EP3008048A4 - Verfahren zur herstellung von 5-hydroxymethylfurfural (hmf) - Google Patents

Verfahren zur herstellung von 5-hydroxymethylfurfural (hmf)

Info

Publication number
EP3008048A4
EP3008048A4 EP14810780.8A EP14810780A EP3008048A4 EP 3008048 A4 EP3008048 A4 EP 3008048A4 EP 14810780 A EP14810780 A EP 14810780A EP 3008048 A4 EP3008048 A4 EP 3008048A4
Authority
EP
European Patent Office
Prior art keywords
hydroxymethylfurfural
hmf
preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
EP14810780.8A
Other languages
English (en)
French (fr)
Other versions
EP3008048A2 (de
Inventor
Dr Benoit Blank
Dr Alois Kindler
Dr Peter Bassler
Dr Markus Piepenbrink
Ortmund Lang
Carmen Feldner
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Priority to EP14810780.8A priority Critical patent/EP3008048A4/de
Publication of EP3008048A2 publication Critical patent/EP3008048A2/de
Publication of EP3008048A4 publication Critical patent/EP3008048A4/de
Withdrawn legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D307/00Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40Radicals substituted by oxygen atoms
    • C07D307/46Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/009Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D307/00Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40Radicals substituted by oxygen atoms
    • C07D307/46Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48Furfural
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Furan Compounds (AREA)
  • Catalysts (AREA)
EP14810780.8A 2013-06-12 2014-06-11 Verfahren zur herstellung von 5-hydroxymethylfurfural (hmf) Withdrawn EP3008048A4 (de)

Priority Applications (1)

Application Number Priority Date Filing Date Title
EP14810780.8A EP3008048A4 (de) 2013-06-12 2014-06-11 Verfahren zur herstellung von 5-hydroxymethylfurfural (hmf)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP13171627.6A EP2813494A1 (de) 2013-06-12 2013-06-12 Verfahren zur Herstellung von 5-Hydroxymethylfurfural (HMF)
PCT/IB2014/062121 WO2014199306A2 (de) 2013-06-12 2014-06-11 Verfahren zur herstellung von 5-hydroxymethylfurfural (hmf)
EP14810780.8A EP3008048A4 (de) 2013-06-12 2014-06-11 Verfahren zur herstellung von 5-hydroxymethylfurfural (hmf)

Publications (2)

Publication Number Publication Date
EP3008048A2 EP3008048A2 (de) 2016-04-20
EP3008048A4 true EP3008048A4 (de) 2016-12-14

Family

ID=48577625

Family Applications (2)

Application Number Title Priority Date Filing Date
EP13171627.6A Withdrawn EP2813494A1 (de) 2013-06-12 2013-06-12 Verfahren zur Herstellung von 5-Hydroxymethylfurfural (HMF)
EP14810780.8A Withdrawn EP3008048A4 (de) 2013-06-12 2014-06-11 Verfahren zur herstellung von 5-hydroxymethylfurfural (hmf)

Family Applications Before (1)

Application Number Title Priority Date Filing Date
EP13171627.6A Withdrawn EP2813494A1 (de) 2013-06-12 2013-06-12 Verfahren zur Herstellung von 5-Hydroxymethylfurfural (HMF)

Country Status (8)

Country Link
US (1) US9260402B2 (de)
EP (2) EP2813494A1 (de)
JP (1) JP2016523852A (de)
KR (1) KR20160018703A (de)
CN (1) CN105452231A (de)
CA (1) CA2914308A1 (de)
RU (1) RU2016100205A (de)
WO (1) WO2014199306A2 (de)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
PL3077453T3 (pl) 2013-12-06 2018-10-31 Basf Se Kompozycja plastyfikatora zawierająca pochodne tetrahydrofuranu i estry kwasu 1,2-cykloheksanodikarboksylowego
US10532990B2 (en) 2014-12-12 2020-01-14 Virdia, Inc. Methods for converting cellulose to furanic products
WO2016206909A1 (de) 2015-06-24 2016-12-29 Basf Se Verfahren zur herstellung von 5-hydroxymethylfurfural und huminen
WO2016207025A1 (de) 2015-06-24 2016-12-29 Basf Se Verfahren zum herstellen und abtrennen von hmf
WO2016207365A1 (de) * 2015-06-24 2016-12-29 Basf Se Verfahren zur kontinuierlichen herstellung von 5-hydroxymethyl-furfural (hmf) in einer reaktoranordnung
WO2017184545A1 (en) * 2016-04-18 2017-10-26 Rennovia, Inc. Conversion of fructose-containing feedstocks to hmf-containing product
JP6293333B2 (ja) * 2016-06-27 2018-03-14 日本食品化工株式会社 5−ヒドロキシメチル−2−フルフラールの製造方法
WO2018003295A1 (ja) * 2016-06-27 2018-01-04 日本食品化工株式会社 5-ヒドロキシメチル-2-フルフラールの製造方法
EP3366468B1 (de) * 2017-02-27 2022-04-06 AVA Biochem AG Verfahren zur herstellung thermisch härtbarer harze sowie durch das verfahren erhältliche harze
EP3366714B1 (de) * 2017-02-27 2022-03-30 AVA Biochem AG Verfahren zur herstellung thermisch härtbarer phenolharze sowie durch das verfahren erhältliche phenolharze
EP3366712A1 (de) 2017-02-27 2018-08-29 AVALON Industries AG Neue hmf-oligomere
CN107501215B (zh) * 2017-09-18 2020-10-30 中国农业大学 一种连续化制备5-羟甲基糠醛及其衍生物的方法和装置
EP3498699A1 (de) 2017-12-13 2019-06-19 Basf Se Chromatographieverfahren zur reinigung von furfuralderivaten
CN111187236A (zh) * 2018-11-14 2020-05-22 远东新世纪股份有限公司 自含有葡萄糖的原料制备5-羟甲基糠醛的方法
RU187166U1 (ru) * 2018-11-15 2019-02-21 Нина Владимировна Смирнова Лабораторно-исследовательский стенд для изучения процессов дегидратации углеводов
CN109651308A (zh) * 2019-02-15 2019-04-19 陈茁 一种5-羟甲基糠醛的纯化方法
EP3956319A1 (de) * 2019-04-15 2022-02-23 Stora Enso Oyj Verfahren zur rückgewinnung von lösungsmittel und isolierung von huminmaterialien und zusammensetzungen davon
CN110368985B (zh) * 2019-07-04 2022-05-31 浙江工业大学 一种用于5-hmf合成的催化剂及5-hmf的制备方法
CN110586114A (zh) * 2019-09-19 2019-12-20 天津大学 一种铜铬铝水滑石催化剂的制备方法及催化氧化5-羟甲基糠醛的应用
CN119462576A (zh) * 2024-11-26 2025-02-18 中国科学技术大学 制备5,5'-氧基双亚甲基-2-糠醛的方法及装置

