JP2010533644A5 - - Google Patents
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- Publication number
- JP2010533644A5 JP2010533644A5 JP2010510367A JP2010510367A JP2010533644A5 JP 2010533644 A5 JP2010533644 A5 JP 2010533644A5 JP 2010510367 A JP2010510367 A JP 2010510367A JP 2010510367 A JP2010510367 A JP 2010510367A JP 2010533644 A5 JP2010533644 A5 JP 2010533644A5
- Authority
- JP
- Japan
- Prior art keywords
- hydrolyzing
- ester
- compound
- ester according
- base
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 150000002148 esters Chemical group 0.000 claims 27
- 238000000034 method Methods 0.000 claims 21
- 230000003301 hydrolyzing effect Effects 0.000 claims 19
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims 12
- 239000002585 base Substances 0.000 claims 7
- 150000001875 compounds Chemical class 0.000 claims 7
- 229940126062 Compound A Drugs 0.000 claims 5
- NLDMNSXOCDLTTB-UHFFFAOYSA-N Heterophylliin A Natural products O1C2COC(=O)C3=CC(O)=C(O)C(O)=C3C3=C(O)C(O)=C(O)C=C3C(=O)OC2C(OC(=O)C=2C=C(O)C(O)=C(O)C=2)C(O)C1OC(=O)C1=CC(O)=C(O)C(O)=C1 NLDMNSXOCDLTTB-UHFFFAOYSA-N 0.000 claims 5
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 claims 5
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 claims 4
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 claims 4
- 238000006243 chemical reaction Methods 0.000 claims 4
- 239000002609 medium Substances 0.000 claims 4
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 claims 3
- HUCVOHYBFXVBRW-UHFFFAOYSA-M caesium hydroxide Inorganic materials [OH-].[Cs+] HUCVOHYBFXVBRW-UHFFFAOYSA-M 0.000 claims 3
- 125000004432 carbon atom Chemical group C* 0.000 claims 3
- 239000000126 substance Substances 0.000 claims 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims 2
- 150000005690 diesters Chemical class 0.000 claims 2
- 239000007788 liquid Substances 0.000 claims 2
- 230000035484 reaction time Effects 0.000 claims 2
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 claims 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 2
- MFGOFGRYDNHJTA-UHFFFAOYSA-N 2-amino-1-(2-fluorophenyl)ethanol Chemical compound NCC(O)C1=CC=CC=C1F MFGOFGRYDNHJTA-UHFFFAOYSA-N 0.000 claims 1
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims 1
- 229910052783 alkali metal Inorganic materials 0.000 claims 1
- 150000001340 alkali metals Chemical class 0.000 claims 1
- 125000002877 alkyl aryl group Chemical group 0.000 claims 1
- 125000000217 alkyl group Chemical group 0.000 claims 1
- 239000012736 aqueous medium Substances 0.000 claims 1
- 125000003118 aryl group Chemical group 0.000 claims 1
- 125000002619 bicyclic group Chemical group 0.000 claims 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims 1
- 230000007062 hydrolysis Effects 0.000 claims 1
- 238000006460 hydrolysis reaction Methods 0.000 claims 1
- 125000005647 linker group Chemical group 0.000 claims 1
- -1 malonic acid diester Chemical class 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- 239000012429 reaction media Substances 0.000 claims 1
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US93262907P | 2007-05-31 | 2007-05-31 | |
| PCT/US2008/006907 WO2008150487A2 (en) | 2007-05-31 | 2008-05-30 | Synthesis of half esters |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2013163978A Division JP2013227345A (ja) | 2007-05-31 | 2013-08-07 | ハーフエステルの合成方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2010533644A JP2010533644A (ja) | 2010-10-28 |
| JP2010533644A5 true JP2010533644A5 (enExample) | 2012-03-08 |
Family
ID=40094335
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2010510367A Pending JP2010533644A (ja) | 2007-05-31 | 2008-05-30 | ハーフエステルの合成方法 |
| JP2013163978A Pending JP2013227345A (ja) | 2007-05-31 | 2013-08-07 | ハーフエステルの合成方法 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2013163978A Pending JP2013227345A (ja) | 2007-05-31 | 2013-08-07 | ハーフエステルの合成方法 |
Country Status (3)
| Country | Link |
|---|---|
| US (2) | US8338635B2 (enExample) |
| JP (2) | JP2010533644A (enExample) |
| WO (1) | WO2008150487A2 (enExample) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5970002B2 (ja) | 2011-03-03 | 2016-08-17 | バイエル・インテレクチュアル・プロパティ・ゲゼルシャフト・ミット・ベシュレンクテル・ハフツングＢａｙｅｒ Ｉｎｔｅｌｌｅｃｔｕａｌ Ｐｒｏｐｅｒｔｙ ＧｍｂＨ | ４−ヒドロキシ−２−オキソ−２，５−ジヒドロフラン−３−カルボン酸化合物のナトリウム塩またはカリウム塩の製造方法 |
| MX356231B (es) | 2012-08-01 | 2018-05-18 | Bayer Cropscience Ag | Procedimiento multietapa para la preparación de sales de metales alcalinos de ésteres 4-hidroxi-2-oxo-2,5-dihidrofuran-3-carboxílic os específicos. |
