JP2010519093A - 熱保護材料およびその製造方法 - Google Patents
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B33/00—Layered products characterised by particular properties or particular surface features, e.g. particular surface coatings; Layered products designed for particular purposes not covered by another single class
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2305/00—Condition, form or state of the layers or laminate
- B32B2305/10—Fibres of continuous length
- B32B2305/20—Fibres of continuous length in the form of a non-woven mat
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2305/00—Condition, form or state of the layers or laminate
- B32B2305/22—Fibres of short length
- B32B2305/28—Fibres of short length in the form of a mat
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/30—Properties of the layers or laminate having particular thermal properties
- B32B2307/306—Resistant to heat
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2309/00—Parameters for the laminating or treatment process; Apparatus details
- B32B2309/08—Dimensions, e.g. volume
- B32B2309/10—Dimensions, e.g. volume linear, e.g. length, distance, width
- B32B2309/105—Thickness
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2311/00—Metals, their alloys or their compounds
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B37/00—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding
- B32B37/12—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by using adhesives
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/27—Web or sheet containing structurally defined element or component, the element or component having a specified weight per unit area [e.g., gms/sq cm, lbs/sq ft, etc.]
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/28—Web or sheet containing structurally defined element or component and having an adhesive outermost layer
Abstract
Description
カーボンナノチューブの不織シートを、図1、2および2Aに示されるシステム10を使用してCVD法によって製造する。ナノチューブを気相中で製造し、上記のように移動ベルト上に堆積する。一態様において、密度約1mg/cm2の不織シートを作るために複数の層が必要である。不織シートの密度は、広い範囲、例えば少なくとも約0.1mg/cm2から5mg/cm2超まで、で制御されうる。そのような不織シートの例を、図3に項目30として示す。
不織シート30を熱保護または熱の取り扱い用途で用いるために、一態様において、不織シート30は支持材料に結合されうる。支持材料の例としては、Nomex(登録商標)または、金属、例えばアルミホイル、構造アルミニウムコンポネント、ステンレス鋼、インコンテル(Incontel)、チタンなど、を含む、熱保護が所望される他のあらゆるタイプのテキスタイルもしくは支持体が挙げられる。
別の態様において、本発明の不織カーボンナノチューブシート、例えばシート30、または熱保護シート41を、ポリウレアメチルビニルシラザンCeraset(商標)(Kion Corporation,ペンシルヴェニア州ハンテンドンバレー)(以下、「Ceraset」という。)で被覆して不織シートまたは熱保護シート41の強度およびその耐酸化特性を高めてもよい。もちろん、不織カーボンナノチューブシートまたは熱保護シート41は、この材料のコーティングなしに使用されうる。
実施例IIに記述される被覆技術の別の適用は、Ceraset被覆熱保護シート41を未処理熱保護シート41上に層状構造で重ねることを含む(すなわち、少なくとも一枚の熱保護シートを二枚のウレアシラザン被覆熱保護シートの間にサンドイッチする。)。このタイプの層状構造は、一態様において、燃焼せずに熱が効果的に移動させられるように、実質的に耐酸化性の外部層(すなわち、Ceraset被覆熱保護シート)と、非常に熱伝導性である内部層(すなわち、未処理熱保護シート)と、をもたらすと予想される。
Claims (33)
- ナノチューブの不織シート;
該不織シートに近接する支持材料;および
該不織シートと該支持材料との間に位置する接着材料
を含有する熱保護材料。 - 該不織ナノチューブシートの密度が少なくとも約0.1mg/cm2から5mg/cm2超までである、請求項1に記載の材料。
- 該不織ナノチューブシートの公称強度が約10Kpsi〜約20Kpsiである、請求項1に記載の材料。
- 該不織ナノチューブシートの引張強度が40MPaを超える、請求項1に記載の材料。
- 該支持材料が、Nomex(登録商標)、アルミホイル、構造アルミニウムコンポネント、ステンレス鋼、インコンテル、チタン、または熱保護が所望される他のいずれかのタイプのテキスタイル、金属、もしくは支持体のいずれか一種類を含む、請求項1に記載の材料。
- 該接着材料がガラス状炭素前駆材料を含む、請求項1に記載の材料。
- 該接着材料が比較的高い熱の存在下において、溶融したり破壊的に燃焼したりするというよりもむしろチャーを形成しうる、請求項1に記載の材料。
