EP3008048A4 - Process for the preparation of 5-hydroxymethylfurfural (hmf) - Google Patents
Process for the preparation of 5-hydroxymethylfurfural (hmf)Info
- Publication number
- EP3008048A4 EP3008048A4 EP14810780.8A EP14810780A EP3008048A4 EP 3008048 A4 EP3008048 A4 EP 3008048A4 EP 14810780 A EP14810780 A EP 14810780A EP 3008048 A4 EP3008048 A4 EP 3008048A4
- Authority
- EP
- European Patent Office
- Prior art keywords
- hydroxymethylfurfural
- hmf
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
- C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
- C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
- C07D307/48—Furfural
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Furan Compounds (AREA)
- Catalysts (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP14810780.8A EP3008048A4 (en) | 2013-06-12 | 2014-06-11 | Process for the preparation of 5-hydroxymethylfurfural (hmf) |
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP13171627.6A EP2813494A1 (en) | 2013-06-12 | 2013-06-12 | Method for the preparation of 5-hydroxymethylfurfural (HMF) |
EP14810780.8A EP3008048A4 (en) | 2013-06-12 | 2014-06-11 | Process for the preparation of 5-hydroxymethylfurfural (hmf) |
PCT/IB2014/062121 WO2014199306A2 (en) | 2013-06-12 | 2014-06-11 | Process for the preparation of 5-hydroxymethylfurfural (hmf) |
Publications (2)
Publication Number | Publication Date |
---|---|
EP3008048A2 EP3008048A2 (en) | 2016-04-20 |
EP3008048A4 true EP3008048A4 (en) | 2016-12-14 |
Family
ID=48577625
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP13171627.6A Withdrawn EP2813494A1 (en) | 2013-06-12 | 2013-06-12 | Method for the preparation of 5-hydroxymethylfurfural (HMF) |
EP14810780.8A Withdrawn EP3008048A4 (en) | 2013-06-12 | 2014-06-11 | Process for the preparation of 5-hydroxymethylfurfural (hmf) |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP13171627.6A Withdrawn EP2813494A1 (en) | 2013-06-12 | 2013-06-12 | Method for the preparation of 5-hydroxymethylfurfural (HMF) |
Country Status (8)
Country | Link |
---|---|
US (1) | US9260402B2 (en) |
EP (2) | EP2813494A1 (en) |
JP (1) | JP2016523852A (en) |
KR (1) | KR20160018703A (en) |
CN (1) | CN105452231A (en) |
CA (1) | CA2914308A1 (en) |
RU (1) | RU2016100205A (en) |
WO (1) | WO2014199306A2 (en) |
Families Citing this family (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
TR201808387T4 (en) | 2013-12-06 | 2018-07-23 | Basf Se | Emollient composition comprising tetra hydrofuran derivatives and 1,2-cyclohexane dicarboxylic acid ester. |
US10532990B2 (en) | 2014-12-12 | 2020-01-14 | Virdia, Inc. | Methods for converting cellulose to furanic products |
WO2016206909A1 (en) | 2015-06-24 | 2016-12-29 | Basf Se | Process for preparing 5-hydroxymethylfurfural and humins |
WO2016207365A1 (en) * | 2015-06-24 | 2016-12-29 | Basf Se | Method for continuously producing 5-hydroxymethylfurfural (hmf) in a reactor arrangement |
WO2016207025A1 (en) | 2015-06-24 | 2016-12-29 | Basf Se | Method for synthesizing and separating hmf |
WO2017184545A1 (en) * | 2016-04-18 | 2017-10-26 | Rennovia, Inc. | Conversion of fructose-containing feedstocks to hmf-containing product |
JP6293333B2 (en) * | 2016-06-27 | 2018-03-14 | 日本食品化工株式会社 | Process for producing 5-hydroxymethyl-2-furfural |
WO2018003295A1 (en) * | 2016-06-27 | 2018-01-04 | 日本食品化工株式会社 | 5-hydroxymethyl-2-furfural production method |
EP3366712A1 (en) | 2017-02-27 | 2018-08-29 | AVALON Industries AG | Novel hmf oligomers |
