JP2014169351A - 水生生物付着防止粘着テープ - Google Patents
水生生物付着防止粘着テープ Download PDFInfo
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- JP2014169351A JP2014169351A JP2013040323A JP2013040323A JP2014169351A JP 2014169351 A JP2014169351 A JP 2014169351A JP 2013040323 A JP2013040323 A JP 2013040323A JP 2013040323 A JP2013040323 A JP 2013040323A JP 2014169351 A JP2014169351 A JP 2014169351A
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Abstract
【解決手段】本発明の水生生物付着防止粘着テープは、防汚層と基材層と粘着層をこの順に含む粘着テープであって、該防汚層の該基材層とは反対側にアプリケーションテープを備える。
【選択図】図1
Description
防汚層と基材層と粘着層をこの順に含む粘着テープであって、
該防汚層の該基材層とは反対側にアプリケーションテープを備える。
本発明の水生生物付着防止粘着テープは、防汚層と基材層と粘着層をこの順に含む粘着テープであって、該防汚層の該基材層とは反対側にアプリケーションテープを備える。すなわち、本発明の水生生物付着防止粘着テープは、アプリケーションテープと防汚層と基材層と粘着層をこの順に含む。本発明の水生生物付着防止粘着テープは、好ましくは、アプリケーションテープと粘着層が、それぞれ、最外層となる。本発明の水生生物付着防止粘着テープの特に好ましい実施形態は、アプリケーションテープと防汚層と基材層と粘着層がそれぞれ直接に積層された構成の粘着テープである。
本発明の水生生物付着防止粘着テープが有するアプリケーションテープとしては、一般にアプリケーションテープと称されているものなど、本発明の効果を損なわない範囲で任意の適切なアプリケーションテープを採用し得る。このようなアプリケーションテープとしては、好ましくは、支持体を含むアプリケーションテープである。また、このようなアプリケーションテープとして、支持体とともに、さらに粘着剤層を含むアプリケーションテープであっても良い。本発明の水生生物付着防止粘着テープがアプリケーションテープを有することにより、表面のすべり性が良好なものとなって、スキージ等を用いた貼り付け作業性が良好なものとなる。また、本発明の水生生物付着防止粘着テープがアプリケーションテープを有することにより、スキージ等を用いた貼り付け作業を行っても、防汚層が傷付き難く、表面保護性に優れたものとなる。
防汚層としては、本発明の効果を発現できる層であれば、任意の適切な層を採用し得る。防汚層としては、好ましくは、防汚塗料を用いることなく防汚効果を発現できる層であり、好ましくは、防汚効果を有する任意の適切な樹脂を含む。このような樹脂としては、好ましくは、シリコーン樹脂が挙げられる。
基材層としては、本発明の効果を損なわない範囲で、任意の適切な材料からなる基材層を採用し得る。このような基材層としては、好ましくは、エラストマー樹脂を含む。エラストマー樹脂としては、本発明の効果を損なわない範囲で任意の適切なエラストマー樹脂を採用し得る。このようなエラストマー樹脂としては、例えば、加硫ゴム、熱可塑性エラストマーなどが挙げられる。熱可塑性エラストマーとしては、例えば、スチレン系エラストマー、オレフィン系エラストマー、塩ビ系エラストマー、ウレタン系エラストマー、エステル系エラストマー、アミド系エラストマーなどが挙げられる。基材層がエラストマー樹脂を含む場合、基材層中のエラストマー樹脂の含有割合は、好ましくは50重量%以上であり、より好ましくは60重量%〜100重量%であり、さらに好ましくは70重量%〜99重量%であり、特に好ましくは80重量%〜98重量%であり、最も好ましくは90重量%〜97重量%である。
