JP2012511046A - 多孔質溶解性固体構造を有する物品形態のパーソナルケア組成物 - Google Patents
多孔質溶解性固体構造を有する物品形態のパーソナルケア組成物 Download PDFInfo
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- JP2012511046A JP2012511046A JP2011540816A JP2011540816A JP2012511046A JP 2012511046 A JP2012511046 A JP 2012511046A JP 2011540816 A JP2011540816 A JP 2011540816A JP 2011540816 A JP2011540816 A JP 2011540816A JP 2012511046 A JP2012511046 A JP 2012511046A
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- ammonium
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- 238000000034 method Methods 0.000 claims description 34
- 125000004432 carbon atom Chemical group C* 0.000 claims description 33
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- WYHYDRAHICKYDJ-UHFFFAOYSA-L disodium;3-[2-(2-carboxylatoethoxy)ethyl-[2-(decanoylamino)ethyl]amino]propanoate Chemical compound [Na+].[Na+].CCCCCCCCCC(=O)NCCN(CCC([O-])=O)CCOCCC([O-])=O WYHYDRAHICKYDJ-UHFFFAOYSA-L 0.000 claims description 2
- HQYLVDYBSIUTBB-UHFFFAOYSA-L disodium;3-[2-(2-carboxylatoethoxy)ethyl-[2-(dodecanoylamino)ethyl]amino]propanoate Chemical compound [Na+].[Na+].CCCCCCCCCCCC(=O)NCCN(CCC([O-])=O)CCOCCC([O-])=O HQYLVDYBSIUTBB-UHFFFAOYSA-L 0.000 claims description 2
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- FDKNTODVCFVEDJ-UHFFFAOYSA-N 2-[3-(dodecylamino)propylamino]acetic acid Chemical compound CCCCCCCCCCCCNCCCNCC(O)=O FDKNTODVCFVEDJ-UHFFFAOYSA-N 0.000 claims 1
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- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
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- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
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Abstract
Description
可撓性多孔質溶解性固体構造物品は、本明細書では「物品」又は「溶解性物品」と示され得る。全ての参照は、可撓性溶解性多孔質固体構造物品を意味することが意図される。
