JP2014507407A - フェロモン含有ポリ(メタ)アクリレート系マイクロカプセル - Google Patents
フェロモン含有ポリ(メタ)アクリレート系マイクロカプセル Download PDFInfo
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- JP2014507407A JP2014507407A JP2013548821A JP2013548821A JP2014507407A JP 2014507407 A JP2014507407 A JP 2014507407A JP 2013548821 A JP2013548821 A JP 2013548821A JP 2013548821 A JP2013548821 A JP 2013548821A JP 2014507407 A JP2014507407 A JP 2014507407A
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- pheromone
- weight
- microcapsule
- monomers
- monomer
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- DNTMQTKDNSEIFO-UHFFFAOYSA-N n-(hydroxymethyl)-2-methylprop-2-enamide Chemical compound CC(=C)C(=O)NCO DNTMQTKDNSEIFO-UHFFFAOYSA-N 0.000 description 1
- 125000004108 n-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 125000004123 n-propyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- WASNIKZYIWZQIP-AWEZNQCLSA-N nerolidol Natural products CC(=CCCC(=CCC[C@@H](O)C=C)C)C WASNIKZYIWZQIP-AWEZNQCLSA-N 0.000 description 1
- ZCYXXKJEDCHMGH-UHFFFAOYSA-N nonane Chemical compound CCCC[CH]CCCC ZCYXXKJEDCHMGH-UHFFFAOYSA-N 0.000 description 1
- SNQQPOLDUKLAAF-UHFFFAOYSA-N nonylphenol Chemical compound CCCCCCCCCC1=CC=CC=C1O SNQQPOLDUKLAAF-UHFFFAOYSA-N 0.000 description 1
- BKIMMITUMNQMOS-UHFFFAOYSA-N normal nonane Natural products CCCCCCCCC BKIMMITUMNQMOS-UHFFFAOYSA-N 0.000 description 1
- JPMIIZHYYWMHDT-UHFFFAOYSA-N octhilinone Chemical compound CCCCCCCCN1SC=CC1=O JPMIIZHYYWMHDT-UHFFFAOYSA-N 0.000 description 1
- 229920001542 oligosaccharide Polymers 0.000 description 1
- 150000002482 oligosaccharides Chemical class 0.000 description 1
- 239000004006 olive oil Substances 0.000 description 1
- 235000008390 olive oil Nutrition 0.000 description 1
- 239000000312 peanut oil Substances 0.000 description 1
- 235000010987 pectin Nutrition 0.000 description 1
- 239000001814 pectin Substances 0.000 description 1
- 229920001277 pectin Polymers 0.000 description 1
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 1
- UWJJYHHHVWZFEP-UHFFFAOYSA-N pentane-1,1-diol Chemical compound CCCCC(O)O UWJJYHHHVWZFEP-UHFFFAOYSA-N 0.000 description 1
- 230000000361 pesticidal effect Effects 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 229940044654 phenolsulfonic acid Drugs 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- WVDDGKGOMKODPV-ZQBYOMGUSA-N phenyl(114C)methanol Chemical compound O[14CH2]C1=CC=CC=C1 WVDDGKGOMKODPV-ZQBYOMGUSA-N 0.000 description 1
- 235000021118 plant-derived protein Nutrition 0.000 description 1
- 239000002798 polar solvent Substances 0.000 description 1
- 229920001983 poloxamer Polymers 0.000 description 1
- 229920003229 poly(methyl methacrylate) Polymers 0.000 description 1
- 229920000162 poly(ureaurethane) Polymers 0.000 description 1
- 229920005646 polycarboxylate Polymers 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 239000004926 polymethyl methacrylate Substances 0.000 description 1
- 229920001289 polyvinyl ether Polymers 0.000 description 1
- 239000001267 polyvinylpyrrolidone Substances 0.000 description 1
