JP2015517977A5 - - Google Patents
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- Publication number
- JP2015517977A5 JP2015517977A5 JP2014558764A JP2014558764A JP2015517977A5 JP 2015517977 A5 JP2015517977 A5 JP 2015517977A5 JP 2014558764 A JP2014558764 A JP 2014558764A JP 2014558764 A JP2014558764 A JP 2014558764A JP 2015517977 A5 JP2015517977 A5 JP 2015517977A5
- Authority
- JP
- Japan
- Prior art keywords
- process according
- adipic acid
- group
- mixtures
- metal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 claims 25
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 claims 18
- JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 claims 12
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims 9
- 235000011037 adipic acid Nutrition 0.000 claims 9
- 239000001361 adipic acid Substances 0.000 claims 9
- 229910052751 metal Inorganic materials 0.000 claims 8
- 239000002184 metal Substances 0.000 claims 8
- 239000000758 substrate Substances 0.000 claims 8
- 239000000203 mixture Substances 0.000 claims 7
- 229910052707 ruthenium Inorganic materials 0.000 claims 7
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims 6
- KJTLSVCANCCWHF-UHFFFAOYSA-N Ruthenium Chemical compound [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 claims 4
- 239000002638 heterogeneous catalyst Substances 0.000 claims 4
- 229910052702 rhenium Inorganic materials 0.000 claims 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 4
- 229910021529 ammonia Inorganic materials 0.000 claims 3
- 239000003054 catalyst Substances 0.000 claims 3
- 229910052739 hydrogen Inorganic materials 0.000 claims 3
- 239000001257 hydrogen Substances 0.000 claims 3
- 229910052741 iridium Inorganic materials 0.000 claims 3
- 229910052762 osmium Inorganic materials 0.000 claims 3
- 229910052763 palladium Inorganic materials 0.000 claims 3
- 229910052697 platinum Inorganic materials 0.000 claims 3
- WUAPFZMCVAUBPE-UHFFFAOYSA-N rhenium atom Chemical compound [Re] WUAPFZMCVAUBPE-UHFFFAOYSA-N 0.000 claims 3
- 229910052703 rhodium Inorganic materials 0.000 claims 3
- 239000002904 solvent Substances 0.000 claims 3
- 229920002292 Nylon 6 Polymers 0.000 claims 2
- DKGAVHZHDRPRBM-UHFFFAOYSA-N Tert-Butanol Chemical compound CC(C)(C)O DKGAVHZHDRPRBM-UHFFFAOYSA-N 0.000 claims 2
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims 2
- 150000002431 hydrogen Chemical class 0.000 claims 2
- ZQXSFZAMFNRZOQ-UHFFFAOYSA-N 2-methylpropan-2-ol;hydrate Chemical compound O.CC(C)(C)O ZQXSFZAMFNRZOQ-UHFFFAOYSA-N 0.000 claims 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 1
- 150000001298 alcohols Chemical class 0.000 claims 1
- 125000000217 alkyl group Chemical group 0.000 claims 1
- 150000001408 amides Chemical class 0.000 claims 1
- GCTOSMYFALESJI-UHFFFAOYSA-N azane;2-methylpropan-2-ol Chemical compound N.CC(C)(C)O GCTOSMYFALESJI-UHFFFAOYSA-N 0.000 claims 1
- 150000001720 carbohydrates Chemical class 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 claims 1
- 238000010924 continuous production Methods 0.000 claims 1
- 229910052802 copper Inorganic materials 0.000 claims 1
- 150000002170 ethers Chemical class 0.000 claims 1
- 229910052742 iron Inorganic materials 0.000 claims 1
- 239000007788 liquid Substances 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 239000000463 material Substances 0.000 claims 1
- 229910052759 nickel Inorganic materials 0.000 claims 1
- 150000003839 salts Chemical class 0.000 claims 1
