JP2013085553A - 味と香味を持続的に維持するチューインガム組成物 - Google Patents
味と香味を持続的に維持するチューインガム組成物 Download PDFInfo
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- JP2013085553A JP2013085553A JP2012231990A JP2012231990A JP2013085553A JP 2013085553 A JP2013085553 A JP 2013085553A JP 2012231990 A JP2012231990 A JP 2012231990A JP 2012231990 A JP2012231990 A JP 2012231990A JP 2013085553 A JP2013085553 A JP 2013085553A
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- Prior art keywords
- chewing gum
- taste
- additive
- gum composition
- gum
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- A—HUMAN NECESSITIES
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Abstract
【解決手段】本発明によるチューインガム組成物は、味または香りを発現させる酸味剤、甘味剤、香料のような添加物をポリビニールアセテートと配合して硬い添加剤の粉末を製造し、既存のガム組成物に添加することにより、長時間咀嚼しても味と香りを持続的に維持することを特徴とする。
【選択図】なし
Description
したがって、本発明者らは咀嚼初期に味わえる味と香りをガムを噛む際に持続的に維持できる新たな組成のチューインガムを開発することで本発明を完成した。
本発明のチューインガム組成物は、通常のガムベースと添加物からなり、前記添加物をポリビニールアセテートなどと配合して粉砕した粉末状添加物を製造して使用することにその特徴がある。
下記表1の組成で粉末状添加物を製造した。
具体的には、ポリビニールアセテートに添加物を混合し、高温でミキシングした後、充分に冷まし、30〜100メッシュの一定の粒度に粉砕して粉末状添加物を製造した。
また、製造された粉末状添加物の粘度を測定するためにブルックフィールド粘度計(RVDV II+Pro Viscometers、Brookfield社)を用い、Disposable Sample Chamber HT−2DB、SC4−27 Thermosel spindleを用いて温度は130℃、RPMは0.1に設定し、粘度を測定して下記表1に示す。
本実施例では下記表2に示す組成からなるチューインガムの試料に前記製造例により製造した粉末状添加物を配合して通常の方法で板ガムまたはコーティングガムを製造した。
前記表2に示したチューインガムの試料に、製造例により製造した粉末状添加物を下記表3の組成比で配合して板ガムを製造した。
前記表2に示したチューインガムの組成物に、製造例により製造した粉末状添加物を配合して下記表5の組成を形成するコーティング層の試料でコーティングしてコーティングガムを製造した。
実験例1:味または香りの維持効果1
本発明により粉末状添加物を配合して製造した板状チューインガム(実施例5)の味または香りの維持効果を下記の実験方法で確認した。比較群では比較例3の板状チューインガムを選択した。
味または香りの維持効果の分析は咀嚼機械(AB FIA Odarslovs molla社のChewing Apparatuses)を用いて比較実験を行った。咀嚼機械に実施例5と比較例3により製造した板状チューインガムを入れて咀嚼させながら5分ごとに水溶液を交換し、交換した水溶液から甘味成分を測定して評価した。咀嚼機械の条件で水溶液は蒸溜水、温度は37℃、咀嚼時間は総50分で、5分ごとに水溶液を交換し、咀嚼角度は20°に設定した。5分ごとに交換される水溶液はHPLC分析により甘味成分を分析した。
2)結果
5分ごとに交換された水溶液の甘味成分をHPLCで分析した結果は下記表7に示す。
本発明により甘味剤を用いて粉末状添加物を製造して配合したチューインガムの味または香りの維持効果を(株)Sensometricsという官能調査専門機関に依頼して味の持続性を比較評価した。
1.専門パネル:Sensometrics社の味品質評価パネル60名(味評価活動期間6ケ月〜2年6ケ月)のうち、月2回以上ガムを購入したパネル8〜10名を選抜
