JP2015502309A5 - - Google Patents
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- Publication number
- JP2015502309A5 JP2015502309A5 JP2014535715A JP2014535715A JP2015502309A5 JP 2015502309 A5 JP2015502309 A5 JP 2015502309A5 JP 2014535715 A JP2014535715 A JP 2014535715A JP 2014535715 A JP2014535715 A JP 2014535715A JP 2015502309 A5 JP2015502309 A5 JP 2015502309A5
- Authority
- JP
- Japan
- Prior art keywords
- metal oxide
- zro
- zirconia sol
- airgel
- crystals
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000013078 crystal Substances 0.000 claims 13
- 229910044991 metal oxide Inorganic materials 0.000 claims 13
- 150000004706 metal oxides Chemical class 0.000 claims 13
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims 11
- 239000002245 particle Substances 0.000 claims 7
- 238000000034 method Methods 0.000 claims 3
- 239000003999 initiator Substances 0.000 claims 2
- 239000011368 organic material Substances 0.000 claims 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 1
- 125000003158 alcohol group Chemical group 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 239000003607 modifier Substances 0.000 claims 1
- 239000011148 porous material Substances 0.000 claims 1
- 239000011164 primary particle Substances 0.000 claims 1
- 238000000194 supercritical-fluid extraction Methods 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201161545243P | 2011-10-10 | 2011-10-10 | |
| US61/545,243 | 2011-10-10 | ||
| PCT/US2012/049505 WO2013055432A1 (en) | 2011-10-10 | 2012-08-03 | Aerogels, calcined and crystalline articles and methods of making the same |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2015502309A JP2015502309A (ja) | 2015-01-22 |
| JP2015502309A5 true JP2015502309A5 (https=) | 2015-08-27 |
| JP6181655B2 JP6181655B2 (ja) | 2017-08-16 |
Family
ID=46924515
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2014535715A Active JP6181655B2 (ja) | 2011-10-10 | 2012-08-03 | エアロゲル、焼成及び結晶質製品及びその製造法 |
Country Status (7)
| Country | Link |
|---|---|
| US (3) | US9657152B2 (https=) |
| EP (2) | EP2766304B1 (https=) |
| JP (1) | JP6181655B2 (https=) |
| CN (1) | CN103857625B (https=) |
| BR (1) | BR112014008606A2 (https=) |
| RU (1) | RU2571151C2 (https=) |
| WO (1) | WO2013055432A1 (https=) |
Families Citing this family (52)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2571151C2 (ru) | 2011-10-10 | 2015-12-20 | 3М Инновейтив Пропертиз Компани | Аэрогели, кальцинированные изделия, изделия с кристаллической структурой и способы их получения |
| WO2013070451A1 (en) | 2011-11-07 | 2013-05-16 | 3M Innovative Properties Company | Whitening composition for selectively treating the surface of dental ceramic and related methods |
| US8936848B2 (en) | 2012-02-23 | 2015-01-20 | B&D Dental Corp | Non-pre-colored multi-layer zirconia dental blank that has a gradual change in translucency through a thickness after sintering |
| EP2692311B1 (en) * | 2012-08-03 | 2016-06-22 | 3M Innovative Properties Company | Dental blank comprising a pre-sintered porous zirconia material , process of its production and dental article formed from said dental blank |
| CN104918900B (zh) * | 2012-09-20 | 2020-03-17 | 3M创新有限公司 | 氧化锆陶瓷的着色 |
| EP2909029A1 (en) * | 2012-10-17 | 2015-08-26 | 3M Innovative Properties Company | Multi sectional dental zirconia milling block, process of production and use thereof |
