JP2013544522A5 - - Google Patents
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- JP2013544522A5 JP2013544522A5 JP2013542097A JP2013542097A JP2013544522A5 JP 2013544522 A5 JP2013544522 A5 JP 2013544522A5 JP 2013542097 A JP2013542097 A JP 2013542097A JP 2013542097 A JP2013542097 A JP 2013542097A JP 2013544522 A5 JP2013544522 A5 JP 2013544522A5
- Authority
- JP
- Japan
- Prior art keywords
- component
- plant
- liquid
- extraction solvent
- starch
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000002904 solvent Substances 0.000 claims description 27
- 238000000605 extraction Methods 0.000 claims description 25
- 239000007788 liquid Substances 0.000 claims description 24
- 239000000463 material Substances 0.000 claims description 16
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 8
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 8
- 150000001875 compounds Chemical class 0.000 claims description 8
- 235000002639 sodium chloride Nutrition 0.000 claims description 7
- 229910019142 PO4 Inorganic materials 0.000 claims description 6
- 235000021317 phosphate Nutrition 0.000 claims description 6
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 claims description 5
- 239000003963 antioxidant agent Substances 0.000 claims description 5
- 235000006708 antioxidants Nutrition 0.000 claims description 5
- -1 halide salts Chemical class 0.000 claims description 5
- HRZFUMHJMZEROT-UHFFFAOYSA-L sodium disulfite Chemical compound [Na+].[Na+].[O-]S(=O)S([O-])(=O)=O HRZFUMHJMZEROT-UHFFFAOYSA-L 0.000 claims description 5
- 235000010323 ascorbic acid Nutrition 0.000 claims description 4
- 239000011668 ascorbic acid Substances 0.000 claims description 4
- 150000003013 phosphoric acid derivatives Chemical class 0.000 claims description 4
- 239000011780 sodium chloride Substances 0.000 claims description 4
- 229940001584 sodium metabisulfite Drugs 0.000 claims description 4
- 235000010262 sodium metabisulphite Nutrition 0.000 claims description 4
- 229960005070 ascorbic acid Drugs 0.000 claims description 3
- 239000000872 buffer Substances 0.000 claims description 3
- PYLIXCKOHOHGKQ-UHFFFAOYSA-L disodium;hydrogen phosphate;heptahydrate Chemical compound O.O.O.O.O.O.O.[Na+].[Na+].OP([O-])([O-])=O PYLIXCKOHOHGKQ-UHFFFAOYSA-L 0.000 claims description 3
- WBZKQQHYRPRKNJ-UHFFFAOYSA-L disulfite Chemical compound [O-]S(=O)S([O-])(=O)=O WBZKQQHYRPRKNJ-UHFFFAOYSA-L 0.000 claims description 3
- 230000003078 antioxidant effect Effects 0.000 claims description 2
- 239000007853 buffer solution Substances 0.000 claims description 2
- 229940052354 dibasic sodium phosphate heptahydrate Drugs 0.000 claims description 2
- BBMHARZCALWXSL-UHFFFAOYSA-M sodium dihydrogenphosphate monohydrate Chemical compound O.[Na+].OP(O)([O-])=O BBMHARZCALWXSL-UHFFFAOYSA-M 0.000 claims description 2
- 238000000034 method Methods 0.000 claims 47
- 241000196324 Embryophyta Species 0.000 claims 40
- 239000007787 solid Substances 0.000 claims 16
- 229920002472 Starch Polymers 0.000 claims 15
- 235000019698 starch Nutrition 0.000 claims 15
- 239000008107 starch Substances 0.000 claims 15
- 238000001035 drying Methods 0.000 claims 7
- 239000002245 particle Substances 0.000 claims 7
- 235000018102 proteins Nutrition 0.000 claims 6