EP3366714B1 (en) * | 2017-02-27 | 2022-03-30 | AVA Biochem AG | Method for producing thermally curable phenol resins and phenol resin obtainable by the method |
EP3366468B1 (en) * | 2017-02-27 | 2022-04-06 | AVA Biochem AG | Method for producing thermally curable resin and resin obtainable by the method |
CN107501215B (en) * | 2017-09-18 | 2020-10-30 | 中国农业大学 | Method and device for continuously preparing 5-hydroxymethylfurfural and derivatives thereof |
EP3498699A1 (en) | 2017-12-13 | 2019-06-19 | Basf Se | Chromatography method for the purification of furfural derivatives |
TWI664291B (en) * | 2018-11-14 | 2019-07-01 | 遠東新世紀股份有限公司 | Method for preparing 5-hydroxymethyl furfural from raw materials containing glucose |
RU187166U1 (en) * | 2018-11-15 | 2019-02-21 | Нина Владимировна Смирнова | LABORATORY RESEARCH STAND FOR STUDYING CARBOHYDRATE DEHYDRATION PROCESSES |
CN109651308A (en) * | 2019-02-15 | 2019-04-19 | 陈茁 | A kind of purification process of 5 hydroxymethyl furfural |
CN110368985B (en) * | 2019-07-04 | 2022-05-31 | 浙江工业大学 | Catalyst for 5-HMF synthesis and preparation method of 5-HMF |
CN110586114A (en) * | 2019-09-19 | 2019-12-20 | 天津大学 | Preparation method of copper-chromium-aluminum hydrotalcite catalyst and application of catalyst in catalytic oxidation of 5-hydroxymethylfurfural |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102399203A (en) * | 2011-12-19 | 2012-04-04 | 浙江大学 | Method for preparing 5-hydroxymethylfurfural by degrading carbonhydrate through ionic liquid |
Family Cites Families (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4400468A (en) | 1981-10-05 | 1983-08-23 | Hydrocarbon Research Inc. | Process for producing adipic acid from biomass |
DE3601281A1 (en) | 1986-01-17 | 1987-07-23 | Sueddeutsche Zucker Ag | METHOD FOR PRODUCING 5-HYDROXYMETHYLFURFURAL, INCLUDING A CRYSTALINE PRODUCT, WITH THE EXCLUSIVE USE OF WATER AS A SOLVENT |
FR2664273B1 (en) | 1990-06-27 | 1994-04-29 | Beghin Say Sa | NEW PROCESS FOR THE PREPARATION OF 5-HYDROXYMETHYLFURFURAL FROM SACCHARIDES. |
FR2663933B1 (en) | 1990-06-27 | 1994-06-17 | Beghin Say Sa | NEW PROCESS FOR THE PREPARATION OF 5-HYDROXYMETHYLFURFURAL FROM SACCHARIDES. |
FR2670209B1 (en) * | 1990-12-07 | 1995-04-28 | Commissariat Energie Atomique | PROCESS FOR THE PREPARATION OF FURFURAL HYDROXYMETHYL-5 BY HETEROGENEOUS CATALYSIS. |
DE10202838A1 (en) | 2002-01-24 | 2003-08-07 | Basf Ag | Separation of acids from reaction mixtures by means of an auxiliary base that forms a liquid salt with the acid to result in two non-miscible phases with the product or solution of the product in a suitable solvent |
FR2858618B1 (en) * | 2003-08-07 | 2006-02-24 | Sucreries Et Raffineries D Ers | PROCESS AND REACTOR FOR MANUFACTURING HYDROXYMETHYLFURFURAL |
EP1834951A1 (en) | 2006-03-10 | 2007-09-19 | Avantium International B.V. | Method for the synthesis of organic acid esters of 5-hydroxymethylfurfural and their use |
EP1834950A1 (en) | 2006-03-10 | 2007-09-19 | Avantium International B.V. | Method for the synthesis of 5-alkoxymethylfurfural ethers and their use |
AU2008208869B2 (en) | 2007-01-23 | 2014-02-13 | Basf Se | Method for producing glucose by enzymatic hydrolysis of cellulose that can be pretreated with an ionic liquid containing a polyatomic anion |
WO2008090156A1 (en) | 2007-01-23 | 2008-07-31 | Basf Se | Method for producing glucose by enzymatic hydrolysis of cellulose that is obtained from material containing ligno-cellulose using an ionic liquid that comprises a polyatomic anion |
