JP2015212411A5 - - Google Patents
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- Publication number
- JP2015212411A5 JP2015212411A5 JP2014167904A JP2014167904A JP2015212411A5 JP 2015212411 A5 JP2015212411 A5 JP 2015212411A5 JP 2014167904 A JP2014167904 A JP 2014167904A JP 2014167904 A JP2014167904 A JP 2014167904A JP 2015212411 A5 JP2015212411 A5 JP 2015212411A5
- Authority
- JP
- Japan
- Prior art keywords
- nickel
- nickel powder
- sulfur
- powder
- carbon
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 131
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 45
- 229910052717 sulfur Inorganic materials 0.000 claims description 45
- 239000011593 sulfur Substances 0.000 claims description 45
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 42
- 229910052799 carbon Inorganic materials 0.000 claims description 42
- 238000000034 method Methods 0.000 claims description 40
- 229910052759 nickel Inorganic materials 0.000 claims description 29
- 238000005406 washing Methods 0.000 claims description 28
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 27
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 25
- 238000004519 manufacturing process Methods 0.000 claims description 20
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 16
- 229910052739 hydrogen Inorganic materials 0.000 claims description 14
- 239000001257 hydrogen Substances 0.000 claims description 14
- 239000007788 liquid Substances 0.000 claims description 13
- 239000007789 gas Substances 0.000 claims description 8
- 150000002500 ions Chemical class 0.000 claims description 8
- 229910052757 nitrogen Inorganic materials 0.000 claims description 7
- LGQLOGILCSXPEA-UHFFFAOYSA-L nickel sulfate Chemical compound [Ni+2].[O-]S([O-])(=O)=O LGQLOGILCSXPEA-UHFFFAOYSA-L 0.000 claims description 6
- 229910000363 nickel(II) sulfate Inorganic materials 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 5
- 239000008139 complexing agent Substances 0.000 claims description 4
- 238000010668 complexation reaction Methods 0.000 claims description 3
- 239000000843 powder Substances 0.000 description 22
- 238000006722 reduction reaction Methods 0.000 description 21
- 239000000243 solution Substances 0.000 description 16
- 239000012535 impurity Substances 0.000 description 15
- 238000004140 cleaning Methods 0.000 description 13
- 239000002002 slurry Substances 0.000 description 10
- 230000000694 effects Effects 0.000 description 7
- 229910000480 nickel oxide Inorganic materials 0.000 description 6
- GNRSAWUEBMWBQH-UHFFFAOYSA-N oxonickel Chemical compound [Ni]=O GNRSAWUEBMWBQH-UHFFFAOYSA-N 0.000 description 6
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 5
- 229940053662 nickel sulfate Drugs 0.000 description 5
- 229910000863 Ferronickel Inorganic materials 0.000 description 4
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 4
- 229910001873 dinitrogen Inorganic materials 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 239000002994 raw material Substances 0.000 description 4
- 238000000926 separation method Methods 0.000 description 4
- WWNBZGLDODTKEM-UHFFFAOYSA-N sulfanylidenenickel Chemical compound [Ni]=S WWNBZGLDODTKEM-UHFFFAOYSA-N 0.000 description 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 230000000536 complexating effect Effects 0.000 description 3
- 239000013078 crystal Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 238000007664 blowing Methods 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 229910017052 cobalt Inorganic materials 0.000 description 2
- 239000010941 cobalt Substances 0.000 description 2