- 該接着材料がPVA、フルフリルアルコール、またはRESOL(登録商標)樹脂のいずれか一種類を含む、請求項1に記載の材料。
- 該材料が実質的に燃焼せずに約500℃までの熱に耐えうる、請求項1に記載の材料。
- 強度および耐酸化性を高めうるコーティングを更に含む、請求項1に記載の材料。
- 該コーティングが、ポリウレアメチルビニルシラザン、ポリカルボシラン、または類似の化合物のいずれか一種類を含む、請求項10に記載の材料。
- 該材料が実質的に燃焼せずに1000℃以上の熱に耐えうる、請求項10に記載の材料。
- 該材料の強度が約30MPaから約300MPa超まで増加している、請求項10に記載の材料。
- ナノチューブの不織シートを提供する工程;
支持材料を、該不織シートと支持材料との間に位置する接着材料を用いて該不織シートに結合させる工程;および
該不織ナノチューブシートと該支持材料とを不活性雰囲気中で熱分解してその間に薄いガラス状炭素結合層を形成する工程
を包含する、熱保護材料の製造方法。 - 該結合させる工程において、該接着材料がガラス状炭素前駆体を含む、請求項14に記載の方法。
- 該結合させる工程において、該ガラス状炭素前駆体が、レゾール樹脂、リンゴ酸触媒フルフリルアルコール、またはPVAの一種類である、請求項15に記載の方法。
- 該熱分解させる工程が不活性雰囲気または真空において行う工程を含む、請求項14に記載の方法。
- 該材料をポリウレアメチルビニルシラザン、ポリカルボシラン、または強度および耐酸化性を高めうる類似の化合物の一種類でコーティングする工程を更に含む、請求項14に記載の方法。
- 該コーティングする工程が該ポリウレアメチルビニルシラザンをアセトン溶液中に約1%〜約20%の濃度で溶解させる工程を含む、請求項18に記載の方法。
- 該被覆材料を約50℃〜約300℃の高温においてホットプレスする工程を更に含む、請求項18に記載の方法。
- 該ホットプレスする工程が該被覆材料を約1,000psi〜約20,000psiの圧力に曝す工程を含む、請求項20に記載の方法。
- ナノチューブの第一不織シート、該第一不織シートに近接する支持材料、および該第一不織シートと該支持材料との間に位置する接着材料を有する第一層;並びに
該第一層に近接する第二層であって、ナノチューブの第二不織シート、該第二不織シートに近接する支持材料、該第二不織シートと該支持材料との間に位置する接着材料、および該第二層の強度および耐酸化性を高めるコーティングを有する第二層
を備える熱保護材料。 - 該支持材料が、Nomex(登録商標)、アルミホイル、構造アルミニウムコンポネント、ステンレス鋼、インコンテル、チタン、または熱保護が所望される他のいずれかのタイプのテキスタイル、金属、もしくは支持体の一種類を含む、請求項22に記載の材料。
- 熱を熱源から放熱源へと輸送する役割を果たすように、熱源と放熱源との間に置かれるようにデザインされたナノチューブの不織シートを含有する、熱輸送材料。
- 該不織ナノチューブシートの熱輸送能力が横方向に存在する、請求項24に記載の材料。
- 該不織ナノチューブシートの熱輸送能力がシートの面内の横断方向に存在する、請求項25に記載の材料。
- 該ナノチューブの不織シートに結合した支持体を更に含む、請求項25に記載の材料。
- ナノ繊維不織シート形成装置であって、
合成ナノチューブの流れが該装置に入る入口を有するハウジング;
合成ナノチューブの流れに対して実質的に平行に配置された、該入口を通じて入るナノチューブを収集するためのアッセンブリ;
不織シートを形成するように、該アッセンブリの周りに位置する移動表面であって、その上に、合成ナノチューブが実質的に連続的に堆積させられる移動表面;および
該ナノチューブの不織シートをハウジングから移動させるための出口
を備える、装置。 - 該ハウジングが実質的に気密であり、ナノチューブおよび関連微粒子の該ハウジング内からの空中放出を最小にしている、請求項28に記載の装置。
- 該アッセンブリが、ナノチューブの流れよりも相対的に幅広いシートを生成するために、該入口を横切るナノチューブの流れに対して実質的に横断方向に、該ハウジングの片側から該ハウジングの反対側へと移動する能力を含む、請求項28に記載の装置。
- 該アッセンブリがナノチューブの不織シートの移動を容易にするために出口を通じてハウジングから引っ張られるように、該アッセンブリがスライドアームを含む、請求項28に記載の装置。
- 該移動表面が該アッセンブリ上の互いに対向する回転エレメントの周りに配置されたベルトである、請求項28に記載の装置。
- 該移動表面が、ナノチューブをその上に引きつける能力を有する材料を含む、請求項28に記載の装置。
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US90376707P | 2007-02-27 | 2007-02-27 | |
US60/903,767 | 2007-02-27 | ||
PCT/US2008/002548 WO2008106143A2 (en) | 2007-02-27 | 2008-02-27 | Materials for thermal protection and methods of manufacturing same |
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JP2010519093A true JP2010519093A (ja) | 2010-06-03 |
JP5595737B2 JP5595737B2 (ja) | 2014-09-24 |
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US (2) | US20090047513A1 (ja) |
EP (2) | EP2125359B1 (ja) |
JP (1) | JP5595737B2 (ja) |
AU (1) | AU2008219693B2 (ja) |
CA (1) | CA2679401A1 (ja) |
WO (1) | WO2008106143A2 (ja) |
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AU2008219693A1 (en) | 2008-09-04 |
EP2125359B1 (en) | 2016-07-27 |
EP2125359A2 (en) | 2009-12-02 |
EP2962986A1 (en) | 2016-01-06 |
EP2125359A4 (en) | 2012-09-19 |
EP2962986B1 (en) | 2017-04-05 |
CA2679401A1 (en) | 2008-09-04 |
WO2008106143A2 (en) | 2008-09-04 |
AU2008219693B2 (en) | 2012-04-12 |
JP5595737B2 (ja) | 2014-09-24 |
US20090047513A1 (en) | 2009-02-19 |
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US20190202187A1 (en) | 2019-07-04 |
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