CN101812039B (en) * | 2010-05-14 | 2012-09-26 | 天津大学 | Method for generating 5-hydroxymethylfurfural by using ionic liquid catalysis |
KR20140097420A (en) * | 2011-11-23 | 2014-08-06 | 세게티스, 인코포레이티드. | Process to prepare levulinic acid |
-
2013
- 2013-06-12 EP EP13171627.6A patent/EP2813494A1/en not_active Withdrawn
-
2014
- 2014-06-11 RU RU2016100205A patent/RU2016100205A/en not_active Application Discontinuation
- 2014-06-11 JP JP2016518622A patent/JP2016523852A/en not_active Withdrawn
- 2014-06-11 WO PCT/IB2014/062121 patent/WO2014199306A2/en active Application Filing
- 2014-06-11 US US14/302,046 patent/US9260402B2/en not_active Expired - Fee Related
- 2014-06-11 EP EP14810780.8A patent/EP3008048A4/en not_active Withdrawn
- 2014-06-11 CN CN201480044683.9A patent/CN105452231A/en active Pending
- 2014-06-11 KR KR1020167000350A patent/KR20160018703A/en not_active Application Discontinuation
- 2014-06-11 CA CA2914308A patent/CA2914308A1/en not_active Abandoned
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102399203A (en) * | 2011-12-19 | 2012-04-04 | 浙江大学 | Method for preparing 5-hydroxymethylfurfural by degrading carbonhydrate through ionic liquid |
Non-Patent Citations (1)
Title |
---|
ZUONJUN WI ET AL: "Entrainer-intensified vacuum reactive distillation process for the separation of 5-hydroxymethylfurfural from the dehydration of carbohydrates catalyzed by a metal salt-ionic liquid", GREEN CHEMISTRY, vol. 14, 7 March 2012 (2012-03-07), pages 1220 - 1226, XP002712463 * |
Also Published As
Publication number | Publication date |
---|---|
WO2014199306A3 (en) | 2015-04-23 |
JP2016523852A (en) | 2016-08-12 |
EP3008048A2 (en) | 2016-04-20 |
US9260402B2 (en) | 2016-02-16 |
EP2813494A1 (en) | 2014-12-17 |
US20140371473A1 (en) | 2014-12-18 |
WO2014199306A2 (en) | 2014-12-18 |
CA2914308A1 (en) | 2014-12-18 |
KR20160018703A (en) | 2016-02-17 |
RU2016100205A3 (en) | 2018-04-26 |
CN105452231A (en) | 2016-03-30 |
RU2016100205A (en) | 2017-07-17 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PUAI | Public reference made under article 153(3) epc to a published international application that has entered the european phase |
Free format text: ORIGINAL CODE: 0009012 |
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17P | Request for examination filed |
Effective date: 20160112 |
|
AK | Designated contracting states |
Kind code of ref document: A2 Designated state(s): AL AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MK MT NL NO PL PT RO RS SE SI SK SM TR |
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AX | Request for extension of the european patent |
Extension state: BA ME |
|
DAX | Request for extension of the european patent (deleted) | ||
R17P | Request for examination filed (corrected) |
Effective date: 20160112 |
|
A4 | Supplementary search report drawn up and despatched |
Effective date: 20161110 |
|
RIC1 | Information provided on ipc code assigned before grant |
Ipc: B01D 3/00 20060101ALI20161104BHEP Ipc: C07D 307/48 20060101AFI20161104BHEP Ipc: C07D 307/46 20060101ALI20161104BHEP |
|
GRAP | Despatch of communication of intention to grant a patent |
Free format text: ORIGINAL CODE: EPIDOSNIGR1 |
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INTG | Intention to grant announced |
Effective date: 20170726 |
|
STAA | Information on the status of an ep patent application or granted ep patent |
Free format text: STATUS: THE APPLICATION IS DEEMED TO BE WITHDRAWN |
|
18D | Application deemed to be withdrawn |
Effective date: 20171206 |