本発明者らは、便利にかつ迅速に消費者の手の平で溶解して、液体生成物を生じることができる溶解性物品を調製できることを見出した。いったん溶解すると、この製品は、従来の液体製品と同様に使用することができ、すなわち、皮膚及び/又は毛髪に適用することができる。このような溶解性物品は今や所望量の泡を送達し、手の中に投与することができる一方、消費者が許容可能な溶解速度を供給し続けることができることが判明している。
本発明の溶解性物品は、組成物全体の約23重量%〜約75重量%の界面活性剤を含む。別の実施形態においては、本溶解性物品は、組成物全体の約50重量%〜約70重量%の界面活性剤を含む。この界面活性剤は、グループI及びグループIIの界面活性剤のブレンドを含む。本発明の界面活性剤のブレンドは、グループIからの1種以上の界面活性剤と、グループIIからの1種以上の界面活性剤と、を含む。グループIの界面活性剤はアニオン性界面活性剤を含み、グループIIの界面活性剤は両性界面活性剤、双極性界面活性剤、及びこれらの混合物を含む。本発明の1つの実施形態においては、グループIとグループIIの界面活性剤の比は、約95:5〜約30:70である。本発明の別の実施形態においては、グループIとグループIIの界面活性剤の比は、約85:15〜約40:60である。本発明の更に別の実施形態においては、グループIとグループIIの界面活性剤の比は、約70:30〜約55:45である。
本発明のグループIの界面活性剤は、1種以上のアニオン性界面活性剤を含む。本明細書の溶解性物品での使用に好適なアニオン性界面活性剤構成成分には、毛髪ケア又は他のパーソナルケア洗浄剤組成物に用いられる既知のものが挙げられる。本組成物におけるアニオン性界面活性剤構成成分の濃度は、所望の洗浄及び起泡特性を提供するのに十分であるべきであり、乾燥固体の約6.5重量%〜約71重量%は、グループIの界面活性剤である。
本発明のグループIIの界面活性剤は、1種以上の両性界面活性剤、双極性界面活性剤、及び/又はこれらの組み合わせを含む。本明細書の組成物における使用に好適な両性又は双性イオン性界面活性剤としては、ヘアケア又は他のパーソナルケア洗浄における使用が既知のものが包含される。このような両性界面活性剤、双極性界面活性剤及び/又はこれらの組み合わせの濃度は、乾燥固体の約1.0重量%〜約52.5重量%の範囲である。好適な双性イオン性又は両性界面活性剤の非限定例は、米国特許第5,104,646号(Bolich Jr.ら)、同第5,106,609号(Bolich Jr.ら)に記載されている。
本発明の組成物は更に、上記のアニオン性洗浄性界面活性剤成分と組み合わせて用いる追加の界面活性剤を含んでもよい。好適な任意の界面活性剤には、非イオン性及びカチオン性の界面活性剤が挙げられる。毛髪ケア又はパーソナルケア製品において用いられる当該技術分野において既知のあらゆるこのような界面活性剤を、任意の追加の界面活性剤が同様に組成物の必須成分に化学的及び物理的に適合性があるか、又はさもなければ、製品性能、審美性、若しくは安定性を過度に損なわないならば、用いてよい。本組成物における任意の追加の界面活性剤の濃度は、所望の洗浄又は起泡性能、選択された任意の界面活性剤、所望の製品濃度、組成物中の他の成分の存在、及び当該技術分野において周知の他の因子によって異なってもよい。
本発明は、構造化剤として機能する水溶性ポリマーを含む。本明細書で使用するとき、用語「水溶性ポリマー」は、広義に水溶性及び水分散性ポリマーの両方を含み、25℃で測定される少なくとも約0.1グラム/リットル(g/L)の水溶性を備えるポリマーとして定義される。いくつかの実施形態においては、ポリマーは、25℃で測定される約0.1グラム/リットル(g/L)〜約500グラム/リットル(g/L)の水溶性を有する(これは肉眼で等方性の又は透明の、有色又は無色の溶液の製造物を意味する)。これらの固体物を作製するためのポリマーは、人工又は天然由来でもよく、かつ化学反応の方法によって変性されてもよい。それは皮膜形成であってもよく、そうでなくてもよい。ポリマーは、生理学的に許容可能であるべきであり、つまり皮膚、粘膜、毛髪及び頭皮に適合すべきである。