- 229920000036 polyvinylpyrrolidone Polymers 0.000 description 1
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 description 1
- 229920001592 potato starch Polymers 0.000 description 1
- FBCQUCJYYPMKRO-UHFFFAOYSA-N prop-2-enyl 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)OCC=C FBCQUCJYYPMKRO-UHFFFAOYSA-N 0.000 description 1
- QTECDUFMBMSHKR-UHFFFAOYSA-N prop-2-enyl prop-2-enoate Chemical compound C=CCOC(=O)C=C QTECDUFMBMSHKR-UHFFFAOYSA-N 0.000 description 1
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 1
- LYBIZMNPXTXVMV-UHFFFAOYSA-N propan-2-yl prop-2-enoate Chemical compound CC(C)OC(=O)C=C LYBIZMNPXTXVMV-UHFFFAOYSA-N 0.000 description 1
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical compound CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 description 1
- 239000003531 protein hydrolysate Substances 0.000 description 1
- GRWFGVWFFZKLTI-UHFFFAOYSA-N rac-alpha-Pinene Natural products CC1=CCC2C(C)(C)C1C2 GRWFGVWFFZKLTI-UHFFFAOYSA-N 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 229930195734 saturated hydrocarbon Natural products 0.000 description 1
- 125000002914 sec-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 1
- 238000010956 selective crystallization Methods 0.000 description 1
- 150000004666 short chain fatty acids Chemical class 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- SNOOUWRIMMFWNE-UHFFFAOYSA-M sodium;6-[(3,4,5-trimethoxybenzoyl)amino]hexanoate Chemical class [Na+].COC1=CC(C(=O)NCCCCCC([O-])=O)=CC(OC)=C1OC SNOOUWRIMMFWNE-UHFFFAOYSA-M 0.000 description 1
- 239000003549 soybean oil Substances 0.000 description 1
- 235000012424 soybean oil Nutrition 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 239000000021 stimulant Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
- 150000005846 sugar alcohols Chemical class 0.000 description 1
- IHCDKJZZFOUARO-UHFFFAOYSA-M sulfacetamide sodium Chemical compound O.[Na+].CC(=O)[N-]S(=O)(=O)C1=CC=C(N)C=C1 IHCDKJZZFOUARO-UHFFFAOYSA-M 0.000 description 1
- 239000002600 sunflower oil Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- APMORJJNVZMVQK-UHFFFAOYSA-N tert-butyl 4-chloro-2-methylcyclohexane-1-carboxylate Chemical compound CC1CC(Cl)CCC1C(=O)OC(C)(C)C APMORJJNVZMVQK-UHFFFAOYSA-N 0.000 description 1
- SUCYDSJQVVGOIW-UHFFFAOYSA-N trans-8-dodecenyl acetate Natural products CCCC=CCCCCCCCOC(C)=O SUCYDSJQVVGOIW-UHFFFAOYSA-N 0.000 description 1
- 229940074410 trehalose Drugs 0.000 description 1
- 150000003626 triacylglycerols Chemical class 0.000 description 1
- LADGBHLMCUINGV-UHFFFAOYSA-N tricaprin Chemical compound CCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCC)COC(=O)CCCCCCCCC LADGBHLMCUINGV-UHFFFAOYSA-N 0.000 description 1
- PHYFQTYBJUILEZ-IUPFWZBJSA-N triolein Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC(OC(=O)CCCCCCC\C=C/CCCCCCCC)COC(=O)CCCCCCC\C=C/CCCCCCCC PHYFQTYBJUILEZ-IUPFWZBJSA-N 0.000 description 1
