EP3008048A4 - Process for the preparation of 5-hydroxymethylfurfural (hmf) - Google Patents

Process for the preparation of 5-hydroxymethylfurfural (hmf)

Info

Publication number
EP3008048A4
EP3008048A4 EP14810780.8A EP14810780A EP3008048A4 EP 3008048 A4 EP3008048 A4 EP 3008048A4 EP 14810780 A EP14810780 A EP 14810780A EP 3008048 A4 EP3008048 A4 EP 3008048A4
Authority
EP
European Patent Office
Prior art keywords
hydroxymethylfurfural
hmf
preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
EP14810780.8A
Other languages
German (de)
French (fr)
Other versions
EP3008048A2 (en
Inventor
Dr Benoit Blank
Dr Alois Kindler
Dr Peter Bassler
Dr Markus Piepenbrink
Ortmund Lang
Carmen Feldner
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Priority to EP14810780.8A priority Critical patent/EP3008048A4/en
Publication of EP3008048A2 publication Critical patent/EP3008048A2/en
Publication of EP3008048A4 publication Critical patent/EP3008048A4/en
Withdrawn legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48—Furfural
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Furan Compounds (AREA)
  • Catalysts (AREA)
EP14810780.8A 2013-06-12 2014-06-11 Process for the preparation of 5-hydroxymethylfurfural (hmf) Withdrawn EP3008048A4 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
EP14810780.8A EP3008048A4 (en) 2013-06-12 2014-06-11 Process for the preparation of 5-hydroxymethylfurfural (hmf)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP13171627.6A EP2813494A1 (en) 2013-06-12 2013-06-12 Method for the preparation of 5-hydroxymethylfurfural (HMF)
EP14810780.8A EP3008048A4 (en) 2013-06-12 2014-06-11 Process for the preparation of 5-hydroxymethylfurfural (hmf)
PCT/IB2014/062121 WO2014199306A2 (en) 2013-06-12 2014-06-11 Process for the preparation of 5-hydroxymethylfurfural (hmf)

Publications (2)

Publication Number Publication Date
EP3008048A2 EP3008048A2 (en) 2016-04-20
EP3008048A4 true EP3008048A4 (en) 2016-12-14

Family

ID=48577625

Family Applications (2)

Application Number Title Priority Date Filing Date
EP13171627.6A Withdrawn EP2813494A1 (en) 2013-06-12 2013-06-12 Method for the preparation of 5-hydroxymethylfurfural (HMF)
EP14810780.8A Withdrawn EP3008048A4 (en) 2013-06-12 2014-06-11 Process for the preparation of 5-hydroxymethylfurfural (hmf)

Family Applications Before (1)

Application Number Title Priority Date Filing Date
EP13171627.6A Withdrawn EP2813494A1 (en) 2013-06-12 2013-06-12 Method for the preparation of 5-hydroxymethylfurfural (HMF)

Country Status (8)

Country Link
US (1) US9260402B2 (en)
EP (2) EP2813494A1 (en)
JP (1) JP2016523852A (en)
KR (1) KR20160018703A (en)
CN (1) CN105452231A (en)
CA (1) CA2914308A1 (en)
RU (1) RU2016100205A (en)
WO (1) WO2014199306A2 (en)

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TR201808387T4 (en) 2013-12-06 2018-07-23 Basf Se Emollient composition comprising tetra hydrofuran derivatives and 1,2-cyclohexane dicarboxylic acid ester.
US10532990B2 (en) 2014-12-12 2020-01-14 Virdia, Inc. Methods for converting cellulose to furanic products
WO2016206909A1 (en) 2015-06-24 2016-12-29 Basf Se Process for preparing 5-hydroxymethylfurfural and humins
WO2016207365A1 (en) * 2015-06-24 2016-12-29 Basf Se Method for continuously producing 5-hydroxymethylfurfural (hmf) in a reactor arrangement
WO2016207025A1 (en) 2015-06-24 2016-12-29 Basf Se Method for synthesizing and separating hmf
WO2017184545A1 (en) * 2016-04-18 2017-10-26 Rennovia, Inc. Conversion of fructose-containing feedstocks to hmf-containing product
JP6293333B2 (en) * 2016-06-27 2018-03-14 日本食品化工株式会社 Process for producing 5-hydroxymethyl-2-furfural
WO2018003295A1 (en) * 2016-06-27 2018-01-04 日本食品化工株式会社 5-hydroxymethyl-2-furfural production method
EP3366712A1 (en) 2017-02-27 2018-08-29 AVALON Industries AG Novel hmf oligomers
EP3366714B1 (en) * 2017-02-27 2022-03-30 AVA Biochem AG Method for producing thermally curable phenol resins and phenol resin obtainable by the method
EP3366468B1 (en) * 2017-02-27 2022-04-06 AVA Biochem AG Method for producing thermally curable resin and resin obtainable by the method
CN107501215B (en) * 2017-09-18 2020-10-30 中国农业大学 Method and device for continuously preparing 5-hydroxymethylfurfural and derivatives thereof
EP3498699A1 (en) 2017-12-13 2019-06-19 Basf Se Chromatography method for the purification of furfural derivatives
TWI664291B (en) * 2018-11-14 2019-07-01 遠東新世紀股份有限公司 Method for preparing 5-hydroxymethyl furfural from raw materials containing glucose
RU187166U1 (en) * 2018-11-15 2019-02-21 Нина Владимировна Смирнова LABORATORY RESEARCH STAND FOR STUDYING CARBOHYDRATE DEHYDRATION PROCESSES
CN109651308A (en) * 2019-02-15 2019-04-19 陈茁 A kind of purification process of 5 hydroxymethyl furfural
CN110368985B (en) * 2019-07-04 2022-05-31 浙江工业大学 Catalyst for 5-HMF synthesis and preparation method of 5-HMF
CN110586114A (en) * 2019-09-19 2019-12-20 天津大学 Preparation method of copper-chromium-aluminum hydrotalcite catalyst and application of catalyst in catalytic oxidation of 5-hydroxymethylfurfural