| WO2015025929A1 (ja) | 2013-08-23 | 2015-02-26 | ダイキン工業株式会社 | パーフルオロ（ポリ）エーテル基含有二官能化合物、パーフルオロ（ポリ）エーテル基含有二官能化合物を含む組成物およびこれらの製造方法 |
| CN106278895B (zh) * | 2015-05-15 | 2021-07-09 | Dic株式会社 | 羧酸化合物、其制造方法、使用该化合物的液晶组合物 |
Family Cites Families (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3150165A (en) * | 1962-02-23 | 1964-09-22 | Texaco Inc | Non-catalytic hydrolysis of diesters of dicarboxylic acids to the monoesters |
| US4220708A (en) * | 1977-07-22 | 1980-09-02 | Heller Harold G | Photochromic compounds |
| US4267087A (en) * | 1977-08-29 | 1981-05-12 | Ciba-Geigy Corporation | Perfluoroalkyl substituted anhydrides and polyacids, and derivatives thereof |
| US4254111A (en) * | 1978-07-05 | 1981-03-03 | Roecar Holdings (Netherlands Antilles) Nv | Sterolin products |
| DE3034538A1 (de) * | 1980-09-12 | 1982-05-06 | Hoechst Ag, 6000 Frankfurt | -fluorsulfato-perfluorcarbonsaeurederivate und verfahren zu deren herstellung |
| DE3106819A1 (de) * | 1981-02-24 | 1982-09-09 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von 1,4-butandiol |
| US4728466A (en) * | 1985-10-18 | 1988-03-01 | Rhone-Poulenc Nederland B.V. | Process for the production of aliphatic phosphonic acids |
| US5123951A (en) * | 1986-03-31 | 1992-06-23 | Rhone-Poulenc Nederland B.V. | Synergistic plant growth regulator compositions |
| AU614488B2 (en) * | 1986-03-31 | 1991-09-05 | Rhone-Poulenc Nederlands B.V. | Synergistic plant growth regulator compositions |
| JPH0285232A (ja) * | 1988-09-22 | 1990-03-26 | Nippon Mining Co Ltd | 長鎖二塩基酸モノエステル塩の製造方法 |
| US5047574A (en) * | 1988-12-14 | 1991-09-10 | Shionogi & Co., Ltd. | Certain optically active mono esters of dicarboxylic acids |
| US5302305A (en) * | 1989-02-09 | 1994-04-12 | The Lubrizol Corporation | Carboxylic esters, liquid compositions containing said carboxylic esters and methods of lubricating metal parts |
| EP0451790A1 (de) * | 1990-04-12 | 1991-10-16 | Hoechst Aktiengesellschaft | 3,5-disubstituierte 2-Isoxazoline und Isoxazole, Verfahren zu deren Herstellung, diese enthaltende Mittel und ihre Verwendung |
| JPH0429959A (ja) * | 1990-05-24 | 1992-01-31 | Sanken Kako Kk | 高純度ジカルボン酸モノエステルの製造方法 |
| US5597555A (en) * | 1992-04-02 | 1997-01-28 | Croda, Inc. | Fatty alkoxylate esters of aliphatic and aromatic dicarboxylic acids |
| US5773261A (en) * | 1996-08-26 | 1998-06-30 | The Nutrasweet Company | Regioselective α-hydrolysis of amino acid diesters using pig liver esterase |
| JPH11130728A (ja) * | 1997-10-23 | 1999-05-18 | Mitsubishi Rayon Co Ltd | マロン酸モノ第３級アルキルエステルの製造方法 |
| DE19817101A1 (de) * | 1998-04-17 | 1999-10-21 | Degussa | Verfahren zur Herstellung von Kaliummonoethylmalonat |
| DE19934165A1 (de) * | 1999-07-21 | 2001-01-25 | Degussa | Verfahren zur Herstellung von Alkalimetallsalzen der Malonsäuremonoalkylester |
| WO2003033603A1 (en) | 2001-10-17 | 2003-04-24 | Efka Additives B.V. | Levelling agent and anti-cratering agent |
| US7217424B2 (en) * | 2001-10-17 | 2007-05-15 | Croda, Inc. | Compositions containing esters of aromatic alkoxylated alcohols and fatty carboxylic acids |
| JP2005516045A (ja) * | 2002-01-31 | 2005-06-02 | クローダ，インコーポレイテッド | オリゴエステルを含む添加剤および生成物 |
| US7301031B2 (en) * | 2002-09-09 | 2007-11-27 | Biocatalytics, Inc. | Methods for producing hydroxy amino acids, esters, and derivatives thereof |
| US6833471B2 (en) * | 2002-09-09 | 2004-12-21 | Biocatalytics, Inc. | Methods for producing hydroxy amino acids and derivatives thereof |
| US7459460B2 (en) * | 2003-05-28 | 2008-12-02 | Bristol-Myers Squibb Company | Trisubstituted heteroaromatic compounds as calcium sensing receptor modulators |
| US7307183B2 (en) * | 2003-07-29 | 2007-12-11 | Great Lakes Chemical Corporation | Process for producing tetrabromobenzoate esters |
| JP2005170803A (ja) * | 2003-12-08 | 2005-06-30 | Daicel Chem Ind Ltd | 新規なマロン酸モノメチル誘導体とその製造法 |
| ES2398923T3 (es) * | 2006-02-24 | 2013-03-22 | Lubrizol Advanced Materials, Inc. | Polímeros que contienen macrómeros de copoliol de silicona y composiciones para higiene personal que los contienen |
| JP5157154B2 (ja) * | 2006-12-20 | 2013-03-06 | Ｄｉｃ株式会社 | ４’−（アルコキシカルボニル）ビシクロヘキシル−４−イルカルボン酸及びその製造方法 |
-
2008
- 2008-05-30 US US12/156,448 patent/US8338635B2/en not_active Expired - Fee Related
- 2008-05-30 JP JP2010510367A patent/JP2010533644A/ja active Pending
- 2008-05-30 WO PCT/US2008/006907 patent/WO2008150487A2/en not_active Ceased
-
2012
- 2012-11-16 US US13/679,411 patent/US20130150613A1/en not_active Abandoned
-
2013
- 2013-08-07 JP JP2013163978A patent/JP2013227345A/ja active Pending
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