JP2013245351A - 防湿材 - Google Patents
防湿材 Download PDFInfo
- Publication number
- JP2013245351A JP2013245351A JP2013110070A JP2013110070A JP2013245351A JP 2013245351 A JP2013245351 A JP 2013245351A JP 2013110070 A JP2013110070 A JP 2013110070A JP 2013110070 A JP2013110070 A JP 2013110070A JP 2013245351 A JP2013245351 A JP 2013245351A
- Authority
- JP
- Japan
- Prior art keywords
- moisture
- proof material
- flame retardant
- acid
- adhesive layer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000000463 material Substances 0.000 title claims abstract description 168
- 239000003063 flame retardant Substances 0.000 claims abstract description 132
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 claims abstract description 123
- 229920000388 Polyphosphate Polymers 0.000 claims abstract description 54
- 239000001205 polyphosphate Substances 0.000 claims abstract description 54
- 235000011176 polyphosphates Nutrition 0.000 claims abstract description 54
- -1 phosphate triester Chemical class 0.000 claims abstract description 52
- 229910019142 PO4 Inorganic materials 0.000 claims abstract description 51
- 239000010452 phosphate Substances 0.000 claims abstract description 51
- 239000012790 adhesive layer Substances 0.000 claims abstract description 41
- 150000005691 triesters Chemical class 0.000 claims description 43
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 39
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 37
- 238000012360 testing method Methods 0.000 claims description 33
- 238000002485 combustion reaction Methods 0.000 claims description 23
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 18
- 229920000877 Melamine resin Polymers 0.000 claims description 13
- 229920000137 polyphosphoric acid Polymers 0.000 claims description 13
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 claims description 12
- 150000003839 salts Chemical group 0.000 claims description 11
- 239000007789 gas Substances 0.000 claims description 10
- 230000035699 permeability Effects 0.000 claims description 8
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 6
- 238000010521 absorption reaction Methods 0.000 claims description 5
- 240000009125 Myrtillocactus geometrizans Species 0.000 claims description 2
- 235000009781 Myrtillocactus geometrizans Nutrition 0.000 claims description 2
- 230000001070 adhesive effect Effects 0.000 abstract description 33
- 239000000853 adhesive Substances 0.000 abstract description 29
- 239000000758 substrate Substances 0.000 abstract description 18
- 229910052736 halogen Inorganic materials 0.000 abstract description 14
- 150000002367 halogens Chemical class 0.000 abstract description 14
- 231100000331 toxic Toxicity 0.000 abstract description 7
- 230000002588 toxic effect Effects 0.000 abstract description 7
- 239000004820 Pressure-sensitive adhesive Substances 0.000 description 43
- 239000004814 polyurethane Substances 0.000 description 40
- 229920002635 polyurethane Polymers 0.000 description 40
- 239000002253 acid Substances 0.000 description 39
- 150000003077 polyols Chemical class 0.000 description 33
- 239000005056 polyisocyanate Substances 0.000 description 26
- 229920001228 polyisocyanate Polymers 0.000 description 26
- 229920005862 polyol Polymers 0.000 description 25
- 239000010410 layer Substances 0.000 description 20
- 235000011007 phosphoric acid Nutrition 0.000 description 20
- 229920000728 polyester Polymers 0.000 description 16
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 15
- 239000003795 chemical substances by application Substances 0.000 description 15