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102399203A (zh) * 2011-12-19 2012-04-04 浙江大学 一种离子液体降解碳水化合物制备5-羟甲基糠醛的方法

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4400468A (en) 1981-10-05 1983-08-23 Hydrocarbon Research Inc. Process for producing adipic acid from biomass
DE3601281A1 (de) 1986-01-17 1987-07-23 Sueddeutsche Zucker Ag Verfahren zur herstellung von 5-hydroxymethylfurfural einschliesslich eines kristallinen produktes unter ausschliesslicher verwendung von wasser als loesungsmittel
FR2663933B1 (fr) 1990-06-27 1994-06-17 Beghin Say Sa Nouveau procede de preparation du 5-hydroxymethylfurfural a partir de saccharides.
FR2664273B1 (fr) 1990-06-27 1994-04-29 Beghin Say Sa Nouveau procede de preparation du 5-hydroxymethylfurfural a partir de saccharides.
FR2670209B1 (fr) * 1990-12-07 1995-04-28 Commissariat Energie Atomique Procede de preparation d'hydroxymethyl-5 furfural par catalyse heterogene.
DE10202838A1 (de) 2002-01-24 2003-08-07 Basf Ag Verfahren zur Abtrennung von Säuren aus chemischen Reaktionsgemischen mit Hilfe von ionischen Flüssigkeiten
FR2858618B1 (fr) 2003-08-07 2006-02-24 Sucreries Et Raffineries D Ers Procede et reacteur de fabrication d'hydroxymethylfurfural
EP1834950A1 (de) 2006-03-10 2007-09-19 Avantium International B.V. Verfahren zur Herstellung von Alkoxymethylfurfuralen und deren Verwenung
ATE473218T1 (de) 2006-03-10 2010-07-15 Furanix Technologies Bv Verwendung organischer säureester von 5- hydroxymethylfurfural
AU2008208869B2 (en) 2007-01-23 2014-02-13 Basf Se Method for producing glucose by enzymatic hydrolysis of cellulose that can be pretreated with an ionic liquid containing a polyatomic anion
AU2008208870B2 (en) 2007-01-23 2013-05-02 Basf Se Method for producing glucose by enzymatic hydrolysis of cellulose that is obtained from material containing ligno-cellulose using an ionic liquid that comprises a polyatomic anion
CN101812039B (zh) * 2010-05-14 2012-09-26 天津大学 一种利用离子液体催化生成5-羟甲基糠醛的方法
EP2782897A4 (de) * 2011-11-23 2015-06-24 Segetis Inc Verfahren zur herstellung von lävulinsäure

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102399203A (zh) * 2011-12-19 2012-04-04 浙江大学 一种离子液体降解碳水化合物制备5-羟甲基糠醛的方法

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
ZUONJUN WI ET AL: "Entrainer-intensified vacuum reactive distillation process for the separation of 5-hydroxymethylfurfural from the dehydration of carbohydrates catalyzed by a metal salt-ionic liquid", GREEN CHEMISTRY, vol. 14, 7 March 2012 (2012-03-07), pages 1220 - 1226, XP002712463 *

Also Published As

Publication number Publication date
WO2014199306A3 (de) 2015-04-23
JP2016523852A (ja) 2016-08-12
WO2014199306A2 (de) 2014-12-18
RU2016100205A3 (de) 2018-04-26
CA2914308A1 (en) 2014-12-18
CN105452231A (zh) 2016-03-30
US9260402B2 (en) 2016-02-16
US20140371473A1 (en) 2014-12-18
EP3008048A2 (de) 2016-04-20
RU2016100205A (ru) 2017-07-17
KR20160018703A (ko) 2016-02-17
EP2813494A1 (de) 2014-12-17

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