JP2009522366A - 改善されたフッ素化反応器 - Google Patents

改善されたフッ素化反応器 Download PDF

Info

Publication number
JP2009522366A
JP2009522366A JP2008549557A JP2008549557A JP2009522366A JP 2009522366 A JP2009522366 A JP 2009522366A JP 2008549557 A JP2008549557 A JP 2008549557A JP 2008549557 A JP2008549557 A JP 2008549557A JP 2009522366 A JP2009522366 A JP 2009522366A
Authority
JP
Japan
Prior art keywords
reaction
reactor
fluoride
composition
organic compound
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
JP2008549557A
Other languages
English (en)
Japanese (ja)
Other versions
JP2009522366A5 (enExample
Inventor
ラリー，マシュー・エイチ
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Honeywell International Inc
Original Assignee
Honeywell International Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Honeywell International Inc filed Critical Honeywell International Inc
Publication of JP2009522366A publication Critical patent/JP2009522366A/ja
Publication of JP2009522366A5 publication Critical patent/JP2009522366A5/ja
Withdrawn legal-status Critical Current

Links

Images

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/0242—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid flow within the bed being predominantly vertical
    • B01J8/025—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid flow within the bed being predominantly vertical in a cylindrical shaped bed
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/013—Preparation of halogenated hydrocarbons by addition of halogens
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B39/00—Halogenation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/07—Preparation of halogenated hydrocarbons by addition of hydrogen halides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
    • C07C17/10—Preparation of halogenated hydrocarbons by replacement by halogens of hydrogen atoms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/0053—Controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00743—Feeding or discharging of solids
    • B01J2208/00752—Feeding
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00743—Feeding or discharging of solids
    • B01J2208/00761—Discharging
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00946—Features relating to the reactants or products
    • B01J2208/00955—Sampling of the particulate material, the reactants or the products
    • B01J2208/00973—Products
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00027—Process aspects
    • B01J2219/00038—Processes in parallel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00191—Control algorithm
    • B01J2219/00193—Sensing a parameter
    • B01J2219/00195—Sensing a parameter of the reaction system
    • B01J2219/00202—Sensing a parameter of the reaction system at the reactor outlet
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00191—Control algorithm
    • B01J2219/00211—Control algorithm comparing a sensed parameter with a pre-set value
    • B01J2219/00213—Fixed parameter value
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00191—Control algorithm
    • B01J2219/00222—Control algorithm taking actions
    • B01J2219/00227—Control algorithm taking actions modifying the operating conditions
    • B01J2219/00229—Control algorithm taking actions modifying the operating conditions of the reaction system
    • B01J2219/00231—Control algorithm taking actions modifying the operating conditions of the reaction system at the reactor inlet
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Fluid Mechanics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Separation Of Gases By Adsorption (AREA)
JP2008549557A 2006-01-04 2007-01-03 改善されたフッ素化反応器 Withdrawn JP2009522366A (ja)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US11/326,379 US7247759B1 (en) 2006-01-04 2006-01-04 Fluorination reactor
PCT/US2007/000171 WO2007089386A2 (en) 2006-01-04 2007-01-03 Improved fluoriation reactor

Related Child Applications (1)

Application Number Title Priority Date Filing Date
JP2013229238A Division JP2014055152A (ja) 2006-01-04 2013-11-05 改善されたフッ素化反応器

Publications (2)

Publication Number Publication Date
JP2009522366A true JP2009522366A (ja) 2009-06-11
JP2009522366A5 JP2009522366A5 (enExample) 2010-02-12

Family

ID=38224624

Family Applications (2)

Application Number Title Priority Date Filing Date
JP2008549557A Withdrawn JP2009522366A (ja) 2006-01-04 2007-01-03 改善されたフッ素化反応器
JP2013229238A Pending JP2014055152A (ja) 2006-01-04 2013-11-05 改善されたフッ素化反応器

Family Applications After (1)

Application Number Title Priority Date Filing Date
JP2013229238A Pending JP2014055152A (ja) 2006-01-04 2013-11-05 改善されたフッ素化反応器

Country Status (7)

Country Link
US (2) US7247759B1 (enExample)
EP (1) EP1968921A2 (enExample)
JP (2) JP2009522366A (enExample)
KR (1) KR101352471B1 (enExample)
CN (1) CN101365669B (enExample)
RU (1) RU2446139C2 (enExample)
WO (1) WO2007089386A2 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPWO2019116789A1 (ja) * 2017-12-12 2021-01-07 昭和電工株式会社 含フッ素有機化合物の製造方法及び製造装置