- OOLLAFOLCSJHRE-ZHAKMVSLSA-N ulipristal acetate Chemical compound C1=CC(N(C)C)=CC=C1[C@@H]1C2=C3CCC(=O)C=C3CC[C@H]2[C@H](CC[C@]2(OC(C)=O)C(C)=O)[C@]2(C)C1 OOLLAFOLCSJHRE-ZHAKMVSLSA-N 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 239000003981 vehicle Substances 0.000 description 1
- 239000000052 vinegar Substances 0.000 description 1
- 235000021419 vinegar Nutrition 0.000 description 1
- ZTWTYVWXUKTLCP-UHFFFAOYSA-N vinylphosphonic acid Chemical compound OP(O)(=O)C=C ZTWTYVWXUKTLCP-UHFFFAOYSA-N 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 239000004563 wettable powder Substances 0.000 description 1
- 239000000230 xanthan gum Substances 0.000 description 1
- 229920001285 xanthan gum Polymers 0.000 description 1
- 235000010493 xanthan gum Nutrition 0.000 description 1
- 229940082509 xanthan gum Drugs 0.000 description 1
- 239000000811 xylitol Substances 0.000 description 1
- 235000010447 xylitol Nutrition 0.000 description 1
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 description 1
- 229960002675 xylitol Drugs 0.000 description 1
- 239000012138 yeast extract Substances 0.000 description 1
- FYGDTMLNYKFZSV-BYLHFPJWSA-N β-1,4-galactotrioside Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@H](CO)O[C@@H](O[C@@H]2[C@@H](O[C@@H](O)[C@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O FYGDTMLNYKFZSV-BYLHFPJWSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/26—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests in coated particulate form
- A01N25/28—Microcapsules or nanocapsules
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/02—Acyclic compounds
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/02—Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
Landscapes
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Agronomy & Crop Science (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Toxicology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Catching Or Destruction (AREA)
Abstract
【選択図】なし
Description
30〜90重量%の、1種以上の、アクリル酸及び/又はメタクリル酸のC1〜C24-アルキルエステル、アクリル酸、メタクリル酸及び/又はマレイン酸(モノマーI)、
10〜70重量%の1種以上の二官能性及び/又は多官能性モノマー(モノマーII)、及び
0〜40重量%の1種以上の他のモノマー(モノマーIII)
を含有するカプセル壁とを含むマイクロカプセルによって解決された。
-例えば、肉粉、魚粉、魚エキス、海産物、海産物エキス、又は血粉、昆虫各部、コオロギ粉、酵母エキス、卵黄、タンパク質加水分解物、酵母自己消化物、グルテン加水分解物、及び同様のものの形態の動物タンパク質及び植物タンパク質を含むタンパク質;
-炭水化物及び水素化炭水化物、特に、ブドウ糖、アラビノース、果糖、マンノース、ショ糖、乳糖、ガラクトース、マルトース、マルトトリオース、マルトテトロース、マルトペントースなどの単糖及び二糖、又は、それらの混合物、例えば、糖蜜、コーンシロップ、メープルシロップ、転化糖、及びハチミツなど;デンプンを含めた多糖、例えばジャガイモデンプン、トウモロコシデンプン、及び、例えば穀物粉(例えば小麦粉、トウモロコシ粉、麦芽粉、米粉、米ぬか)、ペクチン、及びグリセロールなどのデンプン系の材料、例えばキシリトール、ソルビトール、マンニトール、イソマルトース、トレハロース及びマルチトールなどの水素化単糖及びオリゴ糖(糖アルコール)、並びにマルチトール含有シロップ;
好ましい誘引物質は、3-メチルブタン酸エチル、サリチル酸メチル、酢酸アミル、リモネン又は果実エキスである(例えば、乾燥及び抽出されたリンゴからできたリンゴエキスは、果糖、ブドウ糖、ソルビトール、及びリンゴの香味料を含む)。誘引物質の混合物もまた適している。
1〜20重量%のフェロモン(例えばコドレモン)、
5〜60重量%の水に非混和性の有機溶媒(例えば脂肪酸グリセリド)、及び
35〜85重量%の誘引物質(例えば3-メチルブタン酸エチル)
を含み、
ここで、成分は合計で100重量%になる。
3〜10重量%のフェロモン、
15〜45重量%の水に非混和性の有機溶媒、及び
45〜75重量%の誘引物質
を含み、
ここで、成分は合計で100重量%になる。
