JP2011502043A5 - - Google Patents
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- JP2011502043A5 JP2011502043A5 JP2010532034A JP2010532034A JP2011502043A5 JP 2011502043 A5 JP2011502043 A5 JP 2011502043A5 JP 2010532034 A JP2010532034 A JP 2010532034A JP 2010532034 A JP2010532034 A JP 2010532034A JP 2011502043 A5 JP2011502043 A5 JP 2011502043A5
- Authority
- JP
- Japan
- Prior art keywords
- milling
- less
- solid compound
- rotor
- particle size
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000003801 milling Methods 0.000 claims 11
- 239000007787 solid Substances 0.000 claims 9
- 150000001875 compounds Chemical class 0.000 claims 8
- 239000002245 particle Substances 0.000 claims 7
- 239000000203 mixture Substances 0.000 claims 6
- 239000007788 liquid Substances 0.000 claims 4
- 239000006185 dispersion Substances 0.000 claims 2
- 230000036909 Volume distribution Effects 0.000 claims 1
- 238000000034 method Methods 0.000 claims 1
- 238000003756 stirring Methods 0.000 claims 1
Claims (5)
- 化合物のミリングされた固体粒子の分散体を形成するための方法であって、
混合容器内で、液体媒体と３００ミクロン以下の平均粒径を有するミリング媒体と固体化合物のミリング混合物を形成すること、および
ミリング混合物をミキサーにより攪拌して、ミリング媒体と固体化合物とを接触させ、固体化合物を所望の平均粒径まで小さくして、液体媒体中のミリングされた固体粒子の分散体を形成すること、
を含み、ミリング混合物における液体媒体と固体化合物の合計体積に対するミリング媒体の体積比が１未満であり、ミリング媒体の平均粒径を超え且つ２．５ｍｍ以下のローター−ステーターギャップで分離されたローター要素およびステーター要素を含んで成るローター−ステーターミキサーを使用して、当該ローター−ステーターミキサーのミリングチャンバ内でミリング混合物を攪拌し、固体化合物が２００ｎｍ以下の体積加重平均等価球直径粒径に粉砕されることを特徴とする方法。 - ローター−ステーターを少なくとも３３ｍ／秒の先端速度で動作させる、請求項１に記載の方法。
- 固体化合物が、液体媒体に対して少なくとも１５質量％の濃度でミリング混合物中に存在する、請求項１または２に記載の方法。
- 固体化合物が、２４時間以内に、１００ｎｍ以下の体積加重平均等価球直径粒径、および１７５ｎｍ以下の９５番目パーセンタイル体積分布等価球直径に粉砕される、請求項１〜３のいずれか一項に記載の方法。
- ローター−ステーターミキサーが混合容器内のミリング混合物中に浸漬される、請求項１〜４のいずれか一項に記載の方法。
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US11/931,948 US7441717B1 (en) | 2007-10-31 | 2007-10-31 | Micromedia milling process |
| PCT/US2008/012207 WO2009058257A2 (en) | 2007-10-31 | 2008-10-28 | Improved micromedia milling process |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2011502043A JP2011502043A (ja) | 2011-01-20 |
| JP2011502043A5 true JP2011502043A5 (ja) | 2011-12-15 |
Family
ID=39874243
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2010532034A Pending JP2011502043A (ja) | 2007-10-31 | 2008-10-28 | 改良されたミクロ媒体ミリング方法 |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US7441717B1 (ja) |
| EP (1) | EP2212385B1 (ja) |
| JP (1) | JP2011502043A (ja) |
| AT (1) | ATE521671T1 (ja) |
| WO (1) | WO2009058257A2 (ja) |
Families Citing this family (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2922256B1 (fr) * | 2007-10-12 | 2010-03-12 | Spcm Sa | Installation pour la recuperation assistee du petrole mettant en oeuvre des polymeres hydrosolubles, procede mettant en oeuvre l'installation |
| US8563282B2 (en) * | 2008-08-27 | 2013-10-22 | Edeniq, Inc. | Materials and methods for converting biomass to biofuel |
| KR101821846B1 (ko) | 2010-12-13 | 2018-01-24 | 썬 케미칼 코포레이션 | 안료 입자 분산액 중 밀링 매질의 가용화 방법 |
| WO2013039941A1 (en) | 2011-09-16 | 2013-03-21 | Eastman Kodak Company | Ink composition for continuous inkjet printer |
| JP2013148821A (ja) * | 2012-01-23 | 2013-08-01 | Fuji Xerox Co Ltd | 液体現像剤の製造装置 |
| CN105121023B (zh) * | 2013-02-28 | 2017-08-25 | 太阳化学公司 | 用于在液体分散液中制造研磨的固体的装置和连续方法 |
| WO2014132445A1 (ja) * | 2013-03-01 | 2014-09-04 | 国立大学法人京都大学 | セラミックス微粒子分散液の製造方法 |
| US9421477B2 (en) * | 2013-08-12 | 2016-08-23 | Green Extraction Technologies | Biomass fractionation and extraction apparatus |
| WO2015071841A1 (en) | 2013-11-12 | 2015-05-21 | Druggability Technologies Holdings Limited | Complexes of dabigatran and its derivatives, process for the preparation thereof and pharmaceutical compositions containing them |
| US9315685B2 (en) * | 2014-04-19 | 2016-04-19 | Xerox Corporation | Process for preparing an aqueous ink jet printing ink |
| US9249329B2 (en) * | 2014-04-19 | 2016-02-02 | Xerox Corporation | Aqueous ink jet printing ink |
| EP3154732A4 (en) * | 2014-06-16 | 2018-02-14 | Commonwealth Scientific and Industrial Research Organisation | Method of producing a powder product |
| US11096402B2 (en) * | 2014-07-08 | 2021-08-24 | Gea Process Engineering A/S | Production of a coffee extract preserving flavour components |