2.消費者パネル:月2回以上ガムを購入した20代または30代の成人男女各々100名ずつ総200名を募集選抜
1.評価試料:実施例5のチューインガム
2.評価方法:時間強度テスト(Time intensity test)
3.使用基準:10点の構造化された強度基準
0点:なし 1点:非常に弱い
3点:弱い 5点:普通
7点:強い 9点:非常に強い
4.評価間隔:0点、すなわち味がない(何の味も感じられない)と感じる時点から2回程度(2分)の追加評価後にテストを終了する。しかし、遺伝的に鋭敏な人の場合は相当な時間が経過しても味を認識できるため、評価参加者の80%(累積比率基準)が0点に到達する時点をテストの終了時点とする。通常、全体人員の80%が終了時点に到達すると、残り20%は多少特別な人と看做してテストを終了することにより、少数の鋭敏な人によって全体平均値が増加する誤りを排除した。
相当な時間(例えば、70〜80分)が経過した時点にも80%以下の評価者だけがテストの終了(0点)に到達した場合は回答者の70%または60%が終了した時点をテストの終了時点に変更して全体テストを終了する。
−専門パネル(n=9):「実施例5のチューインガムの味の持続時間」の95%信頼区間は65±8分であり、1点到達の味の持続時間の95%信頼区間は57±10分であった。
−消費者パネル(n=200、20代または30代の成人男女):「実施例5のチューインガムの味の持続時間」の95%信頼区間は58±3分であり、1点到達の味の持続時間の95%信頼区間は43±3分であった。
−専門パネルは消費者パネルに比べて実施例5のチューインガムの味の持続時間は7分、1点到達の味の持続時間は14分程度長いことが分かった。
−消費者パネルを基準とする場合、95%信頼水準で評価した実施例5のチューインガムの味の持続時間は40分以上であるといえる。(1点到達の味の持続時間の95%信頼区間の下限値は40分である)
*95%信頼区間の下限値と上限値の範囲は、100回の同じ規模の消費者テストを実施し、その中、95回は平均値が下限値と上限値との間にあることを意味する。
Claims (5)
- ガムベース、酸味剤、甘味剤、及び香料から選択された添加物を含むチューインガム組成物であって、
前記酸味剤、甘味剤、及び香料から選択された添加物をポリビニールアセテートと配合して粉砕することにより製造される粉末状添加物を含むことを特徴とするチューインガム組成物。 - 前記ポリビニールアセテートは、重量平均分子量(Mw)が45,000〜100,000g/molであり、ガラス転移温度が38〜43℃であることを特徴とする請求項1に記載のチューインガム組成物。
- 前記添加物がポリビニールアセテート100重量部に対して1〜25重量部の範囲で配合されることを特徴とする請求項1に記載のチューインガム組成物。
- 前記粉末状添加物の粉砕粒度が30〜100メッシュの範囲であることを特徴とする請求項1に記載のチューインガム組成物。
- 前記添加物が、天然樹脂及び天然ゴム、エステルガム、ポリイソブチレン、乳化剤、ワックス、及び充填剤から選択された1種以上をさらに含むことを特徴とする請求項1から4のうち何れか1項に記載のるチューインガム組成物。
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JP2014064510A (ja) * | 2012-09-26 | 2014-04-17 | Meiji Co Ltd | チューインガム用香味供給組成物及び香味供給組成物含有チューインガム |
JP2015137274A (ja) * | 2014-01-24 | 2015-07-30 | 株式会社ロッテ | ステイン除去用口腔用組成物 |
JP2018115212A (ja) * | 2018-04-27 | 2018-07-26 | 株式会社ロッテ | ステイン除去用口腔用組成物 |
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KR101743657B1 (ko) | 2015-07-02 | 2017-06-20 | 롯데제과주식회사 | 향미 변화를 순차적으로 내는 껌 조성물 및 이를 이용한 껌 제조방법 |
KR101798477B1 (ko) * | 2015-09-24 | 2017-12-12 | 롯데제과 주식회사 | 시럽의 누수가 없는 센터 필링 츄잉껌 조성물 |
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