粘着層としては、本発明の効果を損なわない範囲で、任意の適切な粘着層を採用し得る。このような粘着層の材料としては、例えば、アクリル樹脂系粘着剤、エポキシ樹脂系粘着剤、アミノ樹脂系粘着剤、ビニル樹脂(酢酸ビニル系重合体など)系粘着剤、硬化型アクリル樹脂系粘着剤、シリコーン樹脂系粘着剤などが挙げられる。粘着層の材料は、1種のみであっても良いし、2種以上であっても良い。
本発明の水生生物付着防止粘着テープは、防汚層と基材層と粘着層から選ばれる少なくとも1層が耐候剤を含んでいても良い。すなわち、本発明の水生生物付着防止粘着テープの形態としては、(1)防汚層が耐候剤を含み、基材層と粘着層が耐候剤を含まない場合や、(2)基材層が耐候剤を含み、防汚層と粘着層が耐候剤を含まない場合や、(3)粘着層が耐候剤を含み、防汚層と基材層とが耐候剤を含まない場合や、(4)防汚層と基材層が耐候剤を含み、粘着層が耐候剤を含まない場合や、(5)防汚層と粘着層が耐候剤を含み、基材層が耐候剤を含まない場合や、(5)基材層と粘着層が耐候剤を含み、防汚層が耐候剤を含まない場合や、(6)防汚層と基材層と粘着層の全てが耐候剤を含む場合が挙げられる。これらの形態の中でも、基材層が耐候剤を含む形態が好ましい。基材層が耐候剤を含むことにより、本発明の水生生物付着防止粘着テープ自体の耐候性が向上し、野外での使用において太陽光によって基材が劣化し難くなり、当初の基材強度を十分に維持できる。一方、基材が劣化してしまうと、使用済みの本発明の水生生物付着防止粘着テープを被着体から剥がす際に、基材層が頻繁に切断してしまい、作業効率が著しく悪くなるおそれがある。
本発明の水生生物付着防止粘着テープは、任意の適切な方法によって製造し得る。このような方法としては、例えば、別途準備した基材層と粘着層を貼付した後に防汚層形成材料を基材層上に塗布して防汚層を形成する方法、基材層の一方の面に粘着層形成材料を塗布して粘着層を形成し、基材層のもう一方の面に防汚層形成材料を塗布して防汚層を形成する方法、基材層形成材料と粘着層形成材料を共押出しして基材層/粘着層の積層体を形成させた後に防汚層形成材料を基材層上に塗布して防汚層を形成する方法、などが挙げられる。
試験対象の粘着テープから50cm×300cmの大きさのサンプルを切り出した。被着体としては、プレジャーボート(Toprun FX24Z、ヤンマー(株)製)の船底を使用した。船底表面はゲルコート面である。
上記サンプルを被着体にスキージ(XE1032、エイブリィ製)を使用して貼り付け作業を行い、スキージのすべり性、防汚層の保護性、作業性、および汚染性を、下記の基準で評価した。
(スキージのすべり性)
○:非常にすべりやすい。
△:すべりやすい。
×:すべりにくい。
(防汚層の保護性)
○:防汚層の破損なし。
△:防汚層の破損小。
×:防汚層の破損多数。
(作業性)
○:非常に作業しやすい、作業時間も短縮する。
△:作業しやすい。
×:作業しにくい。
(汚染性)
○:汚染しない。
△:汚染しにくい。
×:汚染する。特に被着体や手に汚染する。
粘着テープを貼りつけた上記プレジャーボートをクレーンベルトで一度吊り上げ、その後に粘着テープ表面を観察し、保護性を下記の基準で評価した。
○:テープ表面に破損なし。
△:テープ表面の破損小。
×:テープ表面の破損多数。
粘着テープを貼りつけた上記プレジャーボートを船台に乗せ、10mほど移動させ、その後にプレジャーボートのすべり具合および粘着テープ表面の保護性を○△×で評価した。
