JP2016523852A - 5−ヒドロキシメチルフルフラール(hmf)の調製のための方法 - Google Patents
5−ヒドロキシメチルフルフラール(hmf)の調製のための方法 Download PDFInfo
- Publication number
- JP2016523852A JP2016523852A JP2016518622A JP2016518622A JP2016523852A JP 2016523852 A JP2016523852 A JP 2016523852A JP 2016518622 A JP2016518622 A JP 2016518622A JP 2016518622 A JP2016518622 A JP 2016518622A JP 2016523852 A JP2016523852 A JP 2016523852A
- Authority
- JP
- Japan
- Prior art keywords
- hmf
- mixture
- product mixture
- reactor
- intermediate product
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 0 *C(NC(*=C)=O)=O Chemical compound *C(NC(*=C)=O)=O 0.000 description 3
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
- C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
- C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
- C07D307/48—Furfural
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Furan Compounds (AREA)
- Catalysts (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP13171627.6 | 2013-06-12 | ||
| EP13171627.6A EP2813494A1 (de) | 2013-06-12 | 2013-06-12 | Verfahren zur Herstellung von 5-Hydroxymethylfurfural (HMF) |
| PCT/IB2014/062121 WO2014199306A2 (de) | 2013-06-12 | 2014-06-11 | Verfahren zur herstellung von 5-hydroxymethylfurfural (hmf) |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2016523852A true JP2016523852A (ja) | 2016-08-12 |
| JP2016523852A5 JP2016523852A5 (enExample) | 2017-07-20 |
Family
ID=48577625
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2016518622A Withdrawn JP2016523852A (ja) | 2013-06-12 | 2014-06-11 | 5−ヒドロキシメチルフルフラール(hmf)の調製のための方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US9260402B2 (enExample) |
| EP (2) | EP2813494A1 (enExample) |
| JP (1) | JP2016523852A (enExample) |
| KR (1) | KR20160018703A (enExample) |
| CN (1) | CN105452231A (enExample) |
| CA (1) | CA2914308A1 (enExample) |
| RU (1) | RU2016100205A (enExample) |
| WO (1) | WO2014199306A2 (enExample) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| PL3077453T3 (pl) | 2013-12-06 | 2018-10-31 | Basf Se | Kompozycja plastyfikatora zawierająca pochodne tetrahydrofuranu i estry kwasu 1,2-cykloheksanodikarboksylowego |
| US10532990B2 (en) | 2014-12-12 | 2020-01-14 | Virdia, Inc. | Methods for converting cellulose to furanic products |
| WO2016206909A1 (de) | 2015-06-24 | 2016-12-29 | Basf Se | Verfahren zur herstellung von 5-hydroxymethylfurfural und huminen |
| WO2016207025A1 (de) | 2015-06-24 | 2016-12-29 | Basf Se | Verfahren zum herstellen und abtrennen von hmf |
| WO2016207365A1 (de) * | 2015-06-24 | 2016-12-29 | Basf Se | Verfahren zur kontinuierlichen herstellung von 5-hydroxymethyl-furfural (hmf) in einer reaktoranordnung |
| WO2017184545A1 (en) * | 2016-04-18 | 2017-10-26 | Rennovia, Inc. | Conversion of fructose-containing feedstocks to hmf-containing product |
| JP6293333B2 (ja) * | 2016-06-27 | 2018-03-14 | 日本食品化工株式会社 | 5−ヒドロキシメチル−2−フルフラールの製造方法 |
| WO2018003295A1 (ja) * | 2016-06-27 | 2018-01-04 | 日本食品化工株式会社 | 5-ヒドロキシメチル-2-フルフラールの製造方法 |
| EP3366468B1 (de) * | 2017-02-27 | 2022-04-06 | AVA Biochem AG | Verfahren zur herstellung thermisch härtbarer harze sowie durch das verfahren erhältliche harze |
| EP3366714B1 (de) * | 2017-02-27 | 2022-03-30 | AVA Biochem AG | Verfahren zur herstellung thermisch härtbarer phenolharze sowie durch das verfahren erhältliche phenolharze |
| EP3366712A1 (de) | 2017-02-27 | 2018-08-29 | AVALON Industries AG | Neue hmf-oligomere |
| CN107501215B (zh) * | 2017-09-18 | 2020-10-30 | 中国农业大学 | 一种连续化制备5-羟甲基糠醛及其衍生物的方法和装置 |
| EP3498699A1 (en) | 2017-12-13 | 2019-06-19 | Basf Se | Chromatography method for the purification of furfural derivatives |
| CN111187236A (zh) * | 2018-11-14 | 2020-05-22 | 远东新世纪股份有限公司 | 自含有葡萄糖的原料制备5-羟甲基糠醛的方法 |
| RU187166U1 (ru) * | 2018-11-15 | 2019-02-21 | Нина Владимировна Смирнова | Лабораторно-исследовательский стенд для изучения процессов дегидратации углеводов |
| CN109651308A (zh) * | 2019-02-15 | 2019-04-19 | 陈茁 | 一种5-羟甲基糠醛的纯化方法 |
| EP3956319A1 (en) * | 2019-04-15 | 2022-02-23 | Stora Enso Oyj | Process for the recovery of solvent and isolation of humin materials and compositions thereof |
| CN110368985B (zh) * | 2019-07-04 | 2022-05-31 | 浙江工业大学 | 一种用于5-hmf合成的催化剂及5-hmf的制备方法 |