- LMBFAGIMSUYTBN-MPZNNTNKSA-N teixobactin Chemical group C([C@H](C(=O)N[C@@H]([C@@H](C)CC)C(=O)N[C@@H](CO)C(=O)N[C@H](CCC(N)=O)C(=O)N[C@H]([C@@H](C)CC)C(=O)N[C@@H]([C@@H](C)CC)C(=O)N[C@@H](CO)C(=O)N[C@H]1C(N[C@@H](C)C(=O)N[C@@H](C[C@@H]2NC(=N)NC2)C(=O)N[C@H](C(=O)O[C@H]1C)[C@@H](C)CC)=O)NC)C1=CC=CC=C1 LMBFAGIMSUYTBN-MPZNNTNKSA-N 0.000 claims 1
- 229910052721 tungsten Inorganic materials 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201261602533P | 2012-02-23 | 2012-02-23 | |
| US61/602,533 | 2012-02-23 | ||
| PCT/US2013/025846 WO2013126250A1 (en) | 2012-02-23 | 2013-02-13 | Production of caprolactam from adipic acid |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2015517977A JP2015517977A (ja) | 2015-06-25 |
| JP2015517977A5 true JP2015517977A5 (enExample) | 2016-03-31 |
Family
ID=47748790
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2014558764A Pending JP2015517977A (ja) | 2012-02-23 | 2013-02-13 | アジピン酸からのカプロラクタムの生成 |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US8946411B2 (enExample) |
| EP (1) | EP2817293A1 (enExample) |
| JP (1) | JP2015517977A (enExample) |
| KR (1) | KR20140129076A (enExample) |
| CN (1) | CN104169259B (enExample) |
| AR (1) | AR089980A1 (enExample) |
| BR (1) | BR112014020642B1 (enExample) |
| HK (1) | HK1205121A1 (enExample) |
| IN (1) | IN2014DN07028A (enExample) |
| SA (1) | SA113340296B1 (enExample) |
| SG (1) | SG11201405045YA (enExample) |
| WO (1) | WO2013126250A1 (enExample) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2013090031A2 (en) | 2011-12-14 | 2013-06-20 | Rennovia, Inc. | Water concentration reduction process |
| WO2013090032A1 (en) | 2011-12-14 | 2013-06-20 | Rennovia, Inc. | Process for the separation of mono-and di-carboxylic acid compounds |
| CN104557705B (zh) * | 2013-10-15 | 2017-06-09 | 中国石油化工股份有限公司 | 一种己内酰胺精制的方法和装置 |
| BR112017005823B1 (pt) | 2014-09-29 | 2023-03-28 | Archer-Daniels-Midland Company | Processo para a preparação de um extrato |
| CA2966147A1 (en) | 2014-10-30 | 2016-05-06 | Toray Industries, Inc. | Method for producing .epsilon.-caprolactam |
| TW201718088A (zh) * | 2015-09-11 | 2017-06-01 | 東麗股份有限公司 | ε－己內醯胺之製造方法 |
| JP7125674B2 (ja) * | 2016-12-06 | 2022-08-25 | 東レ株式会社 | ε－カプロラクタムの製造方法 |
| KR102739203B1 (ko) * | 2018-08-28 | 2024-12-05 | 현대자동차주식회사 | 바이오 나일론 원료의 중간체 물질인 아디프아마이드 제조방법 |
| CN114160120B (zh) * | 2021-12-24 | 2024-01-26 | 郑州中科新兴产业技术研究院 | 一种用于己二酸酯生产己二腈的催化剂的制备方法 |
Family Cites Families (35)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2351939A (en) * | 1944-06-20 | Method of producing lactams | ||
| GB778253A (en) * | 1955-02-02 | 1957-07-03 | Inventa Ag | Process for the manufacture of -e-caprolactam |
| US3652549A (en) * | 1968-07-18 | 1972-03-28 | Kanegafuchi Spinning Co Ltd | Production of epsilon-caprolactam |
| JPS4919250B1 (enExample) * | 1969-01-09 | 1974-05-16 | ||
| JPS4919250A (enExample) * | 1972-06-16 | 1974-02-20 | ||
| US4042490A (en) * | 1973-12-26 | 1977-08-16 | Texaco Inc. | Hydrocarbon upgrading process |
| US4800227A (en) | 1984-08-20 | 1989-01-24 | Phillips Petroleum Company | Process for the production of lactams |
| IT1214622B (it) | 1985-07-10 | 1990-01-18 | Montedipe Spa | Processo catalitico per laproduzione di cicloesanonossima. |
| US5717089A (en) * | 1995-03-01 | 1998-02-10 | Dsm N.V. | Process for the preparation of E-caprolactam |
| DE19548289A1 (de) * | 1995-12-22 | 1997-06-26 | Basf Ag | Verfahren zur gleichzeitigen Herstellung von Caprolactam und Hexamethylendiamin |
| US5780623A (en) * | 1996-02-23 | 1998-07-14 | Dsm N.V. | Process to prepare ε-caprolactam from 6-aminocaproic acid |
| US5977356A (en) * | 1997-07-02 | 1999-11-02 | Industrial Technology Research Institute | Process for preparing caprolactam |