本発明の多孔質溶解性固体物はパーソナルケア組成物での使用に好適な水溶性可塑化剤を含む。水溶性可塑化剤の非限定的な例としては、ポリオール、コポリオール、ポリカルボン酸、ポリエステル及びジメチコンコポリオールが挙げられる。有用なポリオールの例としては、グリセリン、ジグリセリン、プロピレングリコール、エチレングリコール、ブチレングリコール、ペンチレングリコール、シクロヘキサンジメタノール、ヘキサンジオール、ポリエチレングリコール(200〜600)、ソルビトール、マニトール、ラクチトール及び他のモノ−及び多価低分子量アルコール(例、C2〜C8アルコール)のような糖アルコール類;フルクトース、グルコース、スクロース、マルトース、ラクトース、及び高級フルクトースコーンシロップ固形物並びにアスコルビン酸のようなモノ、ジ−及びオリゴ糖が挙げられるが、これらに限定されない。ポリカルボン酸の例としては、クエン酸、マレイン酸、コハク酸、ポリアクリル酸、及びポリマレイン酸が挙げられるが、これらに限定されない。好適なポリエステルの例としては、グリセロールトリアセテート、アセチル化モノグリセリド、ジエチルフタレート、トリエチルシトレート、トリブチルシトレート、アセチルトリエチルシトレート、アセチルトリブチルシトレートが挙げられるが、これらに限定されない。好適なジメチコンコポリオールの例としては、PEG−12ジメチコン、PEG/PPG−18/18ジメチコン、及びPPG−12ジメチコンが挙げられるが、これらに限定されない。本発明の他の好適な可塑剤としては、アルキル及びアリルフタレート、ナフタレート、ラクテート(例えば、ナトリウム、アンモニウム及びカリウム塩)、sorbeth−30、尿素、乳酸、ピロリドンカルボン酸ナトリウム(PCA)、ヒラルロネート又はヒアルロン酸ナトリウム、可溶性コラーゲン、変性タンパク質、L−グルタメートモノナトリウム、例えばグリコール酸、乳酸、クエン酸、マレイン酸及びサリチル酸のようなα & βヒドロキシル酸、グリセリルポリメタクリレート、ポリクオタニウムなどのポリマー可塑剤、タンパク質、及び例えばグルタミン酸、アスパラギン酸、及びリジンなどのアミノ酸、水素デンプンヒドロリセート、他の低分子量エステル(例えば、C2〜C10アルコール及び酸のエステル)、並びに食品及びプラスチック業界の当業者に既知の他の任意の水溶性可塑剤、並びにこれらの混合物が挙げられるが、これらに限定されない。好ましい可塑剤としてはグリセリン及びプロピレングリコールが挙げられる。欧州特許第283165(B1)号は、プロポキシル化グリセロールなどのグリセロール誘導体が挙げられる、他の好適な可塑剤を開示している。
本物品は、本明細書に記載の選択された不可欠な材料と互換性があるか、あるいは過度に製品性能を損なわないようなものであるならば、組成物に使用されることが既知であるか、あるいは有用であるような他の任意成分を更に含んでもよい。
本発明の溶解性物品は、単独で、又は他のパーソナルケア成分との組み合わせにおいて使用される溶解性多孔質固体物を含む、様々な製品形態のいかなる形態でも製造することができる。溶解性多孔質固体物は、パーソナルケア組成物に使用する場合に、連続的であっても又は非連続的であってもよい。製品形態に関わらず、本発明の方法の範囲内で想到される実施形態を形成する全ての製品について重要なものは、その全てが本明細書で定義されているようなものである、固体高分子構造化剤と界面活性剤を含む有効成分との組み合わせを含む、選択され定義される溶解性多孔質固体物である。
本発明の溶解性物品及び方法による使用のための製品タイプの実施形態の非限定的な例としては、ヘアコンディショニング基材、潤いを与える基材、他の毛髪トリートメント基材、他の皮膚又は全身トリートメント基材、髭剃り準備基材、ペットケア基材、薬剤又は他のスキンケア活性剤を含むパーソナルケア基材、潤いを与える基材、日焼け止め基材、長期にわたり皮膚に有効な成分基材(例えば、ビタミンを含む基材、アルファ−ヒドロキシ酸を含む基材など)、脱臭基材、香料を含む基材、及び同様物などが挙げられる。
本発明の溶解性物品は、以下を含む方法によって調製することができる:(1)界面活性剤、溶解した高分子構造化剤、可塑剤及び他の任意成分を含む加工混合物を調製する工程、(2)その混合物内にガスを導入することにより混合物を気泡化する工程、(3)湿潤気泡化混合物を所望の1つ以上の形状に形成する工程、(4)湿潤気泡化混合物を所望の最終水分含量(例えば、エネルギーを加えることにより約0.1〜約25%の水分)まで乾燥させる工程。