| WO2014093329A1 (en) | 2012-12-12 | 2014-06-19 | 3M Innovative Properties Company | Whitening composition for treating the surface of dental ceramic and related methods |
| US10004668B2 (en) | 2013-06-27 | 2018-06-26 | Ivoclar Vivadent, Inc. | Nanocrystalline zirconia and methods of processing thereof |
| US9878954B2 (en) | 2013-09-13 | 2018-01-30 | 3M Innovative Properties Company | Vacuum glazing pillars for insulated glass units |
| TWI565681B (zh) * | 2013-10-15 | 2017-01-11 | 中原大學 | 多孔二氧化矽氣凝膠複合薄膜及其製造方法以及二氧化碳吸收裝置 |
| RU2698021C1 (ru) * | 2013-12-04 | 2019-08-21 | 3М Инновейтив Пропертиз Компани | Стоматологическая заготовка для фрезерования, способ ее изготовления и использования |
| US10350032B2 (en) | 2014-03-25 | 2019-07-16 | 3M Innovative Properties Company | Process for selectively treating the surface of dental ceramic |
| US10273191B2 (en) * | 2015-01-15 | 2019-04-30 | Tosoh Corporation | Translucent zirconia sintered body, method for manufacturing same, and use thereof |
| EP3265436A1 (en) * | 2015-03-03 | 2018-01-10 | 3M Innovative Properties Company | Gel compositions, shaped gel articles and a method of making a sintered article |
| JP6513793B2 (ja) * | 2015-04-09 | 2019-05-15 | 株式会社オーラル28 | プラズマ照射装置及びプラズマ照射方法 |
| DE102015207944A1 (de) * | 2015-04-29 | 2016-11-03 | Wacker Chemie Ag | Verfahren zur Herstellung organisch modifizierter Aerogele |
| CN107635945B (zh) * | 2015-05-28 | 2021-04-30 | 3M创新有限公司 | 使用包含纳米级颗粒的溶胶制作陶瓷制品的增材制造方法 |
| US11339095B2 (en) | 2015-05-28 | 2022-05-24 | 3M Innovative Properties Company | Sol containing nano zirconia particles for use in additive manufacturing processes for the production of 3-dimensional articles |
| EP3178462A1 (de) | 2015-12-07 | 2017-06-14 | WDT-Wolz-Dental-Technik GmbH | Verfahren zur herstellung eines polychrom und/oder räumlich polychrom oder eines monochrom gefärbten keramischen körpers und vorrichtung hierfür |
| KR101776738B1 (ko) * | 2015-12-15 | 2017-09-08 | 현대자동차 주식회사 | 다공성 세라믹 복합입자 및 그 제조방법 |
| DE102015122864A1 (de) | 2015-12-28 | 2017-06-29 | Degudent Gmbh | Verfahren zur Herstellung eines Rohlings sowie dentale Restauration |
| DE102016106370A1 (de) | 2016-03-23 | 2017-09-28 | Degudent Gmbh | Verfahren zur Herstellung eines eingefärbten Rohlings sowie Rohling |
| US9822039B1 (en) | 2016-08-18 | 2017-11-21 | Ivoclar Vivadent Ag | Metal oxide ceramic nanomaterials and methods of making and using same |
| EP3507011B1 (en) * | 2016-09-02 | 2024-06-26 | 3M Innovative Properties Company | Shaped gel articles and sintered articles prepared therefrom |
| DK201600605A1 (en) * | 2016-10-07 | 2018-04-16 | Haldor Topsoe As | Combustion Chamber Hot Face Refractory Lining |
| EP3318218B1 (en) * | 2016-11-07 | 2019-09-11 | Shofu Inc. | Dental zirconia blank having high relative density |
| JP6962657B2 (ja) | 2016-11-07 | 2021-11-05 | 株式会社松風 | 高い相対密度を有する多層の歯科用ジルコニアブランク |
| WO2018101923A1 (en) * | 2016-11-30 | 2018-06-07 | Carestream Dental Technology Topco Limited | Method and system for braces removal from dentition mesh |
| EP3583083B1 (en) * | 2017-02-15 | 2021-11-03 | 3M Innovative Properties Company | Zirconia article with high alumina content, process of production and use thereof |
| JP2020513049A (ja) * | 2017-04-13 | 2020-04-30 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | 多孔質材料を製造する方法 |