| CN110586114A (zh) * | 2019-09-19 | 2019-12-20 | 天津大学 | 一种铜铬铝水滑石催化剂的制备方法及催化氧化5-羟甲基糠醛的应用 |
| CN119462576A (zh) * | 2024-11-26 | 2025-02-18 | 中国科学技术大学 | 制备5,5'-氧基双亚甲基-2-糠醛的方法及装置 |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4400468A (en) | 1981-10-05 | 1983-08-23 | Hydrocarbon Research Inc. | Process for producing adipic acid from biomass |
| DE3601281A1 (de) | 1986-01-17 | 1987-07-23 | Sueddeutsche Zucker Ag | Verfahren zur herstellung von 5-hydroxymethylfurfural einschliesslich eines kristallinen produktes unter ausschliesslicher verwendung von wasser als loesungsmittel |
| FR2663933B1 (fr) | 1990-06-27 | 1994-06-17 | Beghin Say Sa | Nouveau procede de preparation du 5-hydroxymethylfurfural a partir de saccharides. |
| FR2664273B1 (fr) | 1990-06-27 | 1994-04-29 | Beghin Say Sa | Nouveau procede de preparation du 5-hydroxymethylfurfural a partir de saccharides. |
| FR2670209B1 (fr) * | 1990-12-07 | 1995-04-28 | Commissariat Energie Atomique | Procede de preparation d'hydroxymethyl-5 furfural par catalyse heterogene. |
| DE10202838A1 (de) | 2002-01-24 | 2003-08-07 | Basf Ag | Verfahren zur Abtrennung von Säuren aus chemischen Reaktionsgemischen mit Hilfe von ionischen Flüssigkeiten |
| FR2858618B1 (fr) | 2003-08-07 | 2006-02-24 | Sucreries Et Raffineries D Ers | Procede et reacteur de fabrication d'hydroxymethylfurfural |
| EP1834950A1 (en) | 2006-03-10 | 2007-09-19 | Avantium International B.V. | Method for the synthesis of 5-alkoxymethylfurfural ethers and their use |
| ATE473218T1 (de) | 2006-03-10 | 2010-07-15 | Furanix Technologies Bv | Verwendung organischer säureester von 5- hydroxymethylfurfural |
| AU2008208869B2 (en) | 2007-01-23 | 2014-02-13 | Basf Se | Method for producing glucose by enzymatic hydrolysis of cellulose that can be pretreated with an ionic liquid containing a polyatomic anion |
| AU2008208870B2 (en) | 2007-01-23 | 2013-05-02 | Basf Se | Method for producing glucose by enzymatic hydrolysis of cellulose that is obtained from material containing ligno-cellulose using an ionic liquid that comprises a polyatomic anion |
| CN101812039B (zh) * | 2010-05-14 | 2012-09-26 | 天津大学 | 一种利用离子液体催化生成5-羟甲基糠醛的方法 |
| EP2782897A4 (en) * | 2011-11-23 | 2015-06-24 | Segetis Inc | PROCESS FOR PREPARING LÄVULINIC ACID |
| CN102399203B (zh) | 2011-12-19 | 2014-05-07 | 浙江大学 | 一种离子液体降解碳水化合物制备5-羟甲基糠醛的方法 |
-
2013
- 2013-06-12 EP EP13171627.6A patent/EP2813494A1/de not_active Withdrawn
-
2014
- 2014-06-11 CA CA2914308A patent/CA2914308A1/en not_active Abandoned
- 2014-06-11 KR KR1020167000350A patent/KR20160018703A/ko not_active Withdrawn
- 2014-06-11 CN CN201480044683.9A patent/CN105452231A/zh active Pending
- 2014-06-11 US US14/302,046 patent/US9260402B2/en not_active Expired - Fee Related
- 2014-06-11 WO PCT/IB2014/062121 patent/WO2014199306A2/de not_active Ceased
- 2014-06-11 JP JP2016518622A patent/JP2016523852A/ja not_active Withdrawn
- 2014-06-11 RU RU2016100205A patent/RU2016100205A/ru not_active Application Discontinuation
- 2014-06-11 EP EP14810780.8A patent/EP3008048A4/de not_active Withdrawn
Also Published As
| Publication number | Publication date |
|---|---|
| WO2014199306A3 (de) | 2015-04-23 |
| WO2014199306A2 (de) | 2014-12-18 |
| RU2016100205A3 (enExample) | 2018-04-26 |
| EP3008048A4 (de) | 2016-12-14 |
| CA2914308A1 (en) | 2014-12-18 |
| CN105452231A (zh) | 2016-03-30 |
| US9260402B2 (en) | 2016-02-16 |
| US20140371473A1 (en) | 2014-12-18 |
| EP3008048A2 (de) | 2016-04-20 |
| RU2016100205A (ru) | 2017-07-17 |
| KR20160018703A (ko) | 2016-02-17 |
| EP2813494A1 (de) | 2014-12-17 |
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| US9162998B2 (en) | Preparation of 5-hydroxymethylfurfural (HMF) from saccharide solutions in the presence of a solvent having a boiling point greater than 60° C. and less than 200° C. (at standard pressure, called low boiler for short) | |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20170609 |
|
| A621 | Written request for application examination |
Free format text: JAPANESE INTERMEDIATE CODE: A621 Effective date: 20170609 |
|
| A761 | Written withdrawal of application |
Free format text: JAPANESE INTERMEDIATE CODE: A761 Effective date: 20171204 |