- 102000004169 proteins and genes Human genes 0.000 claims 6
- 108090000623 proteins and genes Proteins 0.000 claims 6
- 238000000227 grinding Methods 0.000 claims 5
- 238000001914 filtration Methods 0.000 claims 4
- 239000000203 mixture Substances 0.000 claims 4
- 235000000346 sugar Nutrition 0.000 claims 4
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims 3
- 229930013930 alkaloid Natural products 0.000 claims 3
- 238000005119 centrifugation Methods 0.000 claims 3
- 108090000765 processed proteins & peptides Proteins 0.000 claims 3
- 235000004252 protein component Nutrition 0.000 claims 3
- 239000012465 retentate Substances 0.000 claims 3
- 244000061176 Nicotiana tabacum Species 0.000 claims 2
- ZTHYODDOHIVTJV-UHFFFAOYSA-N Propyl gallate Chemical compound CCCOC(=O)C1=CC(O)=C(O)C(O)=C1 ZTHYODDOHIVTJV-UHFFFAOYSA-N 0.000 claims 2
- LEHOTFFKMJEONL-UHFFFAOYSA-N Uric Acid Chemical compound N1C(=O)NC(=O)C2=C1NC(=O)N2 LEHOTFFKMJEONL-UHFFFAOYSA-N 0.000 claims 2
- 239000001913 cellulose Substances 0.000 claims 2
- 229920002678 cellulose Polymers 0.000 claims 2
- RWSXRVCMGQZWBV-WDSKDSINSA-N glutathione Chemical compound OC(=O)[C@@H](N)CCC(=O)N[C@@H](CS)C(=O)NCC(O)=O RWSXRVCMGQZWBV-WDSKDSINSA-N 0.000 claims 2
- 239000001814 pectin Substances 0.000 claims 2
- 229920001277 pectin Polymers 0.000 claims 2
- 235000010987 pectin Nutrition 0.000 claims 2
- 102000004196 processed proteins & peptides Human genes 0.000 claims 2
- 150000008163 sugars Chemical class 0.000 claims 2
- GJJVAFUKOBZPCB-UHFFFAOYSA-N 2-methyl-2-(4,8,12-trimethyltrideca-3,7,11-trienyl)-3,4-dihydrochromen-6-ol Chemical compound OC1=CC=C2OC(CCC=C(C)CCC=C(C)CCC=C(C)C)(C)CCC2=C1 GJJVAFUKOBZPCB-UHFFFAOYSA-N 0.000 claims 1
- 108010024636 Glutathione Proteins 0.000 claims 1
- 241000208125 Nicotiana Species 0.000 claims 1
- TVWHNULVHGKJHS-UHFFFAOYSA-N Uric acid Natural products N1C(=O)NC(=O)C2NC(=O)NC21 TVWHNULVHGKJHS-UHFFFAOYSA-N 0.000 claims 1
- 150000003797 alkaloid derivatives Chemical class 0.000 claims 1
- 150000001413 amino acids Chemical class 0.000 claims 1
- 229940072107 ascorbate Drugs 0.000 claims 1
- GVJHHUAWPYXKBD-UHFFFAOYSA-N d-alpha-tocopherol Natural products OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims 1
- 230000006378 damage Effects 0.000 claims 1
- 239000003599 detergent Substances 0.000 claims 1
- 235000013325 dietary fiber Nutrition 0.000 claims 1
- 229960003180 glutathione Drugs 0.000 claims 1
- 235000003969 glutathione Nutrition 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- 238000000265 homogenisation Methods 0.000 claims 1
- 239000004615 ingredient Substances 0.000 claims 1
- 230000001678 irradiating effect Effects 0.000 claims 1
- 238000002955 isolation Methods 0.000 claims 1
- 239000011859 microparticle Substances 0.000 claims 1
- 238000002156 mixing Methods 0.000 claims 1
- 150000008442 polyphenolic compounds Chemical class 0.000 claims 1
- 235000013824 polyphenols Nutrition 0.000 claims 1
- 235000010388 propyl gallate Nutrition 0.000 claims 1
- 239000000473 propyl gallate Substances 0.000 claims 1
- 229940075579 propyl gallate Drugs 0.000 claims 1
- 238000000926 separation method Methods 0.000 claims 1
- 239000011343 solid material Substances 0.000 claims 1
- 239000004094 surface-active agent Substances 0.000 claims 1