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 13
- 239000002390 adhesive tape Substances 0.000 description 12
- 238000006243 chemical reaction Methods 0.000 description 11
- 239000004721 Polyphenylene oxide Substances 0.000 description 10
- 229920000570 polyether Polymers 0.000 description 10
- 229920006264 polyurethane film Polymers 0.000 description 10
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 9
- 125000003118 aryl group Chemical group 0.000 description 9
- 239000000835 fiber Substances 0.000 description 9
- 230000000694 effects Effects 0.000 description 8
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 8
- 239000012948 isocyanate Substances 0.000 description 8
- 238000000034 method Methods 0.000 description 8
- 239000000203 mixture Substances 0.000 description 8
- 150000001875 compounds Chemical class 0.000 description 7
- 239000002985 plastic film Substances 0.000 description 7
- 229920001296 polysiloxane Polymers 0.000 description 7
- DZAUWHJDUNRCTF-UHFFFAOYSA-N 3-(3,4-dihydroxyphenyl)propanoic acid Chemical compound OC(=O)CCC1=CC=C(O)C(O)=C1 DZAUWHJDUNRCTF-UHFFFAOYSA-N 0.000 description 6
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 6
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 6
- BDJRBEYXGGNYIS-UHFFFAOYSA-N nonanedioic acid Chemical compound OC(=O)CCCCCCCC(O)=O BDJRBEYXGGNYIS-UHFFFAOYSA-N 0.000 description 6
- 230000000737 periodic effect Effects 0.000 description 6
- 229920006255 plastic film Polymers 0.000 description 6
- 229920005906 polyester polyol Polymers 0.000 description 6
- CXMXRPHRNRROMY-UHFFFAOYSA-N sebacic acid Chemical compound OC(=O)CCCCCCCCC(O)=O CXMXRPHRNRROMY-UHFFFAOYSA-N 0.000 description 6
- 150000007513 acids Chemical class 0.000 description 5
- 125000001931 aliphatic group Chemical group 0.000 description 5
- 150000007974 melamines Chemical class 0.000 description 5
- 239000000123 paper Substances 0.000 description 5
- 229920000139 polyethylene terephthalate Polymers 0.000 description 5
- 239000005020 polyethylene terephthalate Substances 0.000 description 5
- JVYDLYGCSIHCMR-UHFFFAOYSA-N 2,2-bis(hydroxymethyl)butanoic acid Chemical compound CCC(CO)(CO)C(O)=O JVYDLYGCSIHCMR-UHFFFAOYSA-N 0.000 description 4
- GLDQAMYCGOIJDV-UHFFFAOYSA-N 2,3-dihydroxybenzoic acid Chemical compound OC(=O)C1=CC=CC(O)=C1O GLDQAMYCGOIJDV-UHFFFAOYSA-N 0.000 description 4
- WXTMDXOMEHJXQO-UHFFFAOYSA-N 2,5-dihydroxybenzoic acid Chemical compound OC(=O)C1=CC(O)=CC=C1O WXTMDXOMEHJXQO-UHFFFAOYSA-N 0.000 description 4
- YZEZMSPGIPTEBA-UHFFFAOYSA-N 2-n-(4,6-diamino-1,3,5-triazin-2-yl)-1,3,5-triazine-2,4,6-triamine Chemical compound NC1=NC(N)=NC(NC=2N=C(N)N=C(N)N=2)=N1 YZEZMSPGIPTEBA-UHFFFAOYSA-N 0.000 description 4
- CFFZDZCDUFSOFZ-UHFFFAOYSA-N 3,4-Dihydroxy-phenylacetic acid Chemical compound OC(=O)CC1=CC=C(O)C(O)=C1 CFFZDZCDUFSOFZ-UHFFFAOYSA-N 0.000 description 4
- YQUVCSBJEUQKSH-UHFFFAOYSA-N 3,4-dihydroxybenzoic acid Chemical compound OC(=O)C1=CC=C(O)C(O)=C1 YQUVCSBJEUQKSH-UHFFFAOYSA-N 0.000 description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 4
- YSMRWXYRXBRSND-UHFFFAOYSA-N TOTP Chemical compound CC1=CC=CC=C1OP(=O)(OC=1C(=CC=CC=1)C)OC1=CC=CC=C1C YSMRWXYRXBRSND-UHFFFAOYSA-N 0.000 description 4
- WERYXYBDKMZEQL-UHFFFAOYSA-N butane-1,4-diol Chemical compound OCCCCO WERYXYBDKMZEQL-UHFFFAOYSA-N 0.000 description 4
- 125000005442 diisocyanate group Chemical group 0.000 description 4
- 238000011156 evaluation Methods 0.000 description 4
- IGMNYECMUMZDDF-UHFFFAOYSA-N homogentisic acid Chemical compound OC(=O)CC1=CC(O)=CC=C1O IGMNYECMUMZDDF-UHFFFAOYSA-N 0.000 description 4