| WO2019075274A1 (en) * | 2017-10-11 | 2019-04-18 | University Of Utah Research Foundation | METHODS OF MANUFACTURING PERMEABLE AEROGELS |
| RU2675391C1 (ru) * | 2017-11-03 | 2018-12-19 | Федеральное государственное бюджетное учреждение науки Институт металлургии и материаловедения им. А.А. Байкова Российской академии наук (ИМЕТ РАН) | Керамический материал с низкой температурой спекания на основе диоксида циркония тетрагональной модификации |
| JP7326300B2 (ja) | 2018-02-02 | 2023-08-15 | スリーエム イノベイティブ プロパティズ カンパニー | 高い唇側引張強度を有するセラミック自己結紮式ブラケット |
| CN108721205B (zh) * | 2018-07-16 | 2021-07-23 | 浙江工业大学 | 一种缓释多层牙用植入剂及其制备方法和评价方法 |
| CN109160533B (zh) * | 2018-10-25 | 2021-04-20 | 南京工业大学 | 一种块状SrTiO3气凝胶的制备方法 |
| US10995191B2 (en) | 2018-12-20 | 2021-05-04 | Palo Alto Research Center Incoporated | High optical transparency polymer aerogels using low refractive index monomers |
| JP7579058B2 (ja) * | 2019-01-21 | 2024-11-07 | 株式会社松風 | 高速焼結対応高透過ジルコニアブランク |
| US12233599B2 (en) | 2019-03-29 | 2025-02-25 | Solventum Intellectual Properties Company | Build platform for use in an additive manufacturing device |
| WO2021024162A1 (en) | 2019-08-06 | 2021-02-11 | 3M Innovative Properties Company | Continuous additive manufacturing method for making ceramic articles, and ceramic articles |
| FR3103190B1 (fr) * | 2019-11-14 | 2021-12-03 | Saint Gobain Ct Recherches | Article dentaire, poudre pour article dentaire et procede de fabrication d’un tel article |
| US12468138B2 (en) | 2019-12-05 | 2025-11-11 | 3M Innovative Properties Company | Multiphoton imaging methods in a scattering and/or absorbing medium, and articles |
| US11731312B2 (en) | 2020-01-29 | 2023-08-22 | James R. Glidewell Dental Ceramics, Inc. | Casting apparatus, cast zirconia ceramic bodies and methods for making the same |
| RU2744546C1 (ru) * | 2020-08-06 | 2021-03-11 | Федеральное государственное бюджетное учреждение науки Институт металлургии и материаловедения им. А.А. Байкова Российской академии наук (ИМЕТ РАН) | Керамический материал и способ его получения |
| CN112588250B (zh) * | 2020-11-04 | 2022-03-25 | 四川大学 | 一种利用硫酸钛液生产双效晶种的管壳式晶种设备及制造方法 |
| CN112320833B (zh) * | 2020-11-06 | 2022-08-02 | 湖南荣岚智能科技有限公司 | 耐高温SiO2-Gd2O3复合气凝胶及其制备方法 |
| WO2022136969A1 (en) | 2020-12-23 | 2022-06-30 | 3M Innovative Properties Company | Methods of making articles including inkjet printing sols containing metal oxide nanoparticles |
| TWI747694B (zh) | 2020-12-31 | 2021-11-21 | 遠東科技大學 | 以水系膠鑄成型製作氧化鋯陶瓷之方法 |
| KR20240156393A (ko) | 2022-02-28 | 2024-10-29 | 도소 가부시키가이샤 | 소결체, 소결체의 제조 방법, 분말 및 하소체 |
| CN114853470B (zh) * | 2022-05-30 | 2022-12-09 | 天津城建大学 | 一种增强隔热二氧化锆复合陶瓷气凝胶及其制备方法 |
| EP4673082A1 (en) | 2023-03-01 | 2026-01-07 | Solventum Intellectual Properties Company | Ceramic veneers and continuous additive manufacturing method for making ceramic veneers |
| CN116474735A (zh) * | 2023-04-26 | 2023-07-25 | 陕西科技大学 | 一种高吸附和光热蒸发的纤维素基气凝胶及其制备方法 |
| CN121285362A (zh) | 2023-05-10 | 2026-01-06 | 舒万诺知识产权公司 | 用于生产氧化锆牙科制品的方法 |
Family Cites Families (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5453262A (en) | 1988-12-09 | 1995-09-26 | Battelle Memorial Institute | Continuous process for production of ceramic powders with controlled morphology |
| JPH0679965B2 (ja) * | 1991-04-12 | 1994-10-12 | 株式会社コロイドリサーチ | ジルコニアゾルの製造方法およびジルコニア成形体の製造方法 |