鱗翅目の昆虫(鱗翅目)、例えばタマナヤガ(Agrotis ypsilon)、カブラヤガ(Agrotis segetum)、アラバマアルギラセア(Alabama argillacea)、アンチカルシアゲマタリス(Anticarsia gemmatalis)、リンゴヒメシンクイ(Argyresthia conjugella)、ガンマキンウワバ(Autographa gamma)、ブパルスピニアリウス(Bupalus piniarius)、カコエシアムリナナ(Cacoecia murinana)、カプアレチクラナ(Capua reticulana)、ケイマトビアブルマタ(Cheimatobia brumata)、トウヒノシントメハマキ(Choristoneura fumiferana)、コリストネウラオシデンタリス(Choristoneura occidentalis)、シルフィスウニプンクタ(Cirphis unipuncta)、コドリンガ(Cydia pomonella)、デンドロリムスピニ(Dendrolimus pini)、ディアファニアニチダリス(Diaphania nitidalis)、サウスウエスタンコーンボーラー(Diatraea grandiosella)、ミスジアオリンガ(Earias insulana)、モロコシマダラメイガ(Elasmopalpus lignosellus)、ブドウホソハマキ(Eupoecilia ambiguella)、エベトリアボウリアナ(Evetria bouliana)、フェルチアスブテラネア(Feltia subterranea)、ハチノスツヅリガ(Galleria mellonella)、グラホリタフネブラナ(Grapholitha funebrana)、ナシヒメシンクイ(Grapholitha molesta)、オオタバコガ(Heliothis armigera)、ニセアメリカタバコガ(Heliothis virescens)、アメリカタバコガ(Heliothis zea)、ハイマダラノメイガ(Hellula undalis)、ヒベルニアデホリアリア(Hibernia defoliaria)、アメリカシロヒトリ(Hyphantria cunea)、ヒポノメウタマリネルス(Hyponomeuta malinellus)、ケイフェリアリコペルシセラ(Keiferia lycopersicella)、ラムブディナフィスセラリア(Lambdina fiscellaria)、シロイチモジヨトウ(Laphygma exigua)、ロイコプテラコフェーラ(Leucoptera coffeella)、ロイコプテラシテラ(Leucoptera scitella)、リソコレチスブランカルデラ(Lithocolletis blancardella)、ロベシアボトラナ(Lobesia botrana)、ヘリキスジノメイガ(Loxostege sticticalis)、マイマイガ(Lymantria dispar)、ノンネマイマイ(Lymantria monacha)、モモハモグリガ(Lyonetia clerkella)、オビカレハ(Malacosoma neustria)、ヨトウガ(Mamestra brassicae)、オルギアシュードツガタ(Orgyia pseudotsugata)、アワノメイガ(Ostrinia nubilalis)、パノリスフラメア(Panolis flammea)、ワタアカミムシガ(Pectinophora gossypiella)、ニセタマナヤガ(Peridroma saucia)、ファレラブセファラ(Phalera bucephala)、ジャガイモガ(Phthorimaea operculella)、ミカンハモグリガ(Phyllocnistis citrella)、オオモンシロチョウ(Pieris brassicae)、プラチペナスカブラ(Plathypena scabra)、コナガ(Plutella xylostella)、キンウワバ(Pseudoplusia includens)、リアシオニアフルストラナ(Rhyacionia frustrana)、スクロビパルプラアブソルタ(Scrobipalpula absoluta)、バクガ(Sitotroga cerealella)、テングハマキ(Sparganothis pilleriana)、スポドプテラフルギペルダ(Spodoptera frugiperda)、エジプトヨトウ(Spodoptera littoralis)、ハスモンヨトウ(Spodoptera litura)、タウマトポエアピチオカンパ(Thaumatopoea pityocampa)、トルトリクスビリダナ(Tortrix viridana)、タマナキンウワバガ(Trichoplusiani)及びゼイラフェラカナデンシス(Zeiraphera canadensis)、
甲虫(甲虫目(Coleoptera))、例えば、アグリルス・シヌアツス(Agrilus sinuatus)、アグリオテス・リネアツス(Agriotes lineatus)、アグリオテス・オブスクルス(Agriotes obscurus)、アンヒマルス・ソルスチチアリス(Amphimallus solstitialis)、アニサンドルス・ジスパル(Anisandrus dispar)、アントノムス・グランジス(Anthonomus grandis)、アントノムス・ポモルム(Anthonomus pomorum)、アフトナ・エウフォリダエ(Aphthona euphoridae)、アトウス・ハエモロイダリス(Athous haemorrhoidalis)、アトマリア・リネアリス(Atomaria linearis)、ブラストファグス・ピニペルダ(Blastophagus piniperda)、ブリトファガ・ウンダータ(Blitophaga undata)、ブルクス・ルフィマヌス(Bruchus rufimanus)、ブルクス・ピソルム(Bruchus pisorum)、ブルクス・レンチス(Bruchus lentis)、ビクチスクス・ベツラエ(Byctiscus betulae)、カシダ・ネブロサ(Cassida nebulosa)、セロトマ・トリフルカタ(Cerotoma trifurcata)、セトニア・アウラータ(Cetonia aurata)、ソートリンクス・アシミリス(Ceuthorrhynchus assimilis)、ソートリンクス・ナピ(Ceuthorrhynchus napi)、カエトクネマ・チビアリス(Chaetocnema tibialis)、コノデルス・ベスペルチヌス(Conoderus vespertinus)、クリオセリス・アスパラギ(Crioceris asparagi)、クテニセラ属の種(Ctenicera spp.)