- YSRVJVDFHZYRPA-UHFFFAOYSA-N melem Chemical compound NC1=NC(N23)=NC(N)=NC2=NC(N)=NC3=N1 YSRVJVDFHZYRPA-UHFFFAOYSA-N 0.000 description 4
- SXFJDZNJHVPHPH-UHFFFAOYSA-N 3-methylpentane-1,5-diol Chemical compound OCCC(C)CCO SXFJDZNJHVPHPH-UHFFFAOYSA-N 0.000 description 3
- UPMLOUAZCHDJJD-UHFFFAOYSA-N 4,4'-Diphenylmethane Diisocyanate Chemical compound C1=CC(N=C=O)=CC=C1CC1=CC=C(N=C=O)C=C1 UPMLOUAZCHDJJD-UHFFFAOYSA-N 0.000 description 3
- 239000004698 Polyethylene Substances 0.000 description 3
- 239000004743 Polypropylene Substances 0.000 description 3
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric Acid Chemical compound [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 3
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 3
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 description 3
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 3
- 239000001361 adipic acid Substances 0.000 description 3
- 235000011037 adipic acid Nutrition 0.000 description 3
- 125000002723 alicyclic group Chemical group 0.000 description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
- 229920001577 copolymer Polymers 0.000 description 3
- RBNPOMFGQQGHHO-UHFFFAOYSA-N glyceric acid Chemical compound OCC(O)C(O)=O RBNPOMFGQQGHHO-UHFFFAOYSA-N 0.000 description 3
- ZFSLODLOARCGLH-UHFFFAOYSA-N isocyanuric acid Chemical compound OC1=NC(O)=NC(O)=N1 ZFSLODLOARCGLH-UHFFFAOYSA-N 0.000 description 3
- NIMLQBUJDJZYEJ-UHFFFAOYSA-N isophorone diisocyanate Chemical compound CC1(C)CC(N=C=O)CC(C)(CN=C=O)C1 NIMLQBUJDJZYEJ-UHFFFAOYSA-N 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 150000002736 metal compounds Chemical class 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 description 3
- 239000001301 oxygen Substances 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
- 229920000573 polyethylene Polymers 0.000 description 3
- 229920001155 polypropylene Polymers 0.000 description 3
- DVKJHBMWWAPEIU-UHFFFAOYSA-N toluene 2,4-diisocyanate Chemical compound CC1=CC=C(N=C=O)C=C1N=C=O DVKJHBMWWAPEIU-UHFFFAOYSA-N 0.000 description 3
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 2
- OTOIIPJYVQJATP-BYPYZUCNSA-N (R)-pantoic acid Chemical compound OCC(C)(C)[C@@H](O)C(O)=O OTOIIPJYVQJATP-BYPYZUCNSA-N 0.000 description 2
- FKTHNVSLHLHISI-UHFFFAOYSA-N 1,2-bis(isocyanatomethyl)benzene Chemical compound O=C=NCC1=CC=CC=C1CN=C=O FKTHNVSLHLHISI-UHFFFAOYSA-N 0.000 description 2
- VGHSXKTVMPXHNG-UHFFFAOYSA-N 1,3-diisocyanatobenzene Chemical compound O=C=NC1=CC=CC(N=C=O)=C1 VGHSXKTVMPXHNG-UHFFFAOYSA-N 0.000 description 2
- VOJUXHHACRXLTD-UHFFFAOYSA-N 1,4-dihydroxy-2-naphthoic acid Chemical compound C1=CC=CC2=C(O)C(C(=O)O)=CC(O)=C21 VOJUXHHACRXLTD-UHFFFAOYSA-N 0.000 description 2
- ALQLPWJFHRMHIU-UHFFFAOYSA-N 1,4-diisocyanatobenzene Chemical compound O=C=NC1=CC=C(N=C=O)C=C1 ALQLPWJFHRMHIU-UHFFFAOYSA-N 0.000 description 2
- CDMDQYCEEKCBGR-UHFFFAOYSA-N 1,4-diisocyanatocyclohexane Chemical compound O=C=NC1CCC(N=C=O)CC1 CDMDQYCEEKCBGR-UHFFFAOYSA-N 0.000 description 2
- ALVZNPYWJMLXKV-UHFFFAOYSA-N 1,9-Nonanediol Chemical compound OCCCCCCCCCO ALVZNPYWJMLXKV-UHFFFAOYSA-N 0.000 description 2
- PTBDIHRZYDMNKB-UHFFFAOYSA-N 2,2-Bis(hydroxymethyl)propionic acid Chemical compound OCC(C)(CO)C(O)=O PTBDIHRZYDMNKB-UHFFFAOYSA-N 0.000 description 2
- WVTQQBGZQOPSJL-UHFFFAOYSA-N 2,2-bis(hydroxymethyl)decanoic acid Chemical compound CCCCCCCCC(CO)(CO)C(O)=O WVTQQBGZQOPSJL-UHFFFAOYSA-N 0.000 description 2
- LEFFOHHXJAVELB-UHFFFAOYSA-N 2,2-bis(hydroxymethyl)dodecanoic acid Chemical compound CCCCCCCCCCC(CO)(CO)C(O)=O LEFFOHHXJAVELB-UHFFFAOYSA-N 0.000 description 2