| US5652192A (en) | 1992-07-10 | 1997-07-29 | Battelle Memorial Institute | Catalyst material and method of making |
| DE4430642A1 (de) | 1994-08-29 | 1996-03-07 | Hoechst Ag | Aerogel- und Xerogelverbundstoffe, Verfahren zu ihrer Herstellung sowie ihre Verwendung |
| DE19506141A1 (de) * | 1995-02-22 | 1996-08-29 | Hoechst Ag | Verwendung von Aerogelen in der Pharmazie, in der Kosmetik und im Pflanzenschutz |
| US5989698A (en) | 1997-02-10 | 1999-11-23 | 3M Innovative Properties Company | Coated porous materials |
| JP2003192452A (ja) * | 2001-10-16 | 2003-07-09 | Toray Ind Inc | ジルコニア粉末およびその焼結体 |
| US20100140154A1 (en) | 2004-03-09 | 2010-06-10 | The Research Foundation Of State University Of New York | Group iv metal oxide monolithic columns |
| US7241437B2 (en) * | 2004-12-30 | 2007-07-10 | 3M Innovative Properties Company | Zirconia particles |
| WO2006135882A2 (en) * | 2005-06-11 | 2006-12-21 | Aspen Aerogels Inc. | Microporous polyisocyanate based hybrid materials |
| US20090047562A1 (en) | 2005-07-27 | 2009-02-19 | Kazuo Hata | Method for Producing Solid Electrolyte Sheet and Solid Electrolyte Sheet |
| US8785008B2 (en) * | 2006-07-25 | 2014-07-22 | Tosoh Corporation | Zirconia sintered bodies with high total light transmission and high strength, uses of the same, and process for producing the same |
| EP2104654A2 (en) | 2006-12-29 | 2009-09-30 | 3M Innovative Properties Company | Zirconia body and methods |
| JP5018142B2 (ja) | 2007-03-07 | 2012-09-05 | 東ソー株式会社 | 透光性ジルコニア焼結体及びその製造方法 |
| US8734931B2 (en) | 2007-07-23 | 2014-05-27 | 3M Innovative Properties Company | Aerogel composites |
| EP2620413B1 (en) | 2007-12-28 | 2020-07-01 | 3M Innovative Properties Company | Continuous hydrothermal reactor system comprising a fluorinated polymer tubular reactor |
| CN101456569B (zh) * | 2008-07-22 | 2012-09-12 | 绍兴纳诺气凝胶新材料研发中心有限公司 | 一种水热合成低成本快速制备气凝胶的方法 |
| CN102224106A (zh) * | 2008-10-15 | 2011-10-19 | 3M创新有限公司 | 具有氧化锆和二氧化硅纳米粒子的填料和复合材料 |
| US8598058B2 (en) | 2009-12-29 | 2013-12-03 | 3M Innovative Properties Company | Zirconia-based material doped with yttrium and lanthanum |
| WO2011082031A1 (en) | 2009-12-29 | 2011-07-07 | 3M Innovative Properties Company | Zirconia-based particles doped with a lanthanide element |
| RU2571151C2 (ru) | 2011-10-10 | 2015-12-20 | 3М Инновейтив Пропертиз Компани | Аэрогели, кальцинированные изделия, изделия с кристаллической структурой и способы их получения |
| US10004668B2 (en) | 2013-06-27 | 2018-06-26 | Ivoclar Vivadent, Inc. | Nanocrystalline zirconia and methods of processing thereof |
-
2012
- 2012-08-03 RU RU2014112777/05A patent/RU2571151C2/ru active
- 2012-08-03 EP EP12762691.9A patent/EP2766304B1/en active Active
- 2012-08-03 BR BR112014008606A patent/BR112014008606A2/pt not_active Application Discontinuation
- 2012-08-03 WO PCT/US2012/049505 patent/WO2013055432A1/en not_active Ceased
- 2012-08-03 EP EP17190809.8A patent/EP3284724B1/en active Active
- 2012-08-03 JP JP2014535715A patent/JP6181655B2/ja active Active
- 2012-08-03 US US14/347,382 patent/US9657152B2/en active Active
- 2012-08-03 CN CN201280049605.9A patent/CN103857625B/zh active Active
-
2017
- 2017-04-13 US US15/486,579 patent/US9925126B2/en active Active
-
2018
- 2018-02-13 US US15/895,459 patent/US10052266B2/en active Active
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