、ジアブロチカ・ロンギコルニス(Diabrotica longicornis)、ジアブロチカ・セミプンクタタ(Diabrotica semipunctata)、ジアブロチカ・12-プンクタタ(Diabrotica 12-punctata)、ジアブロティカ・スペキオサ(Diabrotica speciosa)、ジアブロチカ・ビルギフェラ(Diabrotica virgifera)、エピラクナ・バリベスチス(Epilachna varivestis)、エピトリックス・ヒルチペニス(Epitrix hirtipennis)、エウチノボトルス・ブラシリエンシス(Eutinobothrus brasiliensis)、ヒロビウス・アビエチス(Hylobius abietis)、ヒペラ・ブルネイペニス(Hypera brunneipennis)、ヒペラ・ポスチカ(Hypera postica)、イプス・チポグラフス(Ips typographus)、レマ・ビリネアタ(Lema bilineata)、レマ・メラノプス(Lema melanopus)、レプチノタルサ・デセムリネアタ(Leptinotarsa decemlineata)、リモニウス・カリフォルニクス(Limonius californicus)、リソロプトルス・オリゾフィルス(Lissorhoptrus oryzophilus)、メラノツス・コムニス(Melanotus communis)、メリゲテス・アエネウス(Meligethes aeneus)、メロロンタ・ヒポカスタニ(Melolontha hippocastani)、メロロンタ・メロロンタ(Melolontha melolontha)、オウレマ・オリザエ(Oulema oryzae)、オチオリンクス・スルカツス(Otiorrhynchus sulcatus)、オチオリンクス・オバツス(Otiorrhynchus ovatus)、ファエドン・コクレアリアエ(Phaedon cochleariae)、フィロビウス・ピリ(Phyllobius pyri)、フィロトレタ・クリソセファラ(Phyllotreta chrysocephala)、フィロファガ属の種(Phyllophaga spp.)、フィロペルタ・ホルチコラ(Phyllopertha horticola)、フィロトレタ・ネモルム(Phyllotreta nemorum)、フィロトレタ・ストリオラタ(Phyllotreta striolata)、ポピリア・ジャポニカ(Popillia japonica)、シトナ・リネアツス(Sitona lineatus)及びシトフィルス・グラナリア(Sitophilus granaria)、
ハエ、蚊(双翅目(Diptera))、例えば、アエデス・アエギプチ(Aedes aegypti)、アエデス・アルボピクツス(Aedes albopictus)、アエデス・ベキサンス(Aedes vexans)、アナストレファ・ルデンス(Anastrepha ludens)、アノフェレス・マクリペニス(Anopheles maculipennis)、アノフェレス・クルキアンス(Anopheles crucians)、アノフェレス・アルビマヌス(Anopheles albimanus)、アノフェレス・ガンビアエ(Anopheles gambiae)、アノフェレス・フレボルニ(Anopheles freeborni)、アノフェレス・ロイコスフィルス(Anopheles leucosphyrus)、アノフェレス・ミニムス(Anopheles minimus)、アノフェレス・クァドリマクラツス(Anopheles quadrimaculatus)、バクトロセラ・オレア(bactrocera olea)、カリフォラ・ビキナ(Calliphora vicina)、セラチチス・カピタタ(Ceratitis capitata)、クリソミア・ベジアナ(Chrysomya bezziana)、クリソミア・ホミニボラックス(Chrysomya hominivorax)、クリソミア・マセラリア(Chrysomya macellaria)、クリソプス・ジスカリス(Chrysops discalis)、クリソプス・シラセア(Chrysops silacea)、クリソプス・アトランチクス(Chrysops atlanticus)、コクリオミア・ホミニボラックス(Cochliomyia hominivorax)、コンタリニア・ソルギコラ(Contarinia sorghicola)、コルジロビア・アントロポファガ(Cordylobia anthropophaga)、クリコイデス・フレンス(Culicoides furens)、クレックス・ピピエンス(Culex pipiens)、クレックス・ニグリパルパス(Culex nigripalpus)、クレックス・クインクエファシアツス(Culex quinquefasciatus)、クレックス・タルサリス(Culex tarsalis)、クリセタ・イノルナタ(Culiseta inornata)、クリセタ・メラヌラ(Culiseta melanura)、ダクス・ククルビタエ(Dacus cucurbitae)、ダクス・オレアエ(Dacus oleae)、ダシネウラ・ブラシカエ(Dasineura brassicae)、デリア・アンチクエ(Delia antique)、デリア・コアルクタタ(Delia coarctata)、デリア・プラツラ(Delia platura)、デリア・ラジクム(Delia radicum)、デルマトビア・ホミニス(Dermatobia hominis)、ファニア・カニクラリス(Fannia canicularis)、ゲオミザ・トリプンクタタ(Geomyza Tripunctata)、ガステロフィルス・インテスチナリス(Gasterophilus intestinalis)、グロシナ・モルシタンス(Glossina morsitans)、グロシナ・パルパリス(Glossina palpalis)、グロシナ・フシペス(Glossina fuscipes)、グロシナ・タキノイデス(Glossina tachinoides)、ハエマトビア・イリタンス(Haematobia irritans)、ハプロジプロシス・エクエストリス(Haplodiplosis equestris)、ヒッペラテス属の種(Hippelates spp.)、ヒレミア・プラツラ(Hylemyia platura)、ヒポデルマ・リネアタ(Hypoderma lineata)、レプトコノプス・トレンス(Leptoconops torrens)、リリオミザ・サチバエ(Liriomyza sativae)、リリオミザ・トリフォリイ(Liriomyza trifolii)、ルキリア・カプリナ(Lucilia caprina)、ルキリア・クプリナ(Lucilia cuprina)、ルキリア・セリカタ(Lucilia sericata)、リコリア・ペクトラリス(Lycoria pectoralis)、マンソニア・チチラヌス(Mansonia titillanus)、マイエチオラ・デストルクトル(Mayetiola destructor)、ムスカ・ドメスチカ(Musca domestica)、ムシナ・スタブランス(Muscina stabulans)、オエストルス・オビス(Oestrus ovis)、オポミザ・フロルム(Opomyza florum)、オシネラ・フリット(Oscinella frit)、ペゴミア・ヒソキアミ(Pegomya hysocyami)、フォルビア・アンチクア(Phorbia antiqua)、フォルビア・ブラシカエ(Phorbia brassicae)、フォルビア・コアルクタタ(Phorbia coarctata)、フレボトムス・アルゲンチペス(Phlebotomus argentipes)、プソロフォラ・コルンビアエ(Psorophora columbiae)、プシラ・ロサエ(Psila rosae)、プソロフォラ・ジスコロル(Psorophora discolor)、プロシムリウム・ミクスツム(Prosimulium mixtum)、ラゴレチス・セラシ(Rhagoletis cerasi)、ラゴレチス・ポモネラ(Rhagoletis pomonella)、サルコファガ・ハエモロイダリス(Sarcophaga haemorrhoidalis)、サルコファガ属の種(Sarcophaga spp.)