- GHZZINSSYUWTRJ-UHFFFAOYSA-N 2,2-bis(hydroxymethyl)hexadecanoic acid Chemical compound CCCCCCCCCCCCCCC(CO)(CO)C(O)=O GHZZINSSYUWTRJ-UHFFFAOYSA-N 0.000 description 2
- TXSZYEYDDYBUSU-UHFFFAOYSA-N 2,2-bis(hydroxymethyl)hexanoic acid Chemical compound CCCCC(CO)(CO)C(O)=O TXSZYEYDDYBUSU-UHFFFAOYSA-N 0.000 description 2
- VKNBFINDVATXHU-UHFFFAOYSA-N 2,2-bis(hydroxymethyl)nonanoic acid Chemical compound CCCCCCCC(CO)(CO)C(O)=O VKNBFINDVATXHU-UHFFFAOYSA-N 0.000 description 2
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- QVCHPHNGIRHJRL-UHFFFAOYSA-N 2,2-bis(hydroxymethyl)tetradecanoic acid Chemical compound CCCCCCCCCCCCC(CO)(CO)C(O)=O QVCHPHNGIRHJRL-UHFFFAOYSA-N 0.000 description 2
- AOWPAWLEXIYETE-UHFFFAOYSA-N 2,3-Dihydroxy-2-methylbutanoic acid Chemical compound CC(O)C(C)(O)C(O)=O AOWPAWLEXIYETE-UHFFFAOYSA-N 0.000 description 2
- UIAFKZKHHVMJGS-UHFFFAOYSA-N 2,4-dihydroxybenzoic acid Chemical compound OC(=O)C1=CC=C(O)C=C1O UIAFKZKHHVMJGS-UHFFFAOYSA-N 0.000 description 2
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- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 2
- KXEISHUBUXWXGY-UHFFFAOYSA-N 2-hydroxy-2-(1-hydroxyethyl)-3-methylbutanoic acid Chemical compound CC(C)C(O)(C(C)O)C(O)=O KXEISHUBUXWXGY-UHFFFAOYSA-N 0.000 description 2
- UYEMGAFJOZZIFP-UHFFFAOYSA-N 3,5-dihydroxybenzoic acid Chemical compound OC(=O)C1=CC(O)=CC(O)=C1 UYEMGAFJOZZIFP-UHFFFAOYSA-N 0.000 description 2
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- ULMZOZMSDIOZAF-UHFFFAOYSA-N 3-hydroxy-2-(hydroxymethyl)propanoic acid Chemical compound OCC(CO)C(O)=O ULMZOZMSDIOZAF-UHFFFAOYSA-N 0.000 description 2
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- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- 239000004114 Ammonium polyphosphate Substances 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
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- 239000005057 Hexamethylene diisocyanate Substances 0.000 description 2
- 239000005058 Isophorone diisocyanate Substances 0.000 description 2
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 2
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- 238000010030 laminating Methods 0.000 description 2
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- 229910017464 nitrogen compound Inorganic materials 0.000 description 2
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- 150000002902 organometallic compounds Chemical class 0.000 description 2
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- 230000002265 prevention Effects 0.000 description 2
- 230000003449 preventive effect Effects 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
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- AYLRODJJLADBOB-QMMMGPOBSA-N methyl (2s)-2,6-diisocyanatohexanoate Chemical compound COC(=O)[C@@H](N=C=O)CCCCN=C=O AYLRODJJLADBOB-QMMMGPOBSA-N 0.000 description 1
- VOWPVJACXJNHBC-UHFFFAOYSA-N methyl diphenyl phosphate Chemical group C=1C=CC=CC=1OP(=O)(OC)OC1=CC=CC=C1 VOWPVJACXJNHBC-UHFFFAOYSA-N 0.000 description 1
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- AMKYESDOVDKZKV-UHFFFAOYSA-N o-Orsellinic acid Natural products CC1=CC(O)=CC(O)=C1C(O)=O AMKYESDOVDKZKV-UHFFFAOYSA-N 0.000 description 1
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 1
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- ACVYVLVWPXVTIT-UHFFFAOYSA-N phosphinic acid Chemical compound O[PH2]=O ACVYVLVWPXVTIT-UHFFFAOYSA-N 0.000 description 1
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- 229920001200 poly(ethylene-vinyl acetate) Polymers 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