加工混合物は、一般に水、可塑剤及び他の任意成分の存在下でポリマー構造剤を溶解し、熱し、続いて冷却することにより調製する。このことは、任意の好適な熱せられたバッチ攪拌システムにより、又は単軸押出機若しくは双軸押出機若しくは熱交換器を、高せん断又は静的混合に使用する任意の好適な連続的なシステムにより達成することができる。任意の工程は、ポリマーが水、界面活性剤、可塑剤、及び成分の任意の組み合わせのプレミックス部分による段階的加工を含む他の任意成分の存在下で、最終的に溶解するように想定され得る。
加工混合物の気泡化は、ガスをその混合物内に導入することにより、好ましくは機械的混合エネルギーによって達成することができるが、また化学的な方法によって達成してもよい。気泡化は、任意の好適な機械的加工方法によって達成されてもよく、その方法には、(i)遊星ミキサー又は他の好適な混合容器を含む機械的混合によるバッチタンク気泡化、(ii)食品業界で使用される(加圧及び非加圧)半連続的又は連続的気泡化装置、若しくは(iii)多孔質固体物を形成するために熱を有している金型内などで圧縮され得る気泡化ビーズ又は粒子を形成するために、加工混合物をスプレー乾燥させる工程、が挙げられるが、それらに限定されない。
湿潤気泡化加工混合物の形成は、所望の1つの形状又は複数の形状にその混合物を形成するための任意の好適な方法によって達成することができ、それらの方法には、限定するものではないが、以下の方法が挙げられる:(i)テフロン(登録商標)、金属、HDPE、ポリカーボネート、ネオプレーン、ゴム、LDPE、ガラス及び同様物を含む非干渉及び非付着性表面を備える特別に設計された金型への気泡化混合物の堆積、(ii)浅底のトレーに入っている乾燥粒状デンプン内に刻み込まれている空洞の中への気泡化混合物の堆積(菓子産業で広く利用されるデンプン成型形成技術)、並びに(iii)後でスタンプされ、カットされ、ロール上にエンボス加工され又は保管され得る、任意の非干渉又は非付着性材料テフロン(登録商標)、金属、HDPE、ポリカーボネート、ネオプレーン、ゴム、LDPE、ガラス及び同様物を備える連続的ベルト又はスクリーン上への気泡化混合物の堆積。
形成された湿潤気泡化加工混合物の乾燥は、任意の好適な方法によって達成することができ、それらの方法には、限定するものではないが、以下を含む:(i)制御された温度及び圧力又は大気条件を備える部屋を含む乾燥室、(ii)制御された温度及び任意の湿度を備える非対流式又は対流式オーブンを含むオーブン、(iii)トラック/トレー乾燥機、(iv)多段式直列乾燥機、(v)衝突オーブン、(vi)回転式オーブン/乾燥機;(vii)直列焙煎機、(viii)急速高伝熱オーブン及び乾燥機;(ix)二重プレナム焙煎機、(x)コンベヤー乾燥機、(xi)マイクロ波乾燥技術、及びこれらの組み合わせ。好ましくは、凍結乾燥法を含まない任意の好適な乾燥法を使用できる。
本発明の溶解性物品は、毛髪及び/又は皮膚などの哺乳類ケラチン性組織を処理するのに使用することができ、かつ速やかなすすぎ能力を提供することができる。毛髪をコンディショニングする方法は、以下の工程を含んでよい:a)溶解性多孔質固体物の有効量を手に適用する工程、b)溶解性多孔質固体物を水で濡らし、かつ固体物をこすって溶解する工程、c)溶解した物質をトリートメントするために毛髪又は皮膚のいずれかに適用する工程、及びd)薄められたトリートメントを水を用いて毛髪又は皮膚からすすぐ工程。これらの工程は、所望のトリートメント効果を達成するために所望に応じて何度でも繰り返すことができる。
以下の界面活性剤/ポリマー液体加工組成物を、以下に記載のように示された重量百分率で調製した。液体処方は、アニオン性:両性の界面活性剤の比、両性界面活性剤のタイプ及びアニオン性界面活性剤のタイプで異なる。
2 Sigma−Aldrich Catalog No.363081、分子量85,000〜124,000、87〜89%加水分解
3 MACKAM HPL−28ULS、供給元:McIntyre Group Ltd,University Park,IL
4 AMPHOSOL HCA−B、供給元:Stepan Company,Northfield,IL
5 MACKAM DAB−ULS、供給元:McIntyre Group Ltd,University Park,IL