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102399203A (en) * 2011-12-19 2012-04-04 浙江大学 Method for preparing 5-hydroxymethylfurfural by degrading carbonhydrate through ionic liquid

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4400468A (en) 1981-10-05 1983-08-23 Hydrocarbon Research Inc. Process for producing adipic acid from biomass
DE3601281A1 (en) 1986-01-17 1987-07-23 Sueddeutsche Zucker Ag METHOD FOR PRODUCING 5-HYDROXYMETHYLFURFURAL, INCLUDING A CRYSTALINE PRODUCT, WITH THE EXCLUSIVE USE OF WATER AS A SOLVENT
FR2664273B1 (en) 1990-06-27 1994-04-29 Beghin Say Sa NEW PROCESS FOR THE PREPARATION OF 5-HYDROXYMETHYLFURFURAL FROM SACCHARIDES.
FR2663933B1 (en) 1990-06-27 1994-06-17 Beghin Say Sa NEW PROCESS FOR THE PREPARATION OF 5-HYDROXYMETHYLFURFURAL FROM SACCHARIDES.
FR2670209B1 (en) * 1990-12-07 1995-04-28 Commissariat Energie Atomique PROCESS FOR THE PREPARATION OF FURFURAL HYDROXYMETHYL-5 BY HETEROGENEOUS CATALYSIS.
DE10202838A1 (en) 2002-01-24 2003-08-07 Basf Ag Separation of acids from reaction mixtures by means of an auxiliary base that forms a liquid salt with the acid to result in two non-miscible phases with the product or solution of the product in a suitable solvent
FR2858618B1 (en) * 2003-08-07 2006-02-24 Sucreries Et Raffineries D Ers PROCESS AND REACTOR FOR MANUFACTURING HYDROXYMETHYLFURFURAL
EP1834951A1 (en) 2006-03-10 2007-09-19 Avantium International B.V. Method for the synthesis of organic acid esters of 5-hydroxymethylfurfural and their use
EP1834950A1 (en) 2006-03-10 2007-09-19 Avantium International B.V. Method for the synthesis of 5-alkoxymethylfurfural ethers and their use
AU2008208869B2 (en) 2007-01-23 2014-02-13 Basf Se Method for producing glucose by enzymatic hydrolysis of cellulose that can be pretreated with an ionic liquid containing a polyatomic anion
WO2008090156A1 (en) 2007-01-23 2008-07-31 Basf Se Method for producing glucose by enzymatic hydrolysis of cellulose that is obtained from material containing ligno-cellulose using an ionic liquid that comprises a polyatomic anion
CN101812039B (en) * 2010-05-14 2012-09-26 天津大学 Method for generating 5-hydroxymethylfurfural by using ionic liquid catalysis
KR20140097420A (en) * 2011-11-23 2014-08-06 세게티스, 인코포레이티드. Process to prepare levulinic acid

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102399203A (en) * 2011-12-19 2012-04-04 浙江大学 Method for preparing 5-hydroxymethylfurfural by degrading carbonhydrate through ionic liquid

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
ZUONJUN WI ET AL: "Entrainer-intensified vacuum reactive distillation process for the separation of 5-hydroxymethylfurfural from the dehydration of carbohydrates catalyzed by a metal salt-ionic liquid", GREEN CHEMISTRY, vol. 14, 7 March 2012 (2012-03-07), pages 1220 - 1226, XP002712463 *

Also Published As

Publication number Publication date
WO2014199306A3 (en) 2015-04-23
JP2016523852A (en) 2016-08-12
EP3008048A2 (en) 2016-04-20
US9260402B2 (en) 2016-02-16
EP2813494A1 (en) 2014-12-17
US20140371473A1 (en) 2014-12-18
WO2014199306A2 (en) 2014-12-18
CA2914308A1 (en) 2014-12-18
KR20160018703A (en) 2016-02-17
RU2016100205A3 (en) 2018-04-26
CN105452231A (en) 2016-03-30
RU2016100205A (en) 2017-07-17

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