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 2
- 239000002270 dispersing agent Substances 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 150000002815 nickel Chemical class 0.000 description 2
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 2
- 238000000638 solvent extraction Methods 0.000 description 2
- 238000004506 ultrasonic cleaning Methods 0.000 description 2
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
- 239000004484 Briquette Substances 0.000 description 1
- 229910021586 Nickel(II) chloride Inorganic materials 0.000 description 1
- 238000003723 Smelting Methods 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 description 1
- 229910052921 ammonium sulfate Inorganic materials 0.000 description 1
- 235000011130 ammonium sulphate Nutrition 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- INPLXZPZQSLHBR-UHFFFAOYSA-N cobalt(2+);sulfide Chemical compound [S-2].[Co+2] INPLXZPZQSLHBR-UHFFFAOYSA-N 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- YDEXUEFDPVHGHE-GGMCWBHBSA-L disodium;(2r)-3-(2-hydroxy-3-methoxyphenyl)-2-[2-methoxy-4-(3-sulfonatopropyl)phenoxy]propane-1-sulfonate Chemical compound [Na+].[Na+].COC1=CC=CC(C[C@H](CS([O-])(=O)=O)OC=2C(=CC(CCCS([O-])(=O)=O)=CC=2)OC)=C1O YDEXUEFDPVHGHE-GGMCWBHBSA-L 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 230000033444 hydroxylation Effects 0.000 description 1
- 238000005805 hydroxylation reaction Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 229910052987 metal hydride Inorganic materials 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- QMMRZOWCJAIUJA-UHFFFAOYSA-L nickel dichloride Chemical compound Cl[Ni]Cl QMMRZOWCJAIUJA-UHFFFAOYSA-L 0.000 description 1
- -1 nickel metal hydride Chemical class 0.000 description 1
- RRIWRJBSCGCBID-UHFFFAOYSA-L nickel sulfate hexahydrate Chemical compound O.O.O.O.O.O.[Ni+2].[O-]S([O-])(=O)=O RRIWRJBSCGCBID-UHFFFAOYSA-L 0.000 description 1
- 229940116202 nickel sulfate hexahydrate Drugs 0.000 description 1
- BFDHFSHZJLFAMC-UHFFFAOYSA-L nickel(ii) hydroxide Chemical compound [OH-].[OH-].[Ni+2] BFDHFSHZJLFAMC-UHFFFAOYSA-L 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 239000007774 positive electrode material Substances 0.000 description 1
- 238000004663 powder metallurgy Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 150000004763 sulfides Chemical class 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Priority Applications (8)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2014167904A JP6406613B2 (ja) | 2014-04-15 | 2014-08-20 | 含有する炭素及び硫黄の濃度を低減するニッケル粉の製造方法 |
| CN201580016554.3A CN106163707B (zh) | 2014-04-15 | 2015-04-13 | 碳及硫的浓度低的镍粉的制造方法 |
| PCT/JP2015/061358 WO2015159846A1 (ja) | 2014-04-15 | 2015-04-13 | 炭素及び硫黄の濃度が低いニッケル粉の製造方法 |
| AU2015247017A AU2015247017B2 (en) | 2014-04-15 | 2015-04-13 | Method for Producing Nickel Powder for Reducing Carbon Concentration and Low Sulfur Concentration Contained in Nickel Powder |
| EP15779611.1A EP3132874B1 (en) | 2014-04-15 | 2015-04-13 | Method for producing nickel powder having low carbon concentration and low sulfur concentration |
| US15/303,557 US10500644B2 (en) | 2014-04-15 | 2015-04-13 | Method for producing nickel powder having low carbon concentration and low sulfur concentration |
| CA2945918A CA2945918C (en) | 2014-04-15 | 2015-04-13 | Method for producing nickel powder having low carbon concentration and low sulfur concentration |
| PH12016502049A PH12016502049A1 (en) | 2014-04-15 | 2016-10-14 | Method for producing nickel powder having low carbon concentration and low sulfur concentration |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2014083886 | 2014-04-15 | ||