6 0/0.3/0.9/0.5/71.5/1/20/1.9/3.9/0の推定C8/C9/C10/C11/C12/C13/C14/C15/C16/C18アルキル鎖長分布を有し、平均2.0モルのエトキシル化を受けた25%活性でのラウレス−3硫酸アンモニウム、供給元:Procter & Gamble Chemicals
7 0/0/0.6/93.6/5.1/0.7/0/0/0/0の推定C8/C9/C10/C11/C12/C13/C14/C15/C16/C18アルキル鎖長分布を有する24%活性でのウンデシル硫酸アンモニウム、供給元:Procter & Gamble Chemicals
8 0/0.3/1.3/0.5/69.6/1.1/21.8/1.2/4.2/0の推定C8/C9/C10/C11/C12/C13/C14/C15/C16/C18アルキル鎖長分布を有し、平均0.82モルのエトキシル化を受けた70%活性でのラウレス−1硫酸アンモニウム、供給元:Procter & Gamble Chemicals
9 0/0.3/1.1/0.5/70.6/1.1/20.9/1.6/4.1/0の推定C8/C9/C10/C11/C12/C13/C14/C15/C16/C18アルキル鎖長分布を有する25%活性でのラウリル硫酸アンモニウム、供給元:Procter & Gamble Chemicals
10 微細粒状の無水クエン酸51N、供給元:S.A.Citrique Belge N.V.Pastorijstraat 249,B−3300 Tienen,Belgium
2 Sigma−Aldrich Catalog No.363081、分子量85,000〜124,000、87〜89%加水分解
3 MACKAM HPL−28ULS、供給元:McIntyre Group Ltd,University Park,IL
4 AMPHOSOL HCA−B、供給元:Stepan Company,Northfield,IL
5 MACKAM DAB−ULS、供給元:McIntyre Group Ltd,University Park,IL
6 0/0.3/0.9/0.5/71.5/1/20/1.9/3.9/0の推定C8/C9/C10/C11/C12/C13/C14/C15/C16/C18アルキル鎖長分布を有し、平均2.0モルのエトキシル化を受けた25%活性でのラウレス−3硫酸アンモニウム、供給元:Procter & Gamble Chemicals
7 0/0/0.6/93.6/5.1/0.7/0/0/0/0の推定C8/C9/C10/C11/C12/C13/C14/C15/C16/C18アルキル鎖長分布を有する24%活性でのウンデシル硫酸アンモニウム、供給元:Procter & Gamble Chemicals
8 0/0.3/1.3/0.5/69.6/1.1/21.8/1.2/4.2/0の推定C8/C9/C10/C11/C12/C13/C14/C15/C16/C18アルキル鎖長分布を有し、平均0.82モルのエトキシル化を受けた70%活性でのラウレス−1硫酸アンモニウム、供給元:Procter & Gamble Chemicals
9 0/0.3/1.1/0.5/70.6/1.1/20.9/1.6/4.1/0の推定C8/C9/C10/C11/C12/C13/C14/C15/C16/C18アルキル鎖長分布を有する25%活性でのラウリル硫酸アンモニウム、供給元:Procter & Gamble Chemicals
10 CO−1694セチルアルコールNF、供給元:Procter & Gamble Chemicals
11 NINOL COMF、供給元:Stepan Company,Northfield,IL
12 微細粒状の無水クエン酸51N、供給元:S.A.Citrique Belge N.V.Pastorijstraat 249,B−3300 Tienen,Belgium
溶解性多孔質シャンプー固体物の実施例8、9、10、11、12、13及び14を、実施例1、2、3、4、5、6及び7からの界面活性剤/ポリマー液体加工溶液からそれぞれ以下に記載のように調製する。表において、ラウロアンホ酢酸NaはLAAと示され、コカミドプロピルベタインはCAPBと示され、ラウラミドプロピルベタインはLAPBと示される。
Claims (13)
- a.約10%〜約50%の水溶性ポリマーと、
b.約1%〜約25%の可塑剤と、