| US9573349B1 (en) | 2015-07-30 | 2017-02-21 | Eastman Kodak Company | Multilayered structure with water-impermeable substrate |
| US9376582B1 (en) | 2015-07-30 | 2016-06-28 | Eastman Kodak Company | Printing on water-impermeable substrates with water-based inks |
| US11154868B2 (en) | 2017-02-24 | 2021-10-26 | Greenvolt Nano Inc. | Apparatus and method for forming nanoparticles |
| US20180243750A1 (en) * | 2017-02-24 | 2018-08-30 | Greenvolt LTD | Apparatus and method for forming nanoparticles |
| CA3070221C (en) | 2017-07-24 | 2023-10-10 | United States Of America, As Represented By The Secretary Of The Army | Aluminum based nanogalvanic compositions useful for generating hydrogen gas and low temperature processing thereof |
| US10305022B1 (en) | 2017-12-14 | 2019-05-28 | Eastman Kodak Company | Silver-containing electrically-conductive compositions |
| US10297741B1 (en) | 2017-12-14 | 2019-05-21 | Eastman Kodak Company | Electrically-conductive compositions |
| US10763424B2 (en) | 2017-12-14 | 2020-09-01 | Eastman Kodak Company | Composite articles with dielectric layer |
| US10763421B2 (en) | 2017-12-14 | 2020-09-01 | Eastman Kodak Company | Piezoelectric article with dielectric layer and co-planar electrodes |
| US10818835B2 (en) | 2017-12-14 | 2020-10-27 | Eastman Kodak Company | Inertial piezoelectric device |
| US10777732B2 (en) | 2017-12-14 | 2020-09-15 | Eastman Kodak Company | Piezoelectric composite articles |
| US11251359B2 (en) | 2017-12-14 | 2022-02-15 | Eastman Kodak Company | Piezoelectric capacitor |
| US10763422B2 (en) | 2017-12-14 | 2020-09-01 | Eastman Kodak Company | Composite article with co-planar electrodes |
| US11305343B2 (en) | 2018-02-28 | 2022-04-19 | Nanom Inc. | Apparatus and method for programming a crystal lattice structure of nanoparticles |
| EP4047059A4 (en) * | 2019-10-18 | 2023-10-11 | DIC Corporation | METHOD FOR PRODUCING A PIGMENT COMPOSITION |
| US20220372324A1 (en) * | 2019-11-21 | 2022-11-24 | Dic Corporation | Method for producing pigment composition |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH04166246A (ja) * | 1990-10-31 | 1992-06-12 | Matsushita Electric Ind Co Ltd | 媒体撹拌ミル及び粉砕方法 |
| US5971307A (en) * | 1998-02-13 | 1999-10-26 | Davenport; Ricky W. | Rotary grinder |
| US5500331A (en) * | 1994-05-25 | 1996-03-19 | Eastman Kodak Company | Comminution with small particle milling media |
| US5513803A (en) * | 1994-05-25 | 1996-05-07 | Eastman Kodak Company | Continuous media recirculation milling process |
| US5522553A (en) | 1994-09-29 | 1996-06-04 | Kady International | Method and apparatus for producing liquid suspensions of finely divided matter |
| US5632596A (en) | 1995-07-19 | 1997-05-27 | Charles Ross & Son Co. | Low profile rotors and stators for mixers and emulsifiers |
| US5662279A (en) | 1995-12-05 | 1997-09-02 | Eastman Kodak Company | Process for milling and media separation |
| BR9810310A (pt) | 1997-06-24 | 2000-09-19 | Kady International | Moinho de dispersão, equipamento para produzir suspensões lìquidas de material finamente dividido, e, processos para retirada de água de uma corrente de lama e para a produção de extratos |
| JPH11319601A (ja) * | 1998-05-11 | 1999-11-24 | Ricoh Co Ltd | 機械式粉砕装置 |
| US6241472B1 (en) | 1999-03-22 | 2001-06-05 | Charles Ross & Son Company | High shear rotors and stators for mixers and emulsifiers |
| US6305626B1 (en) * | 1999-05-20 | 2001-10-23 | Apv North America, Inc. | Colloid mill |
| DE60012520T3 (de) * | 1999-06-01 | 2009-06-25 | Elan Pharma International Ltd. | Kleinmühle und verfahren dafür |
| KR20050037477A (ko) * | 2001-10-17 | 2005-04-22 | 이 아이 듀폰 디 네모아 앤드 캄파니 | 로터-스테이터 장치와 입자 생성을 위한 방법 |
| JP2007264315A (ja) * | 2006-03-28 | 2007-10-11 | Mitsubishi Chemicals Corp | 着色剤分散体、着色剤分散体の製造方法及び静電荷像現像用トナーの製造方法 |
-
2007
- 2007-10-31 US US11/931,948 patent/US7441717B1/en not_active Expired - Fee Related
-
2008
- 2008-10-28 AT AT08843911T patent/ATE521671T1/de not_active IP Right Cessation
- 2008-10-28 WO PCT/US2008/012207 patent/WO2009058257A2/en active Application Filing
- 2008-10-28 JP JP2010532034A patent/JP2011502043A/ja active Pending
- 2008-10-28 EP EP08843911A patent/EP2212385B1/en not_active Not-in-force
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