JP2019500433A - 電気光学アセンブリのためのポリウレタン接着層 - Google Patents
電気光学アセンブリのためのポリウレタン接着層 Download PDFInfo
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- JP2019500433A JP2019500433A JP2018516171A JP2018516171A JP2019500433A JP 2019500433 A JP2019500433 A JP 2019500433A JP 2018516171 A JP2018516171 A JP 2018516171A JP 2018516171 A JP2018516171 A JP 2018516171A JP 2019500433 A JP2019500433 A JP 2019500433A
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- adhesive
- electro
- polyurethane
- optic
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
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Abstract
Description
本出願は、2015年9月30日に出願された米国出願第62/235,480号および2015年10月1日に出願された米国出願第62/235,580号に基づく優先権を主張している。これら両方の全体の内容、および以下に陳述されるすべての他の米国特許、および公開され、そして同時係属中の出願は、それらの全体が参考として本明細書中に援用される。
ポリウレタンは、広範な用途で(例えば、接着剤として)使用される。この接着剤は、電気光学アセンブリで利用することができ、電気光学アセンブリは、一般に、複数の機能層を含み、電気泳動ディスプレイなどのディスプレイを形成するために使用することができる。かかるアセンブリは、電気光学材料、フロントプレーン、およびバックプレーンの各層を備え得る。電気光学材料は、一般に、異なる電場が材料に印加された場合に少なくとも1つの光学特性(例えば、光伝送、反射率、発光)が異なる少なくとも2つの表示状態を有する。電気光学ディスプレイは、良好な輝度およびコントラスト、視野角の広さ、状態双安定性、および消費電力の低下に寄与し得る。
本発明は、電気光学アセンブリで用いるポリウレタン接着剤材料である。ポリウレタン接着剤は、典型的には、少なくともエンドキャッピング環状カルボナート基を含むが、ポリウレタン接着剤は、さらなる機能的な要素および/または架橋剤を含み得る。いくつかの実施形態では、接着剤を、2つまたはそれを超える硬化工程によって形成する。各硬化工程は、接着剤が各硬化工程で少なくとも1回硬化されるような、例えば、接着剤の架橋、接着剤の熱可塑性乾燥、接着剤のエンドキャッピング、接着剤の鎖延長、および/またはその組み合わせを含み得る。
本発明は、電気光学アセンブリ(例えば、封入電気泳動ディスプレイ)に組み込むのに非常に適している新規のクラスのポリウレタン接着剤層を含む。ポリウレタン接着剤は、典型的には、少なくとも1つの環状カルボナート基を含むが、ポリウレタン接着剤は、さらなる機能的な要素および/または架橋剤を含み得る。いくつかの実施形態では、接着剤を、2つまたはそれを超える硬化工程によって形成する。各硬化工程は、接着剤が各硬化工程で少なくとも1回硬化されるような、例えば、接着剤の架橋、接着剤の熱可塑性乾燥、接着剤のエンドキャッピング、接着剤の鎖延長、および/またはその組み合わせを含み得る。
(a)電気泳動粒子、流体、および流体添加物;例えば、米国特許第7,002,728号;および同第7,679,814号を参照のこと;
(b)カプセル、バインダー、および封入プロセス;例えば、米国特許第6,922,276号;および同第7,411,719号を参照のこと;
(c)電気光学材料を含む薄膜およびサブアセンブリ;例えば、米国特許第6,982,178;および同第7,839,564号を参照のこと;
(d)ディスプレイで使用されるバックプレーン、接着剤層、および他の補助層、ならびに方法;例えば、米国特許第7,116,318号;および同第7,535,624号を参照のこと;
(e)色の形成および色の調整;例えば、米国特許第7,075,502号;および米国特許出願公開第2007/0109219号を参照のこと;
(f)ディスプレイの応用;例えば、米国特許第7,312,784号;および米国特許出願公開第2006/0279527号を参照のこと;ならびに
(g)米国特許第6,241,921号;同第6,950,220号;および同第7,420,549号;ならびに米国特許出願公開第2009/0046082号に記載の非電気泳動ディスプレイ。
いくつかの実施形態では、式(III)は、式(IV):
いくつかの実施形態では、式(IX)は、式(X):
いくつかの実施形態では、式(XX)は、式(XXI):
いくつかの実施形態では、複数のタイプのエンドキャッピング試薬のうちの少なくとも1つは、エーテルを含み、それにより、エーテルを含むエンドキャッピングされたポリウレタンが得られる。いくつかの実施形態では、エーテルを含むエンドキャッピング試薬は、式(XXIII):
いくつかの実施形態では、式(XXVI)は、式(XXVII):
いくつかの実施形態では、式(XXVI)は、式(XXVII):
実施例1.非化学量論量の末端基単量体を使用して鎖延長し、低い溶媒含有量で、触媒を使用し、分散後に鎖延長したポリウレタン分散液の合成−グリセリンカルボナート(CCARB)末端基(EG)を使用(接着剤A)