c.約23%〜約75%の界面活性剤と、を含む多孔質溶解性固体構造形態の溶解性物品であって、前記界面活性剤は、
i.グループIからの1種以上の界面活性剤と、
ii.グループIIからの1種以上の界面活性剤と、を含み、前記グループIはアニオン性界面活性剤を含み、前記グループIIは両性、双極性イオン及びこれらの組み合わせからなる群から選択される界面活性剤を含み、
前記グループIと前記グループIIの界面活性剤の比が約5:95〜約30:70であり、
前記溶解性物品は、約0.05g/cm3〜約0.25g/cm3の密度を有する、溶解性物品。 - 前記グループIIの界面活性剤が、以下の構造に従う両性界面活性剤であり、
- 前記グループIIの界面活性剤が、ラウロアンホ酢酸ナトリウム、ココアンホ酢酸ナトリウム、ラウロアンホ酢酸アンモニウム及びココアンホ酢酸アンモニウムからなる群から選択される両性界面活性剤であり、好ましくは前記両性界面活性剤はラウロアンホ酢酸ナトリウムであり、好ましくは前記グループIIの界面活性剤は、コカミノプロピオン酸ナトリウム、コカミノジプロピオン酸ナトリウム、ココアンホ酢酸ナトリウム、ココアンホヒドロキシプロピルスルホン酸ナトリウム、ココアンホプロピオン酸ナトリウム、コーンアンホプロピオン酸ナトリウム、ラウラミノプロピオン酸ナトリウム、ラウロアンホ酢酸ナトリウム、ラウロアンホヒドロキシプロピルスルホン酸ナトリウム、ラウロアンホプロピオン酸ナトリウム、コーンアンホプロピオン酸ナトリウム、ラウリミノジプロピオン酸ナトリウム、コカミノプロピオン酸アンモニウム、コカミノジプロピオン酸アンモニウム、ココアンホ酢酸アンモニウム、ココアンホヒドロキシプロピルスルホン酸アンモニウム、ココアンホプロピオン酸アンモニウム、コーンアンホプロピオン酸アンモニウム、ラウラミノプロピオン酸アンモニウム、ラウロアンホ酢酸アンモニウム、ラウロアンホヒドロキシプロピルスルホン酸アンモニウム、ラウロアンホプロピオン酸アンモニウム、コーンアンホプロピオン酸アンモニウム、ラウリミノジプロピオン酸アンモニウム、コカミノプロピオン酸トリエタノールアミン、コカミノジプロピオン酸トリエタノールアミン、ココアンホ酢酸トリエタノールアミン、ココアンホヒドロキシプロピルスルホン酸トリエタノールアミン、ココアンホプロピオン酸トリエタノールアミン、コーンアンホプロピオン酸トリエタノールアミン、ラウラミノプロピオン酸トリエタノールアミン、ラウロアンホ酢酸トリエタノールアミン、ラウロアンホヒドロキシプロピルスルホン酸トリエタノールアミン、ラウロアンホプロピオン酸トリエタノールアミン、コーンアンホプロピオン酸トリエタノールアミン、ラウリミノジプロピオン酸トリエタノールアミン、ココアンホジプロピオン酸、カプロアンホ二酢酸二ナトリウム、カプロアンホジプロピオン酸二ナトリウム、カプリロアンホ二酢酸二ナトリウム、カプリロアンホジプロピオン酸二ナトリウム、ココアンホカルボキシエチルヒドロキシプロピルスルホン酸二ナトリウム、ココアンホ二酢酸二ナトリウム、ココアンホジプロピオン酸二ナトリウム、ジカルボキシエチルココプロピレンジアミン二ナトリウム、ラウレス−5カルボキシアンホ二酢酸二ナトリウム、ラウリミノジプロピオン酸二ナトリウム、ラウロアンホ二酢酸二ナトリウム、ラウロアンホジプロピオン酸二ナトリウム、オレオアンホジプロピオン酸二ナトリウム、PPG−2−イソデセチ−7−カルボキシアンホ二酢酸二ナトリウム、ラウラミノプロピオン酸、ラウロアンホジプロピオン酸、ラウリルアミノプロピルグリシン、ラウリルジエチレンジアミノグリシン及びこれらの組み合わせからなる群から選択される両性界面活性剤である、請求項1に記載の溶解性物品。
- 前記グループIIの界面活性剤が、コカミドエチルベタイン、コカミドプロピルアミンオキシド、コカミドプロピルベタイン、コカミドプロピルジメチルアミノヒドロキシプロピル加水分解コラーゲン、コカミドプロピルジモニウムヒドロキシプロピル加水分解コラーゲン、コカミドプロピルヒドロキシスルタイン、ココベタインアミドアンホプロピオネート、ココ−ベタイン、ココ−ヒドロキシスルタイン、ココ/オレアミドプロピルベタイン、ココ−スルタイン、ラウリン酸アミドプロピルベタイン、ラウリルベタイン、ラウリルヒドロキシスルタイン、ラウリルスルタイン及びこれらの組み合わせからなる群から選択される双極性界面活性剤である、請求項1に記載の溶解性物品。