、シムリウム・ビッタツム(Simulium vittatum)、ストモキシス・カルキトランス(Stomoxys calcitrans)、タバヌス・ボビヌス(Tabanus bovinus)、タバヌス・アトラツス(Tabanus atratus)、タバヌス・リネオラ(Tabanus lineola)及びタバナス・シミリス(Tabanus similis)、チプラ・オレラセア(Tipula oleracea)及びチプラ・パルドサ(Tipula paludosa)、
ゴキブリ(ゴキブリ亜目(Blattodea))、例えば、ブラテラ・ゲルマニカ(Blattella germanica)、ブラテラ・アサヒナエ(Blattella asahinae)、ペリプラネタ・アメリカーナ(Periplaneta americana)、ペリプラネタ・ジャポニカ(Periplaneta japonica)、ペリプラネタ・ブルネア(Periplaneta brunnea)、ペリプラネタ・フリギノサ(Periplaneta fuligginosa)、ペリプラネタ・アウストララシアエ(Periplaneta australasiae)、及びブラッタ・オリエンタリス(Blatta orientalis)、
アリ、ミツバチ、狩蜂、ハバチ(膜翅目(Hymenoptera))、例えば、アタリア・ロサエ(Athalia rosae)、アッタ・セファロテス(Atta cephalotes)、アッタ・カピグアラ(Atta capiguara)、アッタ・セファロテス(Atta cephalotes)、アッタ・ラエビガタ(Atta laevigata)、アッタ・ロブスタ(Atta robusta)、アッタ・セクスデンス(Atta sexdens)、アッタ・テキサナ(Atta texana)、クレマトガステル属の種(Crematogaster spp.)、ホプロカンパ・ミヌタ(Hoplocampa minuta)、ホプロカンパ・テスツジネア(Hoplocampa testudinea)、モノモリウム・ファラオニス(Monomorium pharaonis)、ソレノプシス・ゲミナタ(Solenopsis geminata)、ソレノプシス・インビクタ(Solenopsis invicta)、ソレノプシス・リクテリ(Solenopsis richteri)、ソレノプシス・キシロニ(Solenopsis xyloni)、ポゴノミルメックス・バルバツス(Pogonomyrmex barbatus)、ポゴノミルレックス・カリフォルニクス(Pogonomyrmex californicus)、フェイドレ・メガセファラ(Pheidole megacephala)、ダシムチラ・オシデンタリス(Dasymutilla occidentalis)、ボンブス属の種(Bombus spp.)、ベスプラ・スクアモサ(Vespula squamosa)、パラベスプラ・ブルガリス(Paravespula vulgaris)、パラベスプラ・ペンシルバニカ(Paravespula pennsylvanica)、パラベスプラ・ゲルマニカ(Paravespula germanica)、ドリコベスプラ・マクラタ(Dolichovespula maculata)、ベスパ・クラブロ(Vespa crabro)、ポリステス・ルビギノサ(Polistes rubiginosa)、カンポノツス・フロリダヌス(Camponotus floridanus)及びリネピテマ・フミレ(Linepithema humile)、
コオロギ、バッタ、イナゴ(直翅目(Orthoptera))、例えば、アケタ・ドメスティカ(Acheta domestica)、グリロタルパ・グリロタルパ(Gryllotalpa gryllotalpa)、ロクスタ・ミグラトリア(Locusta migratoria)、メラノプラス・ビビタツス(Melanoplus bivittatus)、メラノプラス・フムルールブラム(Melanoplus femurrubrum)、メラノプラス・メキシカヌス(Melanoplus mexicanus)、メラノプラス・サングイニペス(Melanoplus sanguinipes)、メラノプラス・スプレツス(Melanoplus spretus)、ノマダクリス・セプテムファシアタ(Nomadacris septemfasciata)、シストセルカ・アメリカナ(Schistocerca americana)、シストセルカ・グレガリア(Schistocerca gregaria)、ドキオスタウルス・マロカヌス(Dociostaurus maroccanus)、タキキネス・アシナモルス(Tachycines asynamorus)、オエダレウス・セネガレンシス(Oedaleus senegalensis)、ゾノゼルス・バリエガツス(Zonozerus variegatus)、ヒエログリフス・ダガネンシス(Hieroglyphus daganensis)、クラウサリア・アングリフェラ(Kraussaria angulifera)、カリプタムス・イタリクス(Calliptamus italicus)、コルトイセテス・テルミニフェラ(Chortoicetes terminifera)、及びロクスタナ・パルダリナ(Locustana pardalina)。
マイクロカプセルの合成
水相:
52.47g 水
5.90g ポリビニルアルコール(加水分解度74〜80モル%、ブルックフィールド粘度計で測定して、20℃における4%水溶液の粘度 5.2〜6.2mPas)
0.16g 2.5重量%の亜硝酸ナトリウム水溶液
油相:
17.68g 酢酸(E)7-(Z)9-ドデカジエニル(フェロモン)
17.68g 1,8-ジイソプロピルナフタレン(DIPN)
1.18g メタクリル酸メチル
0.79g 1,4-ブタンジオールジアクリレート
1.18g メタクリル酸
0.79g PETIA
供給物1: 0.28gのt-ブチルペルピバレートの75重量%炭化水素溶液
供給物2: 0.43gのt-ブチルヒドロペルオキシドの10重量%水溶液
供給物3: 1.98gの水及び0.02gのアスコルビン酸
