JP2011231130A5 - - Google Patents
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- Publication number
- JP2011231130A5 JP2011231130A5 JP2011179591A JP2011179591A JP2011231130A5 JP 2011231130 A5 JP2011231130 A5 JP 2011231130A5 JP 2011179591 A JP2011179591 A JP 2011179591A JP 2011179591 A JP2011179591 A JP 2011179591A JP 2011231130 A5 JP2011231130 A5 JP 2011231130A5
- Authority
- JP
- Japan
- Prior art keywords
- magnesium
- cyclopentadienyl
- formula
- bis
- purity bis
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- USZGMDQWECZTIQ-UHFFFAOYSA-N [Mg](C1C=CC=C1)C1C=CC=C1 Chemical compound [Mg](C1C=CC=C1)C1C=CC=C1 USZGMDQWECZTIQ-UHFFFAOYSA-N 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 3
- ZSWFCLXCOIISFI-UHFFFAOYSA-N cyclopentadiene Chemical compound C1C=CC=C1 ZSWFCLXCOIISFI-UHFFFAOYSA-N 0.000 claims 5
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims 4
- 229910052749 magnesium Inorganic materials 0.000 claims 4
- 239000011777 magnesium Substances 0.000 claims 4
- 238000004519 manufacturing process Methods 0.000 claims 2
- 125000005270 trialkylamine group Chemical group 0.000 claims 2
- 125000004169 (C1-C6) alkyl group Chemical group 0.000 claims 1
- HECLRDQVFMWTQS-RGOKHQFPSA-N 1755-01-7 Chemical compound C1[C@H]2[C@@H]3CC=C[C@@H]3[C@@H]1C=C2 HECLRDQVFMWTQS-RGOKHQFPSA-N 0.000 claims 1
- 125000000217 alkyl group Chemical group 0.000 claims 1
- 125000004432 carbon atom Chemical group C* 0.000 claims 1
- 238000001816 cooling Methods 0.000 claims 1
- 238000005336 cracking Methods 0.000 claims 1
- 125000000058 cyclopentadienyl group Chemical group C1(=CC=CC1)* 0.000 claims 1
- YHNWUQFTJNJVNU-UHFFFAOYSA-N magnesium;butane;ethane Chemical compound [Mg+2].[CH2-]C.CCC[CH2-] YHNWUQFTJNJVNU-UHFFFAOYSA-N 0.000 claims 1
- 238000002360 preparation method Methods 0.000 claims 1
- 238000000859 sublimation Methods 0.000 claims 1
- 230000008022 sublimation Effects 0.000 claims 1
- SWZDQOUHBYYPJD-UHFFFAOYSA-N tridodecylamine Chemical group CCCCCCCCCCCCN(CCCCCCCCCCCC)CCCCCCCCCCCC SWZDQOUHBYYPJD-UHFFFAOYSA-N 0.000 claims 1
- 238000002354 inductively-coupled plasma atomic emission spectroscopy Methods 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2011179591A JP5348202B2 (ja) | 2011-08-19 | 2011-08-19 | 高純度ビス（シクロペンタジエニル）マグネシウム及びその製法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2011179591A JP5348202B2 (ja) | 2011-08-19 | 2011-08-19 | 高純度ビス（シクロペンタジエニル）マグネシウム及びその製法 |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2006082411A Division JP2007254408A (ja) | 2006-03-24 | 2006-03-24 | 高純度ビス（シクロペンタジエニル）マグネシウム及びその製法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2011231130A JP2011231130A (ja) | 2011-11-17 |
| JP2011231130A5 true JP2011231130A5 (https=) | 2012-01-05 |
| JP5348202B2 JP5348202B2 (ja) | 2013-11-20 |
Family
ID=45320790
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2011179591A Expired - Fee Related JP5348202B2 (ja) | 2011-08-19 | 2011-08-19 | 高純度ビス（シクロペンタジエニル）マグネシウム及びその製法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP5348202B2 (https=) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115043884A (zh) * | 2022-06-15 | 2022-09-13 | 江苏南大光电材料股份有限公司 | 二茂镁制备系统及制备方法 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5659719A (en) * | 1979-10-18 | 1981-05-23 | Daicel Chem Ind Ltd | Preparation of cyclopentadiene |
| JPH0267230A (ja) * | 1988-09-02 | 1990-03-07 | Toyo Stauffer Chem Co | 有機金属化合物の精製法 |
| DE4402192A1 (de) * | 1994-01-26 | 1995-07-27 | Witco Gmbh | Verfahren zur Herstellung von Biscyclopentadienyl-Verbindungen |
| DE4406109A1 (de) * | 1994-02-25 | 1995-08-31 | Witco Gmbh | Verfahren zur Herstellung von verbrückten stereorigiden Metallocenen |
| DE4406110A1 (de) * | 1994-02-25 | 1995-08-31 | Witco Gmbh | Verbrückte Cyclopentadienylmagnesium-Verbindungen und Verfahren zu ihrer Herstellung und ihre Verwendung zur Herstellung von Metallocenen |
| CA2404130A1 (en) * | 2000-04-19 | 2001-10-25 | Saes Getters S.P.A. | A process for the purification of organometallic compounds or heteroatomic organic compounds with a catalyst based on iron and manganese supported on zeolites |
| JP2006290889A (ja) * | 2005-04-12 | 2006-10-26 | Rohm & Haas Electronic Materials Llc | 金属含有化合物精製 |
-
2011
- 2011-08-19 JP JP2011179591A patent/JP5348202B2/ja not_active Expired - Fee Related
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