JP2019182792A - 水中油型睫用化粧料 - Google Patents
水中油型睫用化粧料 Download PDFInfo
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- JP2019182792A JP2019182792A JP2018076351A JP2018076351A JP2019182792A JP 2019182792 A JP2019182792 A JP 2019182792A JP 2018076351 A JP2018076351 A JP 2018076351A JP 2018076351 A JP2018076351 A JP 2018076351A JP 2019182792 A JP2019182792 A JP 2019182792A
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- oil
- water
- cosmetics
- cosmetic
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Abstract
Description
本実施形態の水中油型睫用化粧料は、(A)水溶性皮膜形成剤((A)成分という場合もある)と、(B)水溶性増粘剤((B)成分という場合もある)と、(C)粉体((C)成分という場合もある)と、(D)界面活性剤((D)成分という場合もある)と、を含有する。
水溶性皮膜形成剤としては、例えば、ポリビニルピロリドン(PVP)、ポリビニルアルコール(PVA)、ビニルピロリドン/酢酸ビニル共重合体(VP/VAコポリマー)が挙げられる。(A)成分は、1種を単独で又は2種以上を組み合わせて用いることができる。
水溶性増粘剤としては、セルロース系増粘剤、多糖類系増粘剤、粘土鉱物、デンプン系増粘剤、アルギン酸系増粘剤、動物系増粘剤等が挙げられる。(B)成分は、1種を単独で又は2種以上を組み合わせて用いることができる。
粉体としては、化粧料に用いられる公知の粉体を配合することができ、体質粉体、着色顔料等が挙げられる。粉体は、球状、板状、針状等の形状;煙霧状、微粒子、顔料級等の粒子径;多孔質、無孔質等の粒子構造等について特に限定されず用いることができる。(C)成分は、1種を単独で又は2種以上を組み合わせて用いることができる。
界面活性剤としては、化粧料に用いられる公知の界面活性剤を配合することができる。(D)成分は、2種以上を組み合わせて用いることができる。
本実施形態の水中油型睫用化粧料は、上述した成分以外の水性成分及び油性成分を含むことができる。
加熱により溶融した化粧料を容量30mLのスクリューカップに充填し、25℃にて一晩放置した測定用サンプルを用意する。この測定用サンプルについて、FUDOHレオメーター RT−2002D・D((株)レオテック製)を用い、25℃にて、感圧軸8φ球形、針入速度6cm/min、針入深度10mmで稠度を得た。
本実施形態に係る水中油型睫用化粧料の製造方法としては、例えば、上述した(A)成分、(B)成分及びその他の水性成分、並びに、(C)成分を含む水相部と、上述した(D)成分及び油性成分を含む油相部をそれぞれ調製し、これらを混合、乳化することにより得ることができる。
化粧品評価専門パネル20名に、実施例及び比較例の水中油型睫用化粧料を左右の睫に10回程度塗布し、下記の評価項目について、下記の評価基準に従って5段階評価を行いサンプル毎に評点を付し、更に全パネルの評点の平均点を下記の判定基準に従って判定した。
[評価項目]
(a)化粧膜の均一性(ダマ付きのなさ):重ね塗りしたときにダマ付きがないかを評価
(b)付着性:化粧料が上滑りせず、睫に適量付着するかを評価
(c)ツヤ感:化粧膜にツヤがあるかを評価
(d)黒さ:化粧膜に黒さがあるかを評価
(e)カール効果:化粧料を使用後、睫がカールアップしているかと、その後パネルに通常通り過ごしてもらった6時間後にカールが持続しているかを評価
[評点:評価基準]
5点:非常に良い
4点:良い
3点:普通
2点:悪い
1点:非常に悪い
[判定基準(評点の平均点)]
◎:4以上
○:3以上4未満
△:2以上3未満
×:2未満
保存安定性については、各試料の調整直後の状態を基準として、50℃恒温槽に1ヶ月保管し、稠度の変化及び排液の有無を下記4段階基準により評価した。
[判定基準]
◎:変化なし
○:ごくわずかに変化がある
△:やや変化がある
×:著しい変化がある
表1〜5に示す組成の水中油型睫用化粧料を以下の製法により調製し、上記の評価を行った。その結果を併せて表1〜5に示す。
成分1〜13を混合し、90℃に加熱して溶解、均一化し、これを油相とした。次に、90℃に加熱溶解した成分14〜28を油相に添加し、乳化した。乳化物を冷却した後、成分29を添加し、撹拌した。これを容器に充填し、水中油型睫化粧料を得た。
*2:ゴーセノール EG−25(日本合成化学工業社製、製品名)
*3:PVP/VA S−630(アイエスピー・ジャパン社製、製品名)
*4:DK BLACK No.2(大東化成工業社製、製品名、比重1.8)
*5:TAROX BL−100(チタン工業社製、製品名、比重5)
*6:ヨドゾールGH800F(アクゾノーベル社製、製品名)
(成分) (配合割合(質量%))
1. カルナウバロウ 4.0
2. ミツロウ 4.0
3. ステアリン酸 3.0
4. ステアリルアルコール 2.0
5. トコフェロール 適量
6. シメチコン 適量
7. PEG−60水添ヒマシ油 5.0
8. ステアリン酸グリセリル 1.5
9. カーボンブラック *4 1.0
10.ナイロンファイバー 2.0
11.精製水 残量
12.1,3−ブチレングリコール 5.0
13.防腐剤 適量
14.AMP 1.0
15.ポリビニルピロリドン *1 1.0
16.キサンタンガム 0.2
