JP2015506332A5 - - Google Patents
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- Publication number
- JP2015506332A5 JP2015506332A5 JP2014556024A JP2014556024A JP2015506332A5 JP 2015506332 A5 JP2015506332 A5 JP 2015506332A5 JP 2014556024 A JP2014556024 A JP 2014556024A JP 2014556024 A JP2014556024 A JP 2014556024A JP 2015506332 A5 JP2015506332 A5 JP 2015506332A5
- Authority
- JP
- Japan
- Prior art keywords
- zeolite
- mww
- boron
- zeolitic material
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000010457 zeolite Substances 0.000 claims 40
- 229910021536 Zeolite Inorganic materials 0.000 claims 36
- 238000000034 method Methods 0.000 claims 25
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims 15
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims 14
- 229910052796 boron Inorganic materials 0.000 claims 14
- 239000000463 material Substances 0.000 claims 14
- 239000007788 liquid Substances 0.000 claims 10
- 239000002904 solvent Substances 0.000 claims 10
- 238000010502 deborylation reaction Methods 0.000 claims 6
- 239000000203 mixture Substances 0.000 claims 5
- 239000002243 precursor Substances 0.000 claims 5
- 239000003054 catalyst Substances 0.000 claims 4
- 239000012452 mother liquor Substances 0.000 claims 4
- 239000007921 spray Substances 0.000 claims 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims 3
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims 3
- 239000012190 activator Substances 0.000 claims 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims 2
- NQRYJNQNLNOLGT-UHFFFAOYSA-N Piperidine Chemical compound C1CCNCC1 NQRYJNQNLNOLGT-UHFFFAOYSA-N 0.000 claims 2
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical group [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims 2
- 230000015572 biosynthetic process Effects 0.000 claims 2
- 238000001354 calcination Methods 0.000 claims 2
- 150000001875 compounds Chemical class 0.000 claims 2
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 claims 2
- 238000001035 drying Methods 0.000 claims 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 claims 2
- 150000007522 mineralic acids Chemical class 0.000 claims 2
- 150000007524 organic acids Chemical class 0.000 claims 2
- 239000000843 powder Substances 0.000 claims 2
- YPFDHNVEDLHUCE-UHFFFAOYSA-N propane-1,3-diol Chemical compound OCCCO YPFDHNVEDLHUCE-UHFFFAOYSA-N 0.000 claims 2
- 150000003839 salts Chemical class 0.000 claims 2
- 229910052710 silicon Inorganic materials 0.000 claims 2
- 239000010703 silicon Substances 0.000 claims 2
- 238000003786 synthesis reaction Methods 0.000 claims 2
- 230000002194 synthesizing effect Effects 0.000 claims 2
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 claims 1
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims 1
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims 1
- 239000004146 Propane-1,2-diol Substances 0.000 claims 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims 1
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims 1
- 235000011054 acetic acid Nutrition 0.000 claims 1
- 150000001298 alcohols Chemical class 0.000 claims 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims 1
- ZSIQJIWKELUFRJ-UHFFFAOYSA-N azepane Chemical compound C1CCCNCC1 ZSIQJIWKELUFRJ-UHFFFAOYSA-N 0.000 claims 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims 1
- 239000004327 boric acid Substances 0.000 claims 1