水相を最初に入れた。油相を加えて分散させた。次に、形成したエマルションをフラスコに移し、供給物1を加え、混合物を撹拌下で70℃まで加熱し、70℃で1時間保持した。次にそれを85℃まで加熱し、85℃で2時間保持した。形成されたマイクロカプセル分散液に撹拌下で供給物2を加えた。供給物3を50分以内に量り入れ、その過程で、混合物を60分以内に室温まで冷却した。形成されたマイクロカプセル分散液は、表6に示す固形物含有量及び平均粒径を有していた(サイズはフラウンホーファー回折によって、体積平均で測定した)。
マイクロカプセルの合成
水相:
43.62g 水
15.72g ポリビニルアルコール(水中10重量%、加水分解度88%)
0.16g 2.5重量%の亜硝酸ナトリウム水溶液
油相:
17.68g 酢酸Z-8-ドデセニル(フェロモン)
17.68g 水に非混和性の溶媒
1.18g メタクリル酸メチル
1.18g メタクリル酸
0.79g 1,4-ブタンジオールジアクリレート
0.79g PETIA
供給物1: 0.28g t-ブチルペルピバレートの75重量%脂肪族炭化水素溶液
供給物2: 0.43g t-ブチルヒドロペルオキシドの10重量%水溶液
供給物3: 1.98gの水及び0.02gのアスコルビン酸
水相を最初に入れた。油相を加えて させた。次に、形成されたエマルションをフラスコに移し、供給物1を加え、混合物を撹拌下で70℃まで加熱し、70℃で1時間保持した。次に、それを85℃まで加熱し、85℃で2時間保持した。形成されたマイクロカプセル分散液に撹拌下で供給物2を加えた。供給物3を50分以内に量り入れ、その過程で、混合物を60分以内に室温まで冷却した。形成されたマイクロカプセル分散液は、表1に示す固形物含有量及び平均粒径を有していた。
マイクロカプセルの合成
水相:
236.3g 水
60.0g ポリビニルアルコール(水中10重量%、加水分解度88%)
0.23gの2.5重量%亜硝酸ナトリウム水溶液
油相:
45.2g 水に非混和性の溶媒/コドレモン(重量比 9/1)
3.39g メタクリル酸メチル(MMA)
3.39g メタクリル酸(MAS)
2.26g ブタンジオールジアクリレート(BDDA)
2.26g PETIA
供給物1: 0.40g tert-ブチルペルピバレート(75%)
供給物2: 0.62g 炭化水素中10重量%のtert-ブチルヒドロペルオキシド水溶液
供給物3: 3.3g 1重量%のアスコルビン酸水溶液
まず、上記組成を用いて水相及び油相を別々に生成した。室温で水相を最初に入れた。油相を加え、15000rpmで1分間、分散撹拌機で分散させた。次に、形成されたエマルションを窒素下でフラスコに移し、撹拌した。供給物1を加え、錨型撹拌機を用いた撹拌下で混合物を70℃まで加熱し、70℃で1時間保持した。次に、それを85℃まで加熱し、85℃で2時間保持した。形成されたマイクロカプセル分散液に撹拌下で供給物2を加えた。供給物3を50分以内に量り入れ、その過程で、混合物を60分以内に室温まで冷却した。さまざまな溶媒を使用した(表2参照)。
マイクロカプセルの合成
水相:
27.36g 水
45.63g ポリビニルアルコール(水中10重量%、加水分解度88%)
0.17gの2.5重量%亜硝酸ナトリウム水溶液
油相:
35.0g 水に非混和性の溶媒/フェロモン/誘引物質(重量比 表1参照)
2.58g メタクリル酸メチル
2.58g メタクリル酸
1.72g ブタンジオールジアクリレート
1.72g PETIA
供給物1: 0.30g tert-ブチルペルピバレート(75%)
供給物2: 0.47g 炭化水素中10重量%のtert-ブチルヒドロペルオキシド水溶液
供給物3: 2.51g 1重量%のアスコルビン酸水溶液
フェロモンはコドレモンであり、誘引物質は3-メチルブタン酸エチルであった。PETIAは、ペンタエリトリトールのトリ-及びテトラアクリレートの工業用混合物である。まず、上記組成を用いて水相及び油相を別々に生成した。室温で水相を最初に入れた。油相を加え、15000rpmで1分間、分散撹拌機で分散させた。次に、形成されたエマルションを窒素下でフラスコに移し、撹拌した。供給物1を加え、錨型撹拌機を用いた撹拌下で混合物を70℃まで加熱し、70℃で1時間保持した。次に、それを85℃まで加熱し、85℃で2時間保持した。形成されたマイクロカプセル分散液に撹拌下で供給物2を加えた。供給物3を50分以内に量り入れ、その過程で、混合物を60分以内に室温まで冷却した。形成されたマイクロカプセル分散液は、表4に示す固形物含有量及び平均粒径を有していた(サイズは、フラウンホーファー回折、体積平均で測定された)。
風洞試験
Analytical Research Systems製の12×12×48インチの風洞を使用した。消灯し、暗幕で囲った実験室領域に風洞を設置した。赤色のパーティーライトで上方から風洞に照明を当てた。化学的処理の合間に、風洞及びすべての関連する試験材料を洗浄した。処理ごとに、一度に各2匹の昆虫を用いて10回の実験を行った。
-翼の送風-翼の高速の動き、
-離陸-プラットフォームの動き、
-風上応答-風洞の上方へ半分を超えた動き、
-指向性飛行-風プルーム(wind plume)の追尾、及び
-発生源接触-ゴム隔膜への接触
の行動応答を、発生源に接触するまでの時間とともに記録した。観察は、3分後又は昆虫が発生源と接触したときに完了した。
Claims (17)
- フェロモンを含有するカプセルコアと、重合形態で、いずれの場合もモノマーの全重量に基づいて、
30〜90重量%の、1種以上の、アクリル酸及び/又はメタクリル酸のC1〜C24-アルキルエステル、アクリル酸、メタクリル酸及び/又はマレイン酸(モノマーI)、
10〜70重量%の1種以上の二官能性及び/又は多官能性モノマー(モノマーII)、及び
0〜40重量%の1種以上の他のモノマー(モノマーIII)
を含有するカプセル壁と
を含むマイクロカプセル。 - フェロモンが、カプセルコア内に溶解形態で存在する、請求項1に記載のマイクロカプセル。
- フェロモンが、20℃で、最大で1000mg/lの水への溶解度を有する、請求項1又は2に記載のマイクロカプセル。
- コアが、水に非混和性の有機溶媒を含有する、請求項1から3のいずれか1項に記載のマイクロカプセル。
- 有機溶媒が、脂肪酸トリグリセリド又は炭化水素である、請求項4に記載のマイクロカプセル。
- カプセルコアが、最大で60重量%の有機溶媒を含む、請求項1から5のいずれか1項に記載のマイクロカプセル。
- カプセルコアが、誘引物質を含有する、請求項1から6のいずれか1項に記載のマイクロカプセル。
- 誘引物質が、3-メチルブタン酸エチルである、請求項7に記載のマイクロカプセル。
- フェロモンの誘引物質に対する重量比が、1/99〜40/60の範囲内にある、請求項7又は8に記載のマイクロカプセル。
- マイクロカプセルが、マイクロカプセルの全重量に基づいて、3〜50重量%のカプセルシェルを含む、請求項7から9のいずれか1項に記載のマイクロカプセル。