17.アクリル酸アルキル共重合体エマルション *6 25.0
成分(1)〜(10)を約90℃に加熱し、均一に混合し、これを油相とした。次に、得られた油相に、約90℃に加熱した成分(11)〜(16)を添加し、乳化した。乳化物を冷却した後、成分(17)を添加し、撹拌した。これを容器に充填し、水中油型のマスカラ(繊維入り)を得た。
得られたマスカラ(繊維入り)について、上記同様の評価を行ったところ、(a)化粧膜の均一性(ダマ付きのなさ)、(b)付着性、(c)ツヤ感、(d)黒さ、(e)カール効果、及び(f)保存安定性のすべての評価項目において「◎」の評価であった。
(成分) (配合割合(質量%))
1. パラフィンワックス 3.0
2. ミツロウ 5.0
3. ステアリン酸 2.0
4. パルミチン酸 1.0
5. セトステアリルアルコール 1.0
6. トコフェロール 適量
7. シメチコン 適量
8. PEG−60水添ヒマシ油 5.0
9. ステアリン酸グリセリル 1.5
10.カーボンブラック *4 0.05
11.シリカ 2.0
12.精製水 残量
13.1,3−ブチレングリコール 5.0
14.防腐剤 適量
15.トリエタノールアミン 1.0
16.ポリビニルアルコール *2 1.0
17.キサンタンガム 0.1
18.アクリル酸アルキル共重合体エマルション *6 30.0
成分(1)〜(11)を約90℃に加熱し、均一に混合し、これを油相とした。次に、得られた油相に、約90℃に加熱した成分(12)〜(17)を添加し、乳化した。乳化物を冷却した後、成分(18)を添加し、撹拌した。これを容器に充填し、マスカラ下地を得た。
Claims (6)
- (A)水溶性皮膜形成剤と、(B)水溶性増粘剤と、(C)粉体と、(D)界面活性剤と、を含有し、
前記(B)成分が、セルロース系増粘剤及び多糖類系増粘剤からなる群より選択される少なくとも1種の水溶性増粘剤を含み、
前記(C)成分が、カーボンブラックを含み、
前記(D)成分が、(D1)HLB10〜17の非イオン界面活性剤と、(D2)HLB8未満の非イオン界面活性剤とを含む、水中油型睫用化粧料。 - 前記(C)成分の含有量が、水中油型睫用化粧料全量を基準として、0.01〜10.0質量%である、請求項1に記載の水中油型睫用化粧料。
- 前記カーボンブラックの含有量が、水中油型睫用化粧料全量を基準として、0.01〜5.0質量%である、請求項1又は2に記載の水中油型睫用化粧料。
- 前記カーボンブラック以外の粉体の含有量が、水中油型睫用化粧料全量を基準として、6.0質量%以下である、請求項1〜3のいずれか一項に記載の水中油型睫用化粧料。
- 前記(D1)成分と前記(D2)成分との質量比(D1)/(D2)が、1.4〜6.0である、請求項1〜4のいずれか一項に記載の水中油型睫用化粧料。
- 前記(D1)成分の含有量が、水中油型睫用化粧料全量を基準として、1.0〜10.0質量%であり、
前記(D2)成分の含有量が、水中油型睫用化粧料全量を基準として、0.5〜8.0質量%である、請求項1〜5のいずれか一項に記載の水中油型睫用化粧料。
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JP2004168791A (ja) * | 2002-11-15 | 2004-06-17 | Nippon Shokubai Co Ltd | 蓄熱体及び蓄熱体の製造方法 |
JP2010254670A (ja) * | 2009-03-31 | 2010-11-11 | Kose Corp | 水中油型乳化化粧料 |
JP2013075870A (ja) * | 2011-09-30 | 2013-04-25 | Mandom Corp | 乳化型制汗化粧料 |
WO2014054731A1 (ja) * | 2012-10-03 | 2014-04-10 | 株式会社日本触媒 | 吸水剤及びその製造方法 |
JP2017197460A (ja) * | 2016-04-26 | 2017-11-02 | ジェイオーコスメティックス株式会社 | 水中油型睫毛用化粧料 |
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JP5841163B2 (ja) * | 2011-03-15 | 2016-01-13 | ロレアル | まつ毛用化粧組成物 |
JP5681737B2 (ja) * | 2013-02-19 | 2015-03-11 | 株式会社 資生堂 | 睫毛用化粧料 |
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JP2004168791A (ja) * | 2002-11-15 | 2004-06-17 | Nippon Shokubai Co Ltd | 蓄熱体及び蓄熱体の製造方法 |
JP2010254670A (ja) * | 2009-03-31 | 2010-11-11 | Kose Corp | 水中油型乳化化粧料 |
JP2013075870A (ja) * | 2011-09-30 | 2013-04-25 | Mandom Corp | 乳化型制汗化粧料 |
WO2014054731A1 (ja) * | 2012-10-03 | 2014-04-10 | 株式会社日本触媒 | 吸水剤及びその製造方法 |
JP2017197460A (ja) * | 2016-04-26 | 2017-11-02 | ジェイオーコスメティックス株式会社 | 水中油型睫毛用化粧料 |
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FR3080043B1 (fr) | 2022-09-02 |
CN110354020A (zh) | 2019-10-22 |
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