- 前記アニオン性界面活性剤が、アルキルサルフェート及びアルキルエーテルサルフェートからなる群から選択される、請求項1に記載の溶解性物品。
- 前記アニオン性界面活性剤が、以下の構造に従うアルキルサルフェートであり、
- 前記グループIの界面活性剤と前記グループIIの界面活性剤の比が約85:15〜約40:60であり、好ましくは前記グループIの界面活性剤と前記グループIIの界面活性剤の比が約80:20〜約50:50であり、好ましくは前記グループIの界面活性剤と前記グループIIの界面活性剤の比が約70:30〜約55:45である、請求項1に記載の溶解性物品。
- 前記物品が約20%〜約30%の前記水溶性ポリマーを含み、前記水溶性ポリマーが約40,000〜約500,000の重量平均分子量を有する、請求項1に記載の溶解性物品。
- 約5%〜約15%の前記可塑剤と、約50%〜約70%の前記界面活性剤と、を含む、請求項1に記載の溶解性物品。
- 前記密度が約0.05g/cm3〜約0.25g/cm3であり、好ましくは前記密度が約0.075g/cm3〜約0.20g/cm3であり、更に好ましくは前記密度が約0.10g/cm3〜約0.15g/cm3である、請求項1に記載の溶解性物品。
- 約125グラム/m2〜約3,000グラム/m2の坪量を有し、好ましくは約150グラム/m2〜約1,200グラム/m2の坪量を有し、好ましくは約200グラム/m2〜約1,000グラム/m2の坪量を有し、更に好ましくは約300グラム/m2〜約800グラム/m2の坪量を有する、請求項1に記載の溶解性物品。
- 前記溶解性物品が約80%〜約100%の開放気泡含有百分率を有し、好ましくは前記溶解性物品が約85%〜約97.5%の開放気泡含有百分率を有し、更に好ましくは前記溶解性物品が約90%〜約95%の開放気泡含有百分率を有する、請求項1に記載の溶解性物品。
- 多孔質溶解性固体構造形態の溶解性物品であって、前記物品が、
a.プレミックスを調製する工程であって、前記プレミックスは界面活性剤と、水溶性ポリマーと、可塑剤と、グループIからの1種以上の界面活性剤と、グループIIからの1種以上の界面活性剤と、を含み、前記グループIはアニオン性界面活性剤を含み、前記グループIIは両性、双極性イオン及びこれらの組み合わせからなる群から選択される界面活性剤を含み、前記プレミックスは約20%〜約50%の固形分と、約5,000cps〜約150,000cpsの粘度を有する、プレミックスの調製工程と、
b.気体を前記プレミックス中に導入することにより前記プレミックスを気泡化して、湿潤気泡化されたプレミックスを形成する工程と、
c.前記湿潤気泡化されたプレミックスを所望の1種以上の形状に形成して、成形された湿潤プレミックスを形成する工程と、
d.前記成形した湿潤プレミックスを最終含水量に乾燥させることにより前記溶解性物品を形成する工程と、を含むプロセスにより形成され、前記最終含水量が約0.1%〜約25%の水分である、溶解性物品。
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Also Published As
Publication number | Publication date |
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MX2011005740A (es) | 2011-06-21 |
CN102245155B (zh) | 2015-11-25 |
WO2010077628A2 (en) | 2010-07-08 |
WO2010077628A3 (en) | 2011-09-15 |
EP2355772A2 (en) | 2011-08-17 |
CN102245155A (zh) | 2011-11-16 |
US20100286011A1 (en) | 2010-11-11 |
BRPI0922332A2 (pt) | 2018-06-05 |
EP2355772B1 (en) | 2016-11-09 |
US8461091B2 (en) | 2013-06-11 |
JP5718245B2 (ja) | 2015-05-13 |
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