- 150000003573 thiols Chemical class 0.000 claims 1
- 235000010384 tocopherol Nutrition 0.000 claims 1
- 229930003799 tocopherol Natural products 0.000 claims 1
- 239000011732 tocopherol Substances 0.000 claims 1
- 229960001295 tocopherol Drugs 0.000 claims 1
- 229930003802 tocotrienol Natural products 0.000 claims 1
- 239000011731 tocotrienol Substances 0.000 claims 1
- 235000019148 tocotrienols Nutrition 0.000 claims 1
- 238000000108 ultra-filtration Methods 0.000 claims 1
- 229940116269 uric acid Drugs 0.000 claims 1
- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 claims 1
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 2
- DWAQJAXMDSEUJJ-UHFFFAOYSA-M Sodium bisulfite Chemical compound [Na+].OS([O-])=O DWAQJAXMDSEUJJ-UHFFFAOYSA-M 0.000 description 2
- LOKCTEFSRHRXRJ-UHFFFAOYSA-I dipotassium trisodium dihydrogen phosphate hydrogen phosphate dichloride Chemical compound P(=O)(O)(O)[O-].[K+].P(=O)(O)([O-])[O-].[Na+].[Na+].[Cl-].[K+].[Cl-].[Na+] LOKCTEFSRHRXRJ-UHFFFAOYSA-I 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 2
- 239000010452 phosphate Substances 0.000 description 2
- 239000002953 phosphate buffered saline Substances 0.000 description 2
- 235000010267 sodium hydrogen sulphite Nutrition 0.000 description 2
- 229910000162 sodium phosphate Inorganic materials 0.000 description 2
- 239000001488 sodium phosphate Substances 0.000 description 2
- 235000011008 sodium phosphates Nutrition 0.000 description 2
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 2
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 239000001103 potassium chloride Substances 0.000 description 1
- 235000011164 potassium chloride Nutrition 0.000 description 1
- 229960002816 potassium chloride Drugs 0.000 description 1
- 229940001607 sodium bisulfite Drugs 0.000 description 1
- 229960002668 sodium chloride Drugs 0.000 description 1
- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US12/957,821 | 2010-12-01 | ||
| US12/957,821 US9775376B2 (en) | 2010-12-01 | 2010-12-01 | Smokeless tobacco pastille and moulding process for forming smokeless tobacco products |
| US13/072,019 | 2011-03-25 | ||
| US13/072,019 US9220295B2 (en) | 2010-12-01 | 2011-03-25 | Tobacco separation process for extracting tobacco-derived materials, and associated extraction systems |
| PCT/US2011/062360 WO2012074985A1 (en) | 2010-12-01 | 2011-11-29 | Tobacco separation process for extracting tobacco-derived materials, and associated extraction systems |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2013544522A JP2013544522A (ja) | 2013-12-19 |
| JP2013544522A5 true JP2013544522A5 (enExample) | 2015-01-08 |
| JP5931904B2 JP5931904B2 (ja) | 2016-06-08 |
Family
ID=46162490
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2013542097A Active JP5931904B2 (ja) | 2010-12-01 | 2011-11-29 | タバコ由来材料を抽出するためのタバコ分離方法、および関連の抽出システム |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US9220295B2 (enExample) |
| EP (1) | EP2658406B1 (enExample) |
| JP (1) | JP5931904B2 (enExample) |
| ES (1) | ES2537210T3 (enExample) |
| WO (1) | WO2012074985A1 (enExample) |
Families Citing this family (23)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9458476B2 (en) | 2011-04-18 | 2016-10-04 | R.J. Reynolds Tobacco Company | Method for producing glycerin from tobacco |