- 239000008119 colloidal silica Substances 0.000 claims 1
- 235000019253 formic acid Nutrition 0.000 claims 1
- 229960005150 glycerol Drugs 0.000 claims 1
- 235000011187 glycerol Nutrition 0.000 claims 1
- 239000008187 granular material Substances 0.000 claims 1
- 238000005469 granulation Methods 0.000 claims 1
- 230000003179 granulation Effects 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 229910017604 nitric acid Inorganic materials 0.000 claims 1
- 235000005985 organic acids Nutrition 0.000 claims 1
- 235000006408 oxalic acid Nutrition 0.000 claims 1
- 235000011007 phosphoric acid Nutrition 0.000 claims 1
- 238000012805 post-processing Methods 0.000 claims 1
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims 1
- 235000019260 propionic acid Nutrition 0.000 claims 1
- 229960004063 propylene glycol Drugs 0.000 claims 1
- 235000013772 propylene glycol Nutrition 0.000 claims 1
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 claims 1
- 238000010992 reflux Methods 0.000 claims 1
- 238000001694 spray drying Methods 0.000 claims 1
- 150000005846 sugar alcohols Polymers 0.000 claims 1
- 239000011975 tartaric acid Substances 0.000 claims 1
- 235000002906 tartaric acid Nutrition 0.000 claims 1
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP12154169.2 | 2012-02-07 | ||
| EP12154169 | 2012-02-07 | ||
| EP12189035 | 2012-10-18 | ||
| EP12189035.4 | 2012-10-18 | ||
| PCT/EP2013/052224 WO2013117537A1 (en) | 2012-02-07 | 2013-02-05 | Process for the preparation of a zeolitic material |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2015506332A JP2015506332A (ja) | 2015-03-02 |
| JP2015506332A5 true JP2015506332A5 (enExample) | 2016-03-24 |
| JP6367118B2 JP6367118B2 (ja) | 2018-08-01 |
Family
ID=47631451
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2014556024A Active JP6367118B2 (ja) | 2012-02-07 | 2013-02-05 | ゼオライト材料の製造方法 |
Country Status (13)
| Country | Link |
|---|---|
| EP (2) | EP2812282B1 (enExample) |
| JP (1) | JP6367118B2 (enExample) |
| KR (2) | KR102229855B1 (enExample) |
| CN (2) | CN108264053A (enExample) |
| BR (1) | BR112014019483B1 (enExample) |
| ES (2) | ES2683376T3 (enExample) |
| HU (1) | HUE060651T2 (enExample) |
| MX (1) | MX365892B (enExample) |
| MY (2) | MY195237A (enExample) |
| RU (1) | RU2619685C2 (enExample) |
| SG (2) | SG10201606435XA (enExample) |
| WO (1) | WO2013117537A1 (enExample) |
| ZA (1) | ZA201406464B (enExample) |
Families Citing this family (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| MX361540B (es) * | 2012-11-05 | 2018-12-10 | Basf Se | Un material zeolítico que contiene estaño que tiene una estructura de marco de tipo mww. |
| US9371239B2 (en) * | 2012-11-05 | 2016-06-21 | Basf Se | Tin-containing zeolitic material having an MWW-type framework structure |
| EP3066051B1 (en) | 2013-11-05 | 2022-01-05 | Basf Se | A tin-containing zeolitic material having a bea framework structure |
| JP6526689B2 (ja) * | 2013-11-05 | 2019-06-05 | ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ | Ｍｗｗ型の骨格構造を有するスズ含有のゼオライト材料 |
| CN104709919B (zh) * | 2013-12-16 | 2017-03-08 | 中国科学院大连化学物理研究所 | 一种具有mww拓扑结构的含锡分子筛及其制备和应用 |
| DE102014008081A1 (de) | 2014-05-30 | 2015-11-19 | Basf Se | Verfahren zur Herstellung von Acrylsäure unter Verwendung eines alkali- und erdalkalifreien zeolithischen Materials |
| DE102014008080A1 (de) | 2014-05-30 | 2015-11-12 | Basf Se | Verfahren zur Herstellung von Acrylsäure unter Verwendung eines aluminiumfreien zeolithischen Materials |