○:プレジャーボートのすべりもなく、テープ表面に破損なし。
△:プレジャーボートは少しすべり、テープ表面の破損小。
×:プレジャーボートは大きくすべりもなく、テープ表面の破損多数。
(粘着層)
冷却管、窒素導入管、温度計、および攪拌機を備えた反応容器に、(メタ)アクリル系モノマーとして、2−エチルヘキシルアクリレート(2EHA、東亜合成(株)製):90重量部、アクリル酸(AA):10重量部、アクリルオリゴマー:5重量部、光重合開始剤として2,2−ジメトキシ−1,2−ジフェニルエタン−1−オン(商品名「イルガキュア651」、BASF製):0.1重量部を投入して分散させ、攪拌しながら窒素気流下にて上部よりUV照射することにより、一部のモノマーをポリマーに転化させて塗工可能な粘度に調整し、(メタ)アクリル系モノマー混合物を得た。この(メタ)アクリル系モノマー混合物に、架橋剤として1,6−ヘキサンジオールジアクリレート(HDDA):0.08重量部を添加し、これをセパレーター(商品名「MRF38」、三菱樹脂(株)製、厚み50μm)の表面にアプリケーターにて塗布し、カバーセパレータ(商品名「MRF38」、三菱樹脂(株)製、厚み38μm)をハンドローラーにて貼り合わせ、さらに紫外線ランプ(BLタイプ)により紫外線を照射(紫外線照度:3.4mW/cm2、積算照射量:2000mJ/cm2)することにより、厚み50μmの粘着層(1)を得た。
(基材層)
ウレタン樹脂基材(エスマーURS PXII、日本マタイ(株)製)を用い、厚み100μmの基材層(1)とした。
(粘着テープ)
得られた粘着層(1)と基材層(1)をハンドローラーにて貼り合わせ、テープを得た。そして、このテープの基材層(1)上に、付加型シリコーンエラストマー(KE−1950、信越化学工業(株)製)とシリコーンオイル(KF96‐100Cs、信越化学工業(株)製)とを100:90(重量比)で混合した混合液をアプリケーターにて塗工し、厚み100μmのシロップ層を形成した。これを150℃で5分間硬化させ、防汚層(1)を作成した。
テープの防汚層(1)上に、ポリエチレンを基材層とするアプリケーションテープ(3620、日東電工(株)製)を貼り合せ、粘着テープ(1)を作成した。
粘着テープ(1)の構成は、アプリケーションテープ(基材層厚み=60μm、粘着層厚み=12μm)/防汚層(厚み=100μm)/基材層(厚み=100μm)/粘着層(厚み=50μm)であった。
評価結果を表1に示した。
(粘着層)
実施例1と同様にして、厚み50μmの粘着層(2)を得た。
(基材層)
実施例1と同様にして、厚み100μmの基材層(2)を得た。
(粘着テープ)
得られた粘着層(2)と基材層(2)をハンドローラーにて貼り合わせ、テープを得た。そして、このテープの基材層(2)上に、付加型シリコーンエラストマー(KE−1950、信越化学工業(株)製)とシリコーンオイル(KF96‐100Cs、信越化学工業(株)製)とを100:90(重量比)で混合した混合液をアプリケーターにて塗工し、厚み100μmのシロップ層を形成した。これを150℃で5分間硬化させ、防汚層(2)を作成した。
テープの防汚層(2)上に、ポリエチレンを基材層とするアプリケーションテープ(C−600、日東電工(株)製)を貼り合せ、粘着テープ(2)を作成した。
粘着テープ(2)の構成は、アプリケーションテープ(基材層厚み=70μm、粘着層厚み=20μm)/防汚層(厚み=100μm)/基材層(厚み=100μm)/粘着層(厚み=50μm)であった。
評価結果を表1に示した。
(粘着層)
実施例1と同様にして、厚み50μmの粘着層(3)を得た。
(基材層)
実施例1と同様にして、厚み100μmの基材層(3)を得た。
(粘着テープ)