| EP0984002A1 (en) * | 1998-09-03 | 2000-03-08 | Dsm N.V. | Process to continuously prepare an aqueous mixture of epsilon-caprolactam and epsilon-caprolactam precursors |
| DE19842900A1 (de) * | 1998-09-18 | 2000-03-23 | Basf Ag | Verfahren zur gemeinsamen Herstellung eines cyclischen Lactams und eines cyclischen Amins |
| FR2785608B1 (fr) | 1998-11-05 | 2000-12-29 | Rhone Poulenc Fibres | Procede d'hemihydrogenation de dinitriles |
| JP2000229939A (ja) | 1999-02-09 | 2000-08-22 | Sumitomo Chem Co Ltd | ε−カプロラクタムの製造方法 |
| US6300496B1 (en) * | 1999-10-06 | 2001-10-09 | Union Carbide Chemicals & Plastics Technology Corporation | Processes for producing epsilon caprolactams |
| US6414179B1 (en) * | 2000-02-18 | 2002-07-02 | Bristol-Myers Squibb Company | Alpha-and beta-substituted trifluoromethyl ketones as phospholipase inhibitors |
| DE10028950A1 (de) | 2000-06-16 | 2001-12-20 | Basf Ag | Verfahren zur Herstellung von Caprolactam |
| US6372939B1 (en) | 2000-11-16 | 2002-04-16 | E.I. Du Pont De Nemours And Company | Production of 6-aminocaproic acid |
| DE10103581A1 (de) | 2001-01-26 | 2002-08-01 | Degussa | Durch Ammoniumsalze oder substituierte Ammoniumsalze cokatalysiertes Verfahren zur Herstellung von Oximen |
| EP1741699B1 (en) | 2001-02-14 | 2011-01-26 | Asahi Kasei Kabushiki Kaisha | Method for producing E-caprolactam |
| EP1251122A1 (en) | 2001-04-17 | 2002-10-23 | Dsm N.V. | Process for the preparation of epsilon-Caprolactam |
| US6479620B1 (en) | 2001-06-01 | 2002-11-12 | E. I. Du Pont De Nemours And Company | Process for converting caprolactam to nylon 6 |
| GB0325384D0 (en) * | 2003-10-30 | 2003-12-03 | Davy Process Techn Ltd | Process |
| JP4946869B2 (ja) * | 2005-12-07 | 2012-06-06 | 宇部興産株式会社 | ラクタムの製法 |
| JP5061607B2 (ja) * | 2006-12-12 | 2012-10-31 | 東洋紡績株式会社 | ナイロン６樹脂の製造方法 |
| EP2148856B8 (en) * | 2007-02-20 | 2016-04-06 | Board of Trustees of Michigan State University | Catalytic deamination for caprolactam production |
| US8669397B2 (en) | 2009-06-13 | 2014-03-11 | Rennovia, Inc. | Production of adipic acid and derivatives from carbohydrate-containing materials |
| BRPI1010708B1 (pt) * | 2009-06-13 | 2018-04-03 | Rennovia, Inc. | "processos para preparar um produto de ácido adípico, e ácido adípico ou derivado do mesmo" |
| WO2011109051A1 (en) * | 2010-03-05 | 2011-09-09 | Rennovia, Inc. | Adipic acid composition |
| WO2013090031A2 (en) | 2011-12-14 | 2013-06-20 | Rennovia, Inc. | Water concentration reduction process |
| WO2013090032A1 (en) | 2011-12-14 | 2013-06-20 | Rennovia, Inc. | Process for the separation of mono-and di-carboxylic acid compounds |
| CN104582847B (zh) | 2012-05-15 | 2018-08-31 | 阿彻丹尼尔斯米德兰德公司 | 还原催化剂 |
| KR20150018877A (ko) | 2012-06-11 | 2015-02-24 | 레노비아 인코포레이티드 | 1,6-헥산디올로부터 아디프산의 제조방법 |
-
2013
- 2013-02-13 WO PCT/US2013/025846 patent/WO2013126250A1/en not_active Ceased
- 2013-02-13 CN CN201380009620.5A patent/CN104169259B/zh active Active
- 2013-02-13 EP EP13705896.2A patent/EP2817293A1/en not_active Withdrawn
- 2013-02-13 BR BR112014020642-2A patent/BR112014020642B1/pt active IP Right Grant
- 2013-02-13 IN IN7028DEN2014 patent/IN2014DN07028A/en unknown
- 2013-02-13 AR ARP130100441A patent/AR089980A1/es unknown
- 2013-02-13 JP JP2014558764A patent/JP2015517977A/ja active Pending
- 2013-02-13 KR KR1020147024515A patent/KR20140129076A/ko not_active Withdrawn
- 2013-02-13 SG SG11201405045YA patent/SG11201405045YA/en unknown
- 2013-02-13 US US13/766,705 patent/US8946411B2/en active Active
- 2013-02-13 HK HK15105859.2A patent/HK1205121A1/xx unknown
- 2013-02-13 SA SA113340296A patent/SA113340296B1/ar unknown
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