| DE102014017804A1 (de) | 2014-12-02 | 2016-04-21 | Basf Se | Verfahren zur Herstellung von Acrylsäure |
| US10202323B2 (en) | 2015-07-15 | 2019-02-12 | Basf Se | Process for preparing an arylpropene |
| CN107848929A (zh) | 2015-07-15 | 2018-03-27 | 巴斯夫欧洲公司 | 制备芳基丙烯的方法 |
| ES2899827T3 (es) * | 2015-12-08 | 2022-03-14 | Basf Se | Material zeolítico que contiene estaño y que tiene una estructura de marco BEA |
| EP3554694B1 (en) * | 2016-12-13 | 2024-02-14 | Basf Se | A process for the preparation of a titanium-containing zeolite |
| EP3558516A1 (en) * | 2016-12-20 | 2019-10-30 | Basf Se | A process for preparing an extrudable composition comprising a titanium-containing zeolitic material having framework type mww |
| KR102500933B1 (ko) * | 2017-01-18 | 2023-02-16 | 바스프 에스이 | 아연, 및 티타늄 함유 제올라이트를 포함하는 몰딩의 제조 방법 |
| CN108398422B (zh) * | 2018-01-30 | 2019-12-10 | 北京联合大学 | 同时测定空气中硫化氢、苯和三甲胺的敏感材料 |
| KR20200118129A (ko) * | 2018-02-06 | 2020-10-14 | 바스프 에스이 | Rth 골격 구조 유형을 갖는 제올라이트 물질의 제조 방법 |
| FR3081345B1 (fr) * | 2018-05-24 | 2023-11-10 | Ifp Energies Now | Procede de synthese d'une zeolithe de type structural afx de tres haute purete en presence d'un structurant organique azote |
| US20220403207A1 (en) | 2019-10-24 | 2022-12-22 | Basf Se | Removal of monomeric aliphatic diisocyanate in an aliphatic polyisocyanate using scavengers |
| CN110668463B (zh) * | 2019-11-06 | 2021-04-02 | 中国天辰工程有限公司 | 一种含钛高硅铝比丝光沸石的制备方法 |
| WO2021191135A1 (en) | 2020-03-23 | 2021-09-30 | Basf Se | Zeolitic material having a framework structure comprising si, o, and ti |
| WO2022029076A1 (en) | 2020-08-03 | 2022-02-10 | Basf Se | A polyester molding having a low outgassing of volatile organic compounds |
| CN114180594B (zh) * | 2020-09-14 | 2023-05-02 | 中国石油化工股份有限公司 | 一种ith分子筛的制备方法 |
| KR102408100B1 (ko) * | 2021-05-31 | 2022-06-15 | 충북대학교 산학협력단 | 메탄의 건식 개질 반응용 2차원 니켈 실리케이트 분자체 촉매의 제조방법 및 이에 따라 제조된 메탄의 건식 개질 반응용 2차원 니켈 실리케이트 분자체 촉매 |
| KR102773001B1 (ko) * | 2023-07-27 | 2025-02-27 | 동우 화인켐 주식회사 | 유기용매 정제 방법 및 탈수 시스템 |
Family Cites Families (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NZ201113A (en) * | 1981-06-30 | 1985-08-16 | Standard Oil Co | A method of preparing an ams-1b crystalline borosilicate molecular sieve |
| US5053211A (en) * | 1981-06-30 | 1991-10-01 | Amoco Corporation | Manufacture of AMS-18 crystalline borosilicate molecular sieve |
| US4526880A (en) * | 1984-07-16 | 1985-07-02 | Mobil Oil Corporation | Hydrothermal zeolite activation |
| US5047141A (en) * | 1984-07-16 | 1991-09-10 | Mobil Oil Corporation | Larger pore molecular sieves of controlled activity |
| NZ212649A (en) * | 1984-07-16 | 1988-06-30 | Mobil Oil Corp | Method for increasing zeolite catalytic activity |
| US4721607A (en) * | 1986-01-31 | 1988-01-26 | Amoco Corporation | Process for the production of boronaaronate molecular sieve using ethylenediamine and quinoline or isoquinoline |
| CA1276611C (en) * | 1986-02-14 | 1990-11-20 | Pochen Chu | Controlling the catalytic activity of zeolites |
| US4954325A (en) | 1986-07-29 | 1990-09-04 | Mobil Oil Corp. | Composition of synthetic porous crystalline material, its synthesis and use |
| US5324702A (en) * | 1991-11-22 | 1994-06-28 | Amoco Corporation | Catalytic oxidation and oxidative dehydrogenation using metal-compound-loaded, deboronated hams-1b crystalline borosilicate molecular sieve compositions |