- 239000005023 polychlorotrifluoroethylene (PCTFE) polymer Substances 0.000 description 1
- 229920006267 polyester film Polymers 0.000 description 1
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- 230000000379 polymerizing effect Effects 0.000 description 1
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- 229920000166 polytrimethylene carbonate Polymers 0.000 description 1
- 229920002620 polyvinyl fluoride Polymers 0.000 description 1
- 239000005033 polyvinylidene chloride Substances 0.000 description 1
- 229920002981 polyvinylidene fluoride Polymers 0.000 description 1
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- 238000007151 ring opening polymerisation reaction Methods 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 229920001059 synthetic polymer Polymers 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 239000000057 synthetic resin Substances 0.000 description 1
- 235000002906 tartaric acid Nutrition 0.000 description 1
- 239000011975 tartaric acid Substances 0.000 description 1
- ISIJQEHRDSCQIU-UHFFFAOYSA-N tert-butyl 2,7-diazaspiro[4.5]decane-7-carboxylate Chemical compound C1N(C(=O)OC(C)(C)C)CCCC11CNCC1 ISIJQEHRDSCQIU-UHFFFAOYSA-N 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
- 229920002803 thermoplastic polyurethane Polymers 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- 150000003918 triazines Chemical class 0.000 description 1
- STCOOQWBFONSKY-UHFFFAOYSA-N tributyl phosphate Chemical compound CCCCOP(=O)(OCCCC)OCCCC STCOOQWBFONSKY-UHFFFAOYSA-N 0.000 description 1
- DQWPFSLDHJDLRL-UHFFFAOYSA-N triethyl phosphate Chemical compound CCOP(=O)(OCC)OCC DQWPFSLDHJDLRL-UHFFFAOYSA-N 0.000 description 1
- WVLBCYQITXONBZ-UHFFFAOYSA-N trimethyl phosphate Chemical compound COP(=O)(OC)OC WVLBCYQITXONBZ-UHFFFAOYSA-N 0.000 description 1
- XZZNDPSIHUTMOC-UHFFFAOYSA-N triphenyl phosphate Chemical compound C=1C=CC=CC=1OP(OC=1C=CC=CC=1)(=O)OC1=CC=CC=C1 XZZNDPSIHUTMOC-UHFFFAOYSA-N 0.000 description 1
- UNXRWKVEANCORM-UHFFFAOYSA-N triphosphoric acid Chemical compound OP(O)(=O)OP(O)(=O)OP(O)(O)=O UNXRWKVEANCORM-UHFFFAOYSA-N 0.000 description 1
- 229940048102 triphosphoric acid Drugs 0.000 description 1
- OXFUXNFMHFCELM-UHFFFAOYSA-N tripropan-2-yl phosphate Chemical compound CC(C)OP(=O)(OC(C)C)OC(C)C OXFUXNFMHFCELM-UHFFFAOYSA-N 0.000 description 1
- RXPQRKFMDQNODS-UHFFFAOYSA-N tripropyl phosphate Chemical compound CCCOP(=O)(OCCC)OCCC RXPQRKFMDQNODS-UHFFFAOYSA-N 0.000 description 1
- LIPMRGQQBZJCTM-UHFFFAOYSA-N tris(2-propan-2-ylphenyl) phosphate Chemical compound CC(C)C1=CC=CC=C1OP(=O)(OC=1C(=CC=CC=1)C(C)C)OC1=CC=CC=C1C(C)C LIPMRGQQBZJCTM-UHFFFAOYSA-N 0.000 description 1
- BIKXLKXABVUSMH-UHFFFAOYSA-N trizinc;diborate Chemical compound [Zn+2].[Zn+2].[Zn+2].[O-]B([O-])[O-].[O-]B([O-])[O-] BIKXLKXABVUSMH-UHFFFAOYSA-N 0.000 description 1
- ZXYAAVBXHKCJJB-UHFFFAOYSA-N uracil-5-carboxylic acid Chemical compound OC(=O)C1=CNC(=O)NC1=O ZXYAAVBXHKCJJB-UHFFFAOYSA-N 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 239000013585 weight reducing agent Substances 0.000 description 1
- 239000002759 woven fabric Substances 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
- 238000004383 yellowing Methods 0.000 description 1
- 239000010457 zeolite Substances 0.000 description 1
- 239000011787 zinc oxide Substances 0.000 description 1
- 229910052984 zinc sulfide Inorganic materials 0.000 description 1
- BNEMLSQAJOPTGK-UHFFFAOYSA-N zinc;dioxido(oxo)tin Chemical compound [Zn+2].[O-][Sn]([O-])=O BNEMLSQAJOPTGK-UHFFFAOYSA-N 0.000 description 1
- DRDVZXDWVBGGMH-UHFFFAOYSA-N zinc;sulfide Chemical compound [S-2].[Zn+2] DRDVZXDWVBGGMH-UHFFFAOYSA-N 0.000 description 1
