous fibres |
US7329288B2 (en) | 2004-02-27 | 2008-02-12 | L'oreal S.A. | N-heteroaryl secondary para-phenylenediamine, a dye composition comprising such a para-phenylenediamine, a process for preparing this composition and use thereof |
US7347879B2 (en) | 2004-02-27 | 2008-03-25 | L'Oreál, S.A. | Sulfur-containing secondary para-phenylenediamines dye compositions comprising such para-phenylenediamines, processes, and uses thereof |
US7384432B2 (en) | 2004-02-27 | 2008-06-10 | L'oreal S.A. | Secondary para-phenylenediamines having a carboxyl group, dye compositions comprising the same, and dyeing processes using the compositions |
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DE2714831A1 (de) | 1977-04-02 | 1978-10-12 | Henkel Kgaa | Haarfaerbemittel |
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US7485155B2 (en) | 2004-12-23 | 2009-02-03 | L'oreal S.A. | Process for washing colored keratinous fibers with a composition comprising at least one nonionic surfactant and method for protecting the color |
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US7635394B2 (en) | 2005-11-09 | 2009-12-22 | L'oreal S.A. | Composition for the dyeing of keratin fibers comprising at least one 3-amino-pyrazolopyridine derivatives |
US7857864B2 (en) | 2005-11-09 | 2010-12-28 | L'oreal S.A. | Composition for the dyeing of keratin fibers comprising at least one 3-amino-pyrazolopyridine derivative |
US7674299B2 (en) | 2006-12-21 | 2010-03-09 | L'oreal S.A. | Direct dye composition comprising a cationic surfactant, a bioheteropolysaccharide, an amphoteric surfactant and direct dye |
US7799094B2 (en) | 2006-12-21 | 2010-09-21 | L'oreal S.A. | Oxidation dye composition comprising a cationic surfactant, a bioheteropolysaccharide, an amphoteric surfactant and a dye precursor |
US7578856B2 (en) | 2007-05-09 | 2009-08-25 | L'oreal S.A. | Dyeing compositions comprising at least one aminopyrazolopyridine oxidation base, at least one coupler and at least one C4-C30 polyol and methods and use thereof |
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