| GB201213870D0 (en) * | 2012-08-03 | 2012-09-19 | British American Tobacco Co | Tobacco extract, preparation thereof |
| US9289011B2 (en) | 2013-03-07 | 2016-03-22 | R.J. Reynolds Tobacco Company | Method for producing lutein from tobacco |
| US9301544B2 (en) | 2013-03-14 | 2016-04-05 | R.J. Reynolds Tobacco Company | Protein-enriched tobacco-derived composition |
| US9661876B2 (en) | 2013-03-14 | 2017-05-30 | R.J. Reynolds Tobacco Company | Sugar-enriched extract derived from tobacco |
| US9175052B2 (en) | 2013-05-17 | 2015-11-03 | R.J. Reynolds Tobacco Company | Tobacco-derived protein compositions |
| US20140356295A1 (en) | 2013-06-03 | 2014-12-04 | R.J. Reynolds Tobacco Company | Cosmetic compositions comprising tobacco seed-derived component |
| US10357054B2 (en) * | 2013-10-16 | 2019-07-23 | R.J. Reynolds Tobacco Company | Smokeless tobacco pastille |
| US9265284B2 (en) | 2014-01-17 | 2016-02-23 | R.J. Reynolds Tobacco Company | Process for producing flavorants and related materials |
| SE538741C2 (sv) * | 2014-04-04 | 2016-11-08 | X-International Aps | Tobaksråvara |
| US11080739B2 (en) | 2014-04-25 | 2021-08-03 | R.J. Reynolds Tobacco Company | Data translator |
| US10881133B2 (en) | 2015-04-16 | 2021-01-05 | R.J. Reynolds Tobacco Company | Tobacco-derived cellulosic sugar |
| US11612183B2 (en) | 2015-12-10 | 2023-03-28 | R.J. Reynolds Tobacco Company | Protein-enriched tobacco composition |
| US10499684B2 (en) | 2016-01-28 | 2019-12-10 | R.J. Reynolds Tobacco Company | Tobacco-derived flavorants |
| US11154087B2 (en) | 2016-02-02 | 2021-10-26 | R.J. Reynolds Tobacco Company | Method for preparing flavorful compounds isolated from black liquor and products incorporating the flavorful compounds |
| US20180103680A1 (en) * | 2016-10-18 | 2018-04-19 | Altria Client Services Llc | Methods and systems for improving stability of the pre-vapor formulation of an e-vaping device |
| US11091446B2 (en) | 2017-03-24 | 2021-08-17 | R.J. Reynolds Tobacco Company | Methods of selectively forming substituted pyrazines |
| US10757964B2 (en) | 2017-07-20 | 2020-09-01 | R.J. Reynolds Tobacco Company | Purification of tobacco-derived protein compositions |
| CN108283329B (zh) * | 2018-01-25 | 2021-02-02 | 云南中烟工业有限责任公司 | 一种从烟草废料中提取多酚类化合物的方法和应用 |
| BR112021014081A2 (pt) | 2019-01-18 | 2021-09-21 | R. J. Reynolds Tobacco Company | Purificação de proteínas derivadas de plantas. |
| US11877590B2 (en) | 2019-03-27 | 2024-01-23 | Fiedler & Lundgren Ab | Smokeless tobacco composition |
| CN111035058B (zh) * | 2019-11-27 | 2022-07-05 | 内蒙古昆明卷烟有限责任公司 | 一种废弃烟蒂中焦油提取物的制备方法及其在卷烟中的应用 |
| EP4132266A2 (en) | 2020-04-09 | 2023-02-15 | R. J. Reynolds Tobacco Company | Methods for modulating the nicotine level in nicotiana tabacum |
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-
2011
- 2011-03-25 US US13/072,019 patent/US9220295B2/en active Active
- 2011-11-29 EP EP20110802205 patent/EP2658406B1/en active Active
- 2011-11-29 JP JP2013542097A patent/JP5931904B2/ja active Active
- 2011-11-29 WO PCT/US2011/062360 patent/WO2012074985A1/en not_active Ceased
- 2011-11-29 ES ES11802205.2T patent/ES2537210T3/es active Active
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