得られた粘着層(3)と基材層(3)をハンドローラーにて貼り合わせ、テープを得た。そして、このテープの基材層(3)上に、付加型シリコーンエラストマー(KE−1950、信越化学工業(株)製)とシリコーンオイル(KF96‐100Cs、信越化学工業(株)製)とを100:90(重量比)で混合した混合液をアプリケーターにて塗工し、厚み100μmのシロップ層を形成した。これを150℃で5分間硬化させ、防汚層(3)を作成した。
テープの防汚層(3)上に、ポリ塩化ビニル(PVC)を基材層とするアプリケーションテープ(AL−200、日東電工(株)製)を貼り合せ、粘着テープ(3)を作成した。
粘着テープ(3)の構成は、アプリケーションテープ(基材層厚み=70μm、粘着層厚み=8μm)/防汚層(厚み=100μm)/基材層(厚み=100μm)/粘着層(厚み=50μm)であった。
評価結果を表1に示した。
(粘着層)
実施例1と同様にして、厚み50μmの粘着層(4)を得た。
(基材層)
実施例1と同様にして、厚み100μmの基材層(4)を得た。
(粘着テープ)
得られた粘着層(4)と基材層(4)をハンドローラーにて貼り合わせ、テープを得た。そして、このテープの基材層(4)上に、付加型シリコーンエラストマー(KE−1950、信越化学工業(株)製)とシリコーンオイル(KF96‐100Cs、信越化学工業(株)製)とを100:90(重量比)で混合した混合液をアプリケーターにて塗工し、厚み100μmのシロップ層を形成した。これを150℃で5分間硬化させ、防汚層(4)を作成した。
テープの防汚層(4)上に、ポリエチレンとポリプロピレンからなる基材層からなるアプリケーションテープ(3648F、日東電工(株)製)を貼り合せ、粘着テープ(4)を作成した。
粘着テープ(4)の構成は、アプリケーションテープ(基材層厚み=40μm、粘着層厚み=13μm)/防汚層(厚み=100μm)/基材層(厚み=100μm)/粘着層(厚み=50μm)であった。
評価結果を表1に示した。
(粘着層)
実施例1と同様にして、厚み50μmの粘着層(C1)を得た。
(基材層)
実施例1と同様にして、厚み100μmの基材層(C1)を得た。
(粘着テープ)
得られた粘着層(C1)と基材層(C1)をハンドローラーにて貼り合わせ、テープを得た。そして、このテープの基材層(C1)上に、付加型シリコーンエラストマー(KE−1950、信越化学工業(株)製)とシリコーンオイル(KF96‐100Cs、信越化学工業(株)製)とを100:90(重量比)で混合した混合液をアプリケーターにて塗工し、厚み100μmのシロップ層を形成した。これを150℃で5分間硬化させ、防汚層(C1)を作成し、粘着テープ(C1)を作成した。
粘着テープ(C1)の構成は、防汚層(厚み=100μm)/基材層(厚み=100μm)/粘着層(厚み=50μm)であった。
評価結果を表1に示した。
2 防汚層
3 基材層
4 粘着層
10 剥離フィルム
100 水生生物付着防止粘着テープ
Claims (6)
- 防汚層と基材層と粘着層をこの順に含む粘着テープであって、
該防汚層の該基材層とは反対側にアプリケーションテープを備える、
水生生物付着防止粘着テープ。 - 前記アプリケーションテープが支持体を含む、請求項1に記載の水生生物付着防止粘着テープ。
- 前記アプリケーションテープがさらに粘着剤層を含む、請求項2に記載の水生生物付着防止粘着テープ。
- 前記基材層がエラストマー樹脂を含む、請求項1から3までのいずれかに記載の水生生物付着防止粘着テープ。
- 前記エラストマー樹脂が、ポリウレタンアクリル樹脂、ポリウレタン樹脂から選ばれる少なくとも1種である、請求項4に記載の水生生物付着防止粘着テープ。
- 前記防汚層がシリコーン樹脂を含む、請求項1から5までのいずれかに記載の水生生物付着防止粘着テープ。
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