Classifications
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- E—FIXED CONSTRUCTIONS
- E04—BUILDING
- E04F—FINISHING WORK ON BUILDINGS, e.g. STAIRS, FLOORS
- E04F13/00—Coverings or linings, e.g. for walls or ceilings
- E04F13/07—Coverings or linings, e.g. for walls or ceilings composed of covering or lining elements; Sub-structures therefor; Fastening means therefor
- E04F13/072—Coverings or linings, e.g. for walls or ceilings composed of covering or lining elements; Sub-structures therefor; Fastening means therefor composed of specially adapted, structured or shaped covering or lining elements
- E04F13/075—Coverings or linings, e.g. for walls or ceilings composed of covering or lining elements; Sub-structures therefor; Fastening means therefor composed of specially adapted, structured or shaped covering or lining elements for insulation or surface protection, e.g. against noise or impact
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J9/00—Adhesives characterised by their physical nature or the effects produced, e.g. glue sticks
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J7/00—Adhesives in the form of films or foils
- C09J7/20—Adhesives in the form of films or foils characterised by their carriers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/16—Nitrogen-containing compounds
- C08K5/34—Heterocyclic compounds having nitrogen in the ring
- C08K5/3467—Heterocyclic compounds having nitrogen in the ring having more than two nitrogen atoms in the ring
- C08K5/3477—Six-membered rings
- C08K5/3492—Triazines
- C08K5/34928—Salts
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/49—Phosphorus-containing compounds
- C08K5/51—Phosphorus bound to oxygen
- C08K5/52—Phosphorus bound to oxygen only
- C08K5/521—Esters of phosphoric acids, e.g. of H3PO4
- C08K5/523—Esters of phosphoric acids, e.g. of H3PO4 with hydroxyaryl compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2301/00—Additional features of adhesives in the form of films or foils
- C09J2301/40—Additional features of adhesives in the form of films or foils characterized by the presence of essential components
- C09J2301/408—Additional features of adhesives in the form of films or foils characterized by the presence of essential components additives as essential feature of the adhesive layer
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2301/00—Additional features of adhesives in the form of films or foils
- C09J2301/40—Additional features of adhesives in the form of films or foils characterized by the presence of essential components
- C09J2301/41—Additional features of adhesives in the form of films or foils characterized by the presence of essential components additives as essential feature of the carrier layer
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/28—Web or sheet containing structurally defined element or component and having an adhesive outermost layer
- Y10T428/2852—Adhesive compositions
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Architecture (AREA)
- Civil Engineering (AREA)
- Structural Engineering (AREA)
- Laminated Bodies (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Fireproofing Substances (AREA)
- Adhesive Tapes (AREA)
Abstract
【解決手段】基材と、該基材の少なくとも片面に形成された粘着層とを有する防湿材であり、ポリリン酸塩系難燃剤及びリン酸トリエステル系難燃剤を、それぞれ、基材及び粘着層の少なくとも一方に含有させてなる、防湿材。
【選択図】なし
Description
(1)基材と、該基材の少なくとも片面に形成された粘着層とを有する防湿材であって、ポリリン酸塩系難燃剤及びリン酸トリエステル系難燃剤が、それぞれ、基材及び粘着層の少なくとも一方に含有されてなることを特徴とする、防湿材。
(2)ポリリン酸塩系難燃剤が、ポリリン酸と含窒素複素環式化合物との塩である、上記(1)記載の防湿材。
(3)ポリリン酸塩系難燃剤が、ポリリン酸とメラミンとの塩である、上記(1)記載の防湿材。
(4)リン酸トリエステル系難燃剤が、芳香族リン酸トリエステルである、上記(1)記載の防湿材。