- モノマーIIが、1種以上の二官能性及び多官能性のモノマーを含む、請求項1から10のいずれか1項に記載のマイクロカプセル。
- モノマー、フリーラジカル開始剤、保護コロイド、及びカプセル化すべきフェロモンから水中油型エマルションを調製することと、加熱によってモノマーの重合を誘発することとを含む、請求項1から11のいずれか1項に記載のマイクロカプセルの製造方法。
- 請求項1から11のいずれか1項に記載のマイクロカプセルを、対象とする昆虫の生息場所、又は対象とする昆虫から保護すべき植物に作用させる、望ましくない昆虫侵襲を防除する方法。
- (E,E)-8,10-ドデカジエン-1-オールを含むフェロモン及び3-メチルブタン酸エチルを含む、望ましくない昆虫侵襲を防除する組成物。
- フェロモンの3-メチルブタン酸エチルに対する重量比が、1対10〜1対1000の範囲内にある、請求項15に記載の組成物。
- 3-メチルブタン酸エチルと(E,E)-8,10-ドデカジエン-1-オールとが混合される、請求項14又は15に記載の組成物の製造方法。
- 請求項14又は15に記載の組成物を、対象とする昆虫の生息場所、又は対象とする昆虫から保護すべき植物に作用させる、望ましくない昆虫侵襲を防除する方法。
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CN104814007A (zh) * | 2015-03-25 | 2015-08-05 | 中国林业科学研究院森林生态环境与保护研究所 | 一种松毛虫性信息素微胶囊及其制备方法 |
CN105145557B (zh) * | 2015-08-28 | 2017-10-17 | 华中农业大学 | 一种柑橘大实蝇性信息素 |
FR3041503B1 (fr) * | 2015-09-25 | 2017-10-20 | Melchior Mat And Life Science France | Projectiles oxodegradables contenant des pheromones |
CN106632825A (zh) * | 2015-10-30 | 2017-05-10 | 鸿富锦精密工业(深圳)有限公司 | 着色材料、着色膜及其制备方法、眼用镜片 |
FR3046334B1 (fr) | 2015-12-31 | 2020-03-06 | Melchior Material And Life Science France | Composition solide pour le relargage controle de substances semiochimiques |
JP7145728B2 (ja) * | 2018-10-25 | 2022-10-03 | 信越化学工業株式会社 | ハスモンヨトウの防除方法 |
JP2023508866A (ja) * | 2019-12-20 | 2023-03-06 | ビーエーエスエフ ソシエタス・ヨーロピア | 芳香化学物質としてのドデカンジエン-1-オール及びドデセン-1-オール又はそれらの混合物 |
FR3107667A1 (fr) | 2020-02-27 | 2021-09-03 | Melchior Material And Life Science France | Doses unitaires pour la liberation d’une formulation aqueuse |
FR3114100B1 (fr) | 2020-09-17 | 2023-05-12 | Melchior Mat And Life Science France | Composition fluide pour revetement de surface pour absorption et diffusion de composes volatils |
FR3114099B1 (fr) | 2020-09-17 | 2023-05-26 | Ceva Sante Animale | Composition fluide pour revetement de surface pour absorption et diffusion de composes volatils |
FR3133523A1 (fr) | 2022-03-17 | 2023-09-22 | Ceva Sante Animale | Dispositif multicouche autocollant imprégné d’une substance sémiochimique |
FR3133524A1 (fr) | 2022-03-17 | 2023-09-22 | Melchior Material And Life Science France | Dispositif multicouche autocollant imprégné d’une substance sémiochimique |
WO2024003267A1 (fr) * | 2022-06-30 | 2024-01-04 | Kapsera S.A.S. | Microcapsules contrôlant la diffusion d'un composé organique actif |
CN117397681B (zh) * | 2023-12-15 | 2024-02-27 | 中国医学科学院药用植物研究所 | 一种枸杞实蝇性信息素及其应用 |
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MX369648B (es) | 2019-11-15 |
US20130295154A1 (en) | 2013-11-07 |
PL2735230T3 (pl) | 2017-03-31 |
EP2735230B1 (en) | 2016-09-21 |
CN103458684A (zh) | 2013-12-18 |
JP5916757B2 (ja) | 2016-05-11 |
CN103458684B (zh) | 2016-01-20 |
KR20140006874A (ko) | 2014-01-16 |
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EP2735230A1 (en) | 2014-05-28 |
WO2012095444A3 (en) | 2012-09-07 |
BR112013017900A2 (pt) | 2016-07-12 |
EP2663183A2 (en) | 2013-11-20 |
KR101947574B1 (ko) | 2019-02-14 |
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WO2012095444A2 (en) | 2012-07-19 |
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