| DE19828851A1 (de) * | 1998-06-27 | 2000-02-03 | Hoelderich W F | Poröses kristallines Molybdänsilikat, dessen Herstellung und dessen Verwendung in die Oxidationskatalyse |
| JP2000103613A (ja) * | 1998-09-28 | 2000-04-11 | Japan Chemical Innovation Institute | ホウ素含有ゼオライトの合成方法 |
| US6468501B1 (en) * | 2000-09-14 | 2002-10-22 | Chevrontexaco Corporation | Method for heteroatom lattice substitution in large and extra-large pore borosilicate zeolites |
| JP2002102709A (ja) | 2000-09-29 | 2002-04-09 | Showa Denko Kk | 酸化化合物製造用結晶性ｍｗｗ型チタノシリケート触媒、該触媒の製造方法、及び該触媒を用いた酸化化合物の製造方法 |
| AU2002248274A1 (en) | 2000-12-22 | 2002-07-30 | California Institute Of Technology | Synthesis of molecular sieves by hydrothermal treatment with acid |
| JP4270901B2 (ja) * | 2002-03-07 | 2009-06-03 | 昭和電工株式会社 | チタノシリケート、その製造方法およびチタノシリケートを用いた酸化化合物の製造方法 |
| JP4241068B2 (ja) * | 2002-03-07 | 2009-03-18 | 昭和電工株式会社 | Ｍｗｗ型ゼオライト物質の製造方法 |
| JP2004217449A (ja) * | 2003-01-10 | 2004-08-05 | Tosoh Corp | 高流動性ゼオライト顆粒及びその製造方法 |
| BRPI0407183B8 (pt) * | 2003-02-03 | 2016-05-17 | Showa Denko Kk | processo para produzir um material de metalossilicato em camadas modificado, bem como material de metalossilicato em camadas modificado obtido pelo dito processo |
| US7211239B2 (en) * | 2005-04-22 | 2007-05-01 | Basf Aktiengesellschaft | Process for preparing a nanosized zeolitic material |
| EP2297036B1 (en) * | 2008-05-21 | 2014-04-16 | Basf Se | Process for the direct synthesis of cu containing zeolites having cha structure |
| DE102008057134A1 (de) * | 2008-11-13 | 2010-05-27 | Süd-Chemie AG | Metallhaltige kristalline Silikate |
| US8124555B2 (en) * | 2010-02-01 | 2012-02-28 | Lyondell Chemical Technology L.P. | Process for making titanium-MWW zeolite |
| US20110201860A1 (en) * | 2010-02-18 | 2011-08-18 | Muhammad Naseem Akhtar | Process for conversion of alkanes to aromatics |
| US20110313226A1 (en) * | 2010-06-18 | 2011-12-22 | Tokyo Institute Of Technology | Zeolitic Materials of the LEV-Type Structure And Methods For Their Production |
-
2013
- 2013-02-05 SG SG10201606435XA patent/SG10201606435XA/en unknown
- 2013-02-05 MY MYPI2018002179A patent/MY195237A/en unknown
- 2013-02-05 ES ES13702241.4T patent/ES2683376T3/es active Active
- 2013-02-05 ES ES17205602T patent/ES2935820T3/es active Active
- 2013-02-05 CN CN201810159217.5A patent/CN108264053A/zh active Pending
- 2013-02-05 CN CN201380018886.6A patent/CN104302577A/zh active Pending
- 2013-02-05 BR BR112014019483-1A patent/BR112014019483B1/pt active IP Right Grant
- 2013-02-05 MX MX2014009271A patent/MX365892B/es active IP Right Grant
- 2013-02-05 RU RU2014136174A patent/RU2619685C2/ru active
- 2013-02-05 MY MYPI2014002279A patent/MY169244A/en unknown
- 2013-02-05 EP EP13702241.4A patent/EP2812282B1/en active Active
- 2013-02-05 WO PCT/EP2013/052224 patent/WO2013117537A1/en not_active Ceased
- 2013-02-05 HU HUE17205602A patent/HUE060651T2/hu unknown
- 2013-02-05 SG SG11201404651YA patent/SG11201404651YA/en unknown
- 2013-02-05 KR KR1020207003773A patent/KR102229855B1/ko active Active
- 2013-02-05 KR KR1020147025190A patent/KR102079792B1/ko active Active
- 2013-02-05 EP EP17205602.0A patent/EP3326973B1/en active Active
- 2013-02-05 JP JP2014556024A patent/JP6367118B2/ja active Active
-
2014
- 2014-09-04 ZA ZA2014/06464A patent/ZA201406464B/en unknown
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