(5)ポリリン酸塩系難燃剤の含有量が防湿材全体に対して5〜50重量%であり、リン酸トリエステル系難燃剤の含有量が防湿材全体に対して5〜30重量%である、上記(1)記載の防湿材。
(6)ポリリン酸塩系難燃剤およびリン酸トリエステル系難燃剤が少なくとも粘着層に含有されている、上記(1)記載の防湿材。
(7)粘着層中のポリリン酸塩系難燃剤の含有量が粘着層全体当たり5〜40重量%であり、粘着層中のリン酸トリエステル系難燃剤の含有量が粘着層全体当たり5〜20重量%である、上記(6)記載の防湿材。
(8)基材にポリリン酸塩系難燃剤およびリン酸トリエステル系難燃剤が含有されていない、上記(7)記載の防湿材。
(9)下記の燃焼試験における燃焼時間が15秒以下、燃焼長さが8インチ以下である、上記(1)記載の防湿材
[燃焼試験]
防湿材とフロアーパネルを貼り合わせた平面サイズが3インチ×12インチの試験サンプルを、その長さ方向の軸線が鉛直方向と平行となるようにセットし、該試験サンプルの鉛直下方側に設置した、口径(内径)が10mmのブンゼン或いはTirrillバーナーから、メタンガスによる、鉛直方向へ出炎する長さ38mmの黄色チップのない青色炎を、前記試験サンプルの下端中央部の防湿材に防湿材の下端が炎の長さの1/2(19mm)の高さになる状態で12秒間接炎し、炎を離してからの燃焼時間を計測する。
(10)水分透過率が9.0%以下である、上記(1)記載の防湿材。
(11)水分吸収率が1.0%以下である、上記(1)記載の防湿材。
(12)引張強度が15000psi以下である、上記(1)記載の防湿材。
(13)破断伸度が1500%以下である、上記(1)記載の防湿材。
図1に示されるように、本発明の防湿材1は、基材2と、該基材2の少なくとも片面に形成された粘着層3とを有する。そして、本発明の防湿材1は、ポリリン酸塩系難燃剤及びリン酸トリエステル系難燃剤を含有する。
第1態様:基材2にポリリン酸塩系難燃剤及びリン酸トリエステル系難燃剤を含有させ、粘着層3にはポリリン酸塩系難燃剤及びリン酸トリエステル系難燃剤を含有させない。
本発明の防湿材1において、基材2の材質は特に限定されないが、例えば、ポリエステル(例えば、ポリエチレンテレフタレート(PET)等)、ナイロン、ポリオレフィン(ポリ塩化ビニル、ポリ塩化ビニリデン、ポリエチレン、ポリプロピレン、リアクターTPO(Thermoplastic Olefin)、エチレン−酢酸ビニル共重合体等)、ポリウレタン、フッ素樹脂(ポリテトラフルオロエチレン等)及びアイオノマー樹脂からなる群から選ばれる1種又は2種以上のプラスチックからなるフィルム(単層フィルム)又は金属箔、或いは、これらから選ばれる2つ以上を積層したラミネートフィルム等が挙げられる。これらのフィルムは中実フィルム(無孔フィルム)の状態で使用する他、機械的に穿孔処理を施した有孔フィルムにして使用してもよい。また、ポリエステル(例えば、ポリエチレンテレフタレート(PET)等)等の合成高分子繊維、天然繊維(綿、麻等)、金属繊維及びガラス繊維から選ばれる1種または2種以上の繊維を用いた編布、織布、不織布等の繊維製シート(単層シート、2層以上の積層シート)、かかる繊維製シートの1種又は2種以上を前述のプラスチックフィルムに積層した積層シートも基材1として使用することができる。
本発明の防湿材1の粘着層3に使用する粘着剤は特に限定されず、例えば、ポリウレタン粘着剤、アクリル系粘着剤、ゴム系粘着剤、シリコーン系粘着剤等を用いることができる。これらの中でも、難燃性、再剥離性、長期耐久性などの観点から、ポリウレタン粘着剤が好ましい。
本発明では、ポリリン酸塩系難燃剤及びリン酸トリエステル系難燃剤を併用する。
ポリリン酸塩系難燃剤としては、難燃剤として使用することが可能な公知のポリリン酸塩を特に制限なく使用できる。例えば、ポリリン酸と、周期律表IA族〜IVB族の金属、アンモニア、脂肪族アミン、含窒素複素環式化合物等との塩が好適である。代表的な塩として、金属塩としてリチウム塩、ナトリウム塩、カルシウム塩、バリウム塩、鉄(II)塩、鉄(III)塩、アルミニウム塩など、アンモニウム塩、脂肪族アミン塩としてメチルアミン塩、エチルアミン塩、ジエチルアミン塩、トリエチルアミン塩、エチレンジアミン塩、ピペラジン塩などがあり、含窒素複素環式化合物塩としてはピリジン塩、メラミン塩などが挙げられる。
リン酸トリエステル系難燃剤としては、難燃剤として使用することが可能な公知のリン酸トリエステル化合物を制限なく使用できる。リン酸エステル化合物はリン酸とアルコール化合物又はフェノール化合物のエステル化合物であれば特に制限はなく、脂肪族リン酸エステル、芳香族リン酸エステル及び脂肪族−芳香族リン酸エステルのいずれであってもよい。例えば、脂肪族リン酸エステルとしては、トリメチルホスフェート、トリエチルホスフェート、トリプロピルホスフェート、トリイソプロピルホスフェート、トリブチルホスフェート、トリイソブチルホスフェート、ペンタエリスリトールホスフェート等が挙げられ、芳香族リン酸エステルとしては、トリフェニルホスフェート、トリクレジルホスフェート、トリキシリルホスフェート、ジフェニルクレジルホスフェート、トリ(イソプロピルフェニル)ホスフェート等のリン酸トリC6−20アリールエステルなどが挙げられ、脂肪族−芳香族リン酸エステルとしては、メチルジフェニルホスフェート、フェニルジエチルホスフェート、ジフェニルペンタエリスリトールジホスフェート、ジクレジルペンタエリスリトールジホスフェート、ジキシリルペンタエリスリトールジホスフェート等などが挙げられる。
本発明の防湿材には、使用時まで粘着層3の表面保護、粘着層の粘着力の低下抑制などの観点から、粘着層3に剥離ライナーを積層してもよい。かかる剥離ライナーは防湿材をフロアーパネルなどの被貼付面に貼付する際に剥離される。
図5に示すように、防湿材1とフロアーパネル10を貼り合わせた平面サイズが3インチ×12インチの試験サンプルSを、その長さ方向の軸線が鉛直方向と平行となるようにセットし、該試験サンプルSの鉛直下方側に設置した、口径(内径)が3/8インチ(10mm)のブンゼン或いはTirrillバーナー20から、メタンガスによる、鉛直方向へ出炎する長さ38mmの黄色チップのない青色炎21を、前記試験サンプルSの下端中央部の防湿材1に防湿材の下端1Aが炎の長さの1/2(19mm)の高さになる状態で12秒間接炎し、炎を離してからの燃焼時間および燃焼長さを計測する。
図4に示すように、幅1インチ、長さ40cmのテープTを準備し、テープTの一方の端部(長さ1インチ部分)を被着体50に貼り合わせ、他方の端部をテープの軸線方向に2kgの力で引っ張りながら、テープTの長さ30cm分を被着体50に貼り合わせ、被着体50に貼付されたテープTの最小幅部の幅(W)を測定する。最小幅部の幅(W)の試験前のテープの幅(1インチ)対する減少の程度小さい程、貼付時直線性が優れている。
実施例及び比較例の防湿材の評価試験は次の方法で行った。
重量:24±2時間、75±5°Fで放置後、平面形状が2×3インチのサイズの矩形からなるサンプルの重量を最小目盛り0.001gの量りで測定し、5つのサンプルの平均値を採用した。
厚み:最小目盛りが0.0005インチで7.0〜9.0psiの圧力が測定物にかかるダイヤルシックネスゲージで測定した。
ASTM−D1000に準拠して180°ピール強度を測定し、該180°ピール強度を接着力とした。被着体にはハニカム被着体(BMS4−17)を使用した。接着力の好適範囲は1.3〜2.5lbs/inchである。
周期表の上に防湿材を重ね、その上から目視にて周期律表の原子記号、原子量の視認性によって5段階の評価をした。なお、周期律表はLos Alamos National Laboratory chemistry division(http://periodic.lanl.gov/downloads.shtml)から、ダウンロードしたもの(白黒版)を、レターサイズで印刷して使用した。
ランク5:原子記号および原子量をクリアーに判読できる。
ランク4:原子記号は困難なく判読できるが、原子量はかろうじて判読できる。
ランク3:原子記号はかろうじて判読できるが、原子量は判別不能。