| JP2014083886 | 2014-04-15 | ||
| JP2014167904A JP6406613B2 (ja) | 2014-04-15 | 2014-08-20 | 含有する炭素及び硫黄の濃度を低減するニッケル粉の製造方法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2015212411A JP2015212411A (ja) | 2015-11-26 |
| JP2015212411A5 true JP2015212411A5 (enExample) | 2017-08-10 |
| JP6406613B2 JP6406613B2 (ja) | 2018-10-17 |
Family
ID=54324052
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2014167904A Active JP6406613B2 (ja) | 2014-04-15 | 2014-08-20 | 含有する炭素及び硫黄の濃度を低減するニッケル粉の製造方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US10500644B2 (enExample) |
| EP (1) | EP3132874B1 (enExample) |
| JP (1) | JP6406613B2 (enExample) |
| CN (1) | CN106163707B (enExample) |
| AU (1) | AU2015247017B2 (enExample) |
| CA (1) | CA2945918C (enExample) |
| PH (1) | PH12016502049A1 (enExample) |
| WO (1) | WO2015159846A1 (enExample) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP6726396B2 (ja) * | 2016-02-22 | 2020-07-22 | 住友金属鉱山株式会社 | ニッケル粉の製造方法 |
| JP6245314B2 (ja) * | 2016-05-30 | 2017-12-13 | 住友金属鉱山株式会社 | ニッケル粉の製造方法 |
| JP6819087B2 (ja) * | 2016-06-21 | 2021-01-27 | 住友金属鉱山株式会社 | ニッケル粉の製造方法、ニッケル粉の製造装置 |
| CN107746951A (zh) * | 2017-09-26 | 2018-03-02 | 北京矿冶研究总院 | 一种硫酸盐溶液中镍的分离方法 |
| EP3702330A4 (en) * | 2017-10-26 | 2020-12-23 | Sumitomo Metal Mining Co., Ltd. | COMPOSITE NICKEL OXIDE AND PROCESS FOR THE PRODUCTION OF LITHIUM-NICKEL COMPOSITE OXIDE |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2734821A (en) * | 1956-02-14 | Table ix | ||
| CA970168A (en) * | 1972-10-20 | 1975-07-01 | Vladimir N. Mackiw | Production of nickel powder from impure nickel compounds |
| CA988306A (en) | 1973-04-09 | 1976-05-04 | International Nickel Company Of Canada | Reduction of nickel oxide |
| CN86100739B (zh) * | 1986-01-07 | 1988-06-08 | 中国科学院化工冶金研究所 | 制备超细镍粉的方法 |
| US5584908A (en) * | 1994-11-14 | 1996-12-17 | Sherritt Inc. | Micron-sized nickel metal powder and a process for the preparation thereof |
| CN1060982C (zh) * | 1997-11-17 | 2001-01-24 | 北京有色金属研究总院 | 超细金属粉的制备方法 |
| AUPQ375499A0 (en) * | 1999-10-29 | 1999-11-25 | Wmc Resources Ltd | Nickel powder desulfurisation |
| EP1511564A1 (en) * | 2002-06-12 | 2005-03-09 | Sulzer Metco (Canada) Inc. | Hydrometallurgical process for production of supported catalysts |
| KR101085265B1 (ko) * | 2004-06-16 | 2011-11-22 | 도호 티타늄 가부시키가이샤 | 니켈 분말 및 그 제조 방법 |
| TW200806408A (en) * | 2006-06-27 | 2008-02-01 | Ishihara Sangyo Kaisha | Nickel fine particles, method for preparing the same and fluid composition comprising the same |
| EP1925307A1 (en) | 2006-11-03 | 2008-05-28 | Emotional Brain B.V. | Use of 3-alpha-androstanediol in the treatment of sexual dysfunction |
| JP5445777B2 (ja) | 2010-07-28 | 2014-03-19 | 住友金属鉱山株式会社 | 低品位ニッケル酸化鉱石からのフェロニッケル製錬原料の製造方法 |
| CN102070203A (zh) * | 2010-11-23 | 2011-05-25 | 金川集团有限公司 | 一种提高羰基镍粉纯度的方法 |
-
2014
- 2014-08-20 JP JP2014167904A patent/JP6406613B2/ja active Active
-
2015
- 2015-04-13 AU AU2015247017A patent/AU2015247017B2/en not_active Ceased
- 2015-04-13 US US15/303,557 patent/US10500644B2/en not_active Expired - Fee Related
- 2015-04-13 EP EP15779611.1A patent/EP3132874B1/en active Active
- 2015-04-13 WO PCT/JP2015/061358 patent/WO2015159846A1/ja not_active Ceased
- 2015-04-13 CA CA2945918A patent/CA2945918C/en not_active Expired - Fee Related
- 2015-04-13 CN CN201580016554.3A patent/CN106163707B/zh not_active Expired - Fee Related
-
2016
- 2016-10-14 PH PH12016502049A patent/PH12016502049A1/en unknown
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