試料I:試料I:4.8重量%カルボジイミド架橋剤(単一硬化)
試料II:8.0重量%カルボジイミド架橋剤(単一硬化)
試料III:4.8重量%カルボジイミド架橋剤+2.1重量%エポキシ架橋剤(二重硬化)
試料IV:8.0重量%カルボジイミド架橋剤+1.0重量%エポキシ架橋剤(二重硬化)
Claims (21)
- ポリウレタン層を含む電気光学アセンブリであって、前記ポリウレタン層が、式(XII):
R1は、水素、任意選択的に置換されたアルキル、任意選択的に置換されたヘテロアルキル、任意選択的に置換されたアリール、任意選択的に置換されたヘテロアリール、任意選択的に置換されたハライド、および任意選択的に置換されたヒドロキシルからなる群から選択され;
Lは連結基であり、任意選択的に存在せず;
nは1から4であり;
- Lが、任意選択的に置換されたアルキレンまたは任意選択的に置換されたヘテロアルキレンである、請求項1に記載の電気光学アセンブリ。
- R1が水素である、請求項1に記載の電気光学アセンブリ。
- 前記ポリウレタン層が第2のタイプのエンドキャッピング基をさらに含む、請求項1に記載の電気光学アセンブリ。
- 前記第2のタイプのエンドキャッピング基がピロリドンを含む、請求項4に記載の電気光学アセンブリ。
- 前記ピロリドンが、式(XVI):
各R2は、同一であるか異なり、水素、任意選択的に置換されたアルキル、任意選択的に置換されたヘテロアルキル、任意選択的に置換されたアリール、任意選択的に置換されたヘテロアリールからなる群から選択され;
Mは連結基であり、任意選択的に存在せず;
- Mが、任意選択的に置換されたアルキレンまたは任意選択的に置換されたヘテロアルキレンである、請求項6に記載の電気光学アセンブリ。
- 前記第2のタイプのエンドキャッピング基が、式(XXXIII):
Lは連結基であり、任意選択的に存在せず;
各R3は同一であるか異なり、−(CH2)n−または−O−(CH2)nを含み;
各nは同一であるか異なり、1〜4であり;
- Lが、任意選択的に置換されたアルキレンまたは任意選択的に置換されたヘテロアルキレンである、請求項8に記載の電気光学アセンブリ。
- 前記環状カルボナートエンドキャッピング基の前記第2のタイプのエンドキャッピング基に対する比が1:2と2:1との間である、請求項4に記載の電気光学アセンブリ。
- 前記ポリウレタンが、ジイソシアナート化合物と少なくとも1つのタイプのジオールとの反応、および環状カルボナートエンドキャッピング試薬との反応によって形成される、請求項1に記載の電気光学アセンブリ。
- 前記ジイソシアナートが4,4’−メチレンビス(シクロヘキシルイソシアナート)である、請求項11に記載の電気光学アセンブリ。
- 前記ポリウレタンが、ジイソシアナート化合物と少なくとも1つのタイプのジオールとの反応後に、環状カルボナートエンドキャッピング試薬およびピロリドンを含む第2のタイプのエンドキャッピング試薬と反応させることによって形成される、請求項5に記載の電気光学アセンブリ。
- 前記ジイソシアナートが4,4’−メチレンビス(シクロヘキシルイソシアナート)である、請求項13に記載の電気光学アセンブリ。
- 前記エンドキャッピング環状カルボナートが、いかなる溶媒も含まない全組成に対して約2重量%と約10重量%との間の重量百分率である、請求項1に記載の電気光学アセンブリ。
- 前記エンドキャッピング環状カルボナートがポリウレタンの約5〜15モル%で提供される、請求項1に記載の電気光学アセンブリ。
- 前記エンドキャッピング試薬が、いかなる溶媒も含まない全組成に対して約2重量%と約10重量%との間の重量百分率の量である、請求項4に記載の電気光学アセンブリ。
- 請求項1に記載の電気光学アセンブリを含む電気光学ディスプレイ。
- 前記電気光学媒体が封入電気泳動媒体を含む、請求項18に記載の電気光学ディスプレイ。
- 請求項4に記載の電気光学アセンブリを含む電気光学ディスプレイ。
- 前記電気光学媒体が封入電気泳動媒体を含む、請求項20に記載の電気光学ディスプレイ。
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CN113004854A (zh) | 2021-06-22 |
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EP3356445A4 (en) | 2018-11-14 |
KR20180045032A (ko) | 2018-05-03 |
WO2017059011A1 (en) | 2017-04-06 |
CN108138023A (zh) | 2018-06-08 |
US10174232B2 (en) | 2019-01-08 |
CN113004854B (zh) | 2022-09-30 |
JP2019194717A (ja) | 2019-11-07 |
TWI631200B (zh) | 2018-08-01 |
EP3356445B1 (en) | 2021-01-06 |
TW201831637A (zh) | 2018-09-01 |
TWI674307B (zh) | 2019-10-11 |
KR102044643B1 (ko) | 2019-11-13 |
US20190106609A1 (en) | 2019-04-11 |
JP6704043B2 (ja) | 2020-06-03 |
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