ランク2:原子記号はかろうじて視認できるが、残りは判別不能。
ランク1:周期表の全情報はほとんど判別不能。
ASTM D3759に準拠。
詳細には、12.5mmのサンプル幅で、チャック間距離50mm、引張速度50mm/minの条件にて測定し、引張強度、破断伸度を測定した。
一方向ガラス繊維で強化されたエポキシフェーシングがアラミドハニカムコアに結合して作られた軽量航空機のフロアーパネルであるGillfloor 4417A Panel(M.C. Gill Corporation製、商品名)を3インチ×12インチのサイズにカットし、これに3インチ×12インチのサイズにカットした試料(防湿材)を貼り合わせ、2kgfのローラーで一往復させ、室温で24時間放置して、試験サンプルを作製した。
燃焼時間が15秒以内であれば合格(○)。
ASTM D−3833に準拠。
詳細には、ASTM指定の容器(フランジの外側寸法が50.8mm×152.4mm、内側寸法が25.4mm×101.6mm、容器本体の寸法が25.4mm×101.6mm×38.1mm(深さ))にCaCl2を一杯になる3mm手前くらいの深さまで入れる。フランジの外側寸法と同じサイズにカットしたサンプルをシワや泡が入らないようにフランジに貼り合わせる。38℃×95%のオーブンに24時間放置して、取り出し、室温で15分間放置後、重さを測定する(W1)。再び72時間、38℃×95%のオーブンに放置して、取り出し、15分室温で放置後、再度重さを測定する(W2)。そして、以下の式[I]により、WVTR(水分透過率)を算出する。
式中、Tは暴露時間(72時間)、Aは容器の開口面積(4inch2)である。
BSM 8−346に準拠。
詳細には、1.5×4インチの2024のアルミニウムパネルに1×4インチのサンプルを貼り付けて、24時間、75°F、50%の湿度に保管し、初期の重さを測定する。その後、120°F×95%の湿度に7日間入れて、取り出し、ガーゼで余分な水分などをふき取ったあと、取り出して30分以内に重さを測定し、初期と比較して、水分吸収率を測定した。
前述の方法(図4)にて試験・評価を行った。
被着体50にガラスプレートを使用し、テープの端部(長さ1インチ部分)の中心部分にばね秤51を係着してテープを2kgの力で引っ張った。試験は室温下で実施した。最小幅部の幅(W)が23mmより大きい場合は良好(○)、23mm以下の場合は不良(×)とした。
・ポリエステル系ポリウレタン粘着剤
ポリエステル系ポリウレタン(東洋インキ株式会社製のSH101)100重量部に、イソシアネート系硬化剤(東洋インキ株式会社製のT−501B)を2重量部配合し、粘着剤を作製した。粘着剤の硬化条件は120℃×2分に設定した。
実施例の基材にはアメリカンポリフィルム社(American Polyfilm, Inc.)製のポリエステル系ポリウレタンフィルム基材である、厚みが4milのVLM−4001、厚みが7milのVLM3301、厚みが10milのVLM3301の3種を用意した。
(1)ポリリン酸塩系難燃剤
ブーデンハイム社(Chemische Fabrik Budenheim)製、Budit3141(オルトリン酸を構成単位とするポリリン酸のメラミン塩)
(2)リン酸トリエステル系難燃剤
トリクレジルホスフェート(TCP)
厚み15milの基材の片面に厚み4milの粘着層を形成した防湿材を作製した。2種類の難燃剤を粘着層に含有させ、それぞれの難燃剤の含有量を変更した。
厚み15milの基材の片面に厚み4milの粘着層を形成した防湿材を作製した。比較例1は難燃剤を含有さず、比較例2〜6は1種類の難燃剤を粘着層に含有させた。
表1、2中のTCPおよびBudit3141の含有量は粘着層全体当たりの含有量であり、括弧内が防湿材全体当たりの含有量である。
2 基材
3 粘着層
10 フロアーパネル
11 カーペット
12 両面粘着テープまたはシート
50 被着体
51 ばね秤
T テープ
Claims (13)
- 基材と、該基材の少なくとも片面に形成された粘着層とを有する防湿材であって、ポリリン酸塩系難燃剤及びリン酸トリエステル系難燃剤が、それぞれ、基材及び粘着層の少なくとも一方に含有されてなることを特徴とする、防湿材。
- ポリリン酸塩系難燃剤が、ポリリン酸と含窒素複素環式化合物との塩である、請求項1記載の防湿材。
- ポリリン酸塩系難燃剤が、ポリリン酸とメラミンとの塩である、請求項1記載の防湿材。
- リン酸トリエステル系難燃剤が、芳香族リン酸トリエステルである、請求項1記載の防湿材。
- ポリリン酸塩系難燃剤の含有量が防湿材全体に対して5〜50重量%であり、リン酸トリエステル系難燃剤の含有量が防湿材全体に対して5〜30重量%である、請求項1記載の防湿材。
- ポリリン酸塩系難燃剤およびリン酸トリエステル系難燃剤が少なくとも粘着層に含有されている、請求項1記載の防湿材。
- 粘着層中のポリリン酸塩系難燃剤の含有量が粘着層全体当たり5〜40重量%であり、粘着層中のリン酸トリエステル系難燃剤の含有量が粘着層全体当たり5〜20重量%である、請求項6記載の防湿材。
- 基材にポリリン酸塩系難燃剤およびリン酸トリエステル系難燃剤が含有されていない、請求項7記載の防湿材。
- 下記の燃焼試験における燃焼時間が15秒以下、燃焼長さが8インチ以下である、請求項1記載の防湿材
[燃焼試験]
防湿材とフロアーパネルを貼り合わせた平面サイズが3インチ×12インチの試験サンプルを、その長さ方向の軸線が鉛直方向と平行となるようにセットし、該試験サンプルの鉛直下方側に設置した、口径(内径)が10mmのブンゼン或いはTirrillバーナーから、メタンガスによる、鉛直方向へ出炎する長さ38mmの黄色チップのない青色炎を、前記試験サンプルの下端中央部の防湿材に防湿材の下端が炎の長さの1/2(19mm)の高さになる状態で12秒間接炎し、炎を離してからの燃焼時間を計測する。 - 水分透過率が9.0%以下である、請求項1記載の防湿材。
- 水分吸収率が1.0%以下である、請求項1記載の防湿材。
- 引張強度が15000psi以下である、請求項1記載の防湿材。
- 破断伸度が1500%以下である、請求項1記載の防湿材。
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JP2015143353A (ja) * | 2013-12-27 | 2015-08-06 | 日本合成化学工業株式会社 | 航空機部材固定用両面粘着テープ |
JP2019522071A (ja) * | 2016-05-23 | 2019-08-08 | 日東電工株式会社 | 防湿材料 |
JP7156951B2 (ja) | 2016-05-23 | 2022-10-19 | 日東電工株式会社 | 防湿材料 |
WO2019039430A1 (ja) * | 2017-08-21 | 2019-02-28 | 株式会社寺岡製作所 | 難燃性粘着テープ |
JPWO2019039430A1 (ja) * | 2017-08-21 | 2020-07-30 | 株式会社寺岡製作所 | 難燃性粘着テープ |
JP2022012087A (ja) * | 2020-06-30 | 2022-01-17 | 積水フーラー株式会社 | 湿気硬化型ホットメルト接着剤 |
JP7470406B2 (ja) | 2020-06-30 | 2024-04-18 | 積水フーラー株式会社 | 湿気硬化型ホットメルト接着剤 |
Also Published As
Publication number | Publication date |
---|---|
SG195503A1 (en) | 2013-12-30 |
CN103421442A (zh) | 2013-12-04 |
EP2666836A3 (en) | 2017-03-15 |
EP2666836A2 (en) | 2013-11-27 |
CN103421442B (zh) | 2017-04-19 |
JP6088904B2 (ja) | 2017-03-01 |
US20130337261A1 (en) | 2013-12-19 |
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