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20150093316A1 (en) * 2013-09-30 2015-04-02 Honeywell International, Inc. Purification of pf5
CN108940129A (zh) * 2018-08-29 2018-12-07 山东重山光电材料股份有限公司 一种多级利用氟化剂生产氟化碳材料的系统及生产方法
JP7353012B2 (ja) * 2019-08-22 2023-09-29 フジアン ヨンジン テクノロジー カンパニー リミテッド 直接フッ素化によるフルオロベンゼンの製造プロセス
CN113289557B (zh) * 2021-06-16 2023-05-09 武汉松石科技股份有限公司 一种有机物氟化气液反应系统

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS56142222A (en) * 1980-03-14 1981-11-06 Hoechst Ag Manufacture of high purity partially fluorinated ethane
JPS63501297A (ja) * 1985-11-08 1988-05-19 イクスフロア−・リサ−チ・コ−ポレ−ション エ−テル類のペルフルオル化
JPH02117626A (ja) * 1988-10-26 1990-05-02 Osaka Gas Co Ltd フッ素化反応装置
JPH0657475A (ja) * 1992-08-07 1994-03-01 Tokuyama Soda Co Ltd フッ素化合物の製造方法
JPH06305993A (ja) * 1993-04-03 1994-11-01 Solvay Fluor & Derivate Gmbh ペルフルオロアルカンの製造方法
WO2004035518A1 (ja) * 2002-10-18 2004-04-29 Asahi Glass Company, Limited フッ素化された化合物の製造方法、およびフッ素化装置

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4377715A (en) 1979-12-26 1983-03-22 Allied Corporation Production of perfluoropropane
JPS59204146A (ja) * 1983-04-30 1984-11-19 Central Glass Co Ltd 含フツ素有機化合物の精製法
FR2556340B1 (fr) * 1983-12-13 1986-05-16 Atochem Procede catalytique de preparation d'hexafluoroacetone
JPS60137928A (ja) * 1983-12-26 1985-07-22 Daikin Ind Ltd 新規含フツ素ポリエ−テルおよびその製法
IT1184149B (it) * 1985-03-11 1987-10-22 Montefluos Spa Processo per la preparazione di fluorossi-alo-composti
US4680406A (en) * 1985-10-15 1987-07-14 The Dow Chemical Company Process for fluorinating halogenated organo-compounds
US5093432A (en) * 1988-09-28 1992-03-03 Exfluor Research Corporation Liquid phase fluorination
AU4416289A (en) * 1988-09-28 1990-04-18 Exfluor Research Corporation Liquid phase fluorination
US4990701A (en) * 1990-03-20 1991-02-05 E. I. Dupont De Nemours And Company Halogen exchange fluorination
DE4419534C1 (de) * 1994-06-03 1995-10-19 Hoechst Ag Verfahren zur Regenerierung eines chrom- und magnesiumhaltigen Fluorierungskatalysators
US5675046A (en) 1996-04-10 1997-10-07 Showa Denko K.K. Process for producing perfluorocarbon
JP3792051B2 (ja) * 1997-09-17 2006-06-28 日本ゼオン株式会社 パーハロゲン化シクロペンテンの製造方法
ES2230833T3 (es) * 1998-01-16 2005-05-01 Alliedsignal Inc. Metodo de produccion de compuestos organicos fluorados.
US20020156321A1 (en) * 2001-02-13 2002-10-24 Syvret Robert George Continuous preparation of high purity Bis(fluoroxy)difluoromethane (BDM) at elevated pressure
JP5025052B2 (ja) * 2001-08-06 2012-09-12 昭和電工株式会社 ヘキサフルオロエタンの製造方法およびその用途
DE10159940B4 (de) 2001-12-06 2007-02-08 Air Liquide Deutschland Gmbh Vorrichtung und Verfahren zur Fluorierung von Formteilen aus Kunststoff mit einem fluorhaltigen Gasgemisch
US7557227B2 (en) * 2003-02-17 2009-07-07 Asahi Glass Company, Limited Process for producing hexafluoropropylene oxide

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS56142222A (en) * 1980-03-14 1981-11-06 Hoechst Ag Manufacture of high purity partially fluorinated ethane
JPS63501297A (ja) * 1985-11-08 1988-05-19 イクスフロア−・リサ−チ・コ−ポレ−ション エ−テル類のペルフルオル化
JPH02117626A (ja) * 1988-10-26 1990-05-02 Osaka Gas Co Ltd フッ素化反応装置
JPH0657475A (ja) * 1992-08-07 1994-03-01 Tokuyama Soda Co Ltd フッ素化合物の製造方法
JPH06305993A (ja) * 1993-04-03 1994-11-01 Solvay Fluor & Derivate Gmbh ペルフルオロアルカンの製造方法
WO2004035518A1 (ja) * 2002-10-18 2004-04-29 Asahi Glass Company, Limited フッ素化された化合物の製造方法、およびフッ素化装置

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPWO2019116789A1 (ja) * 2017-12-12 2021-01-07 昭和電工株式会社 含フッ素有機化合物の製造方法及び製造装置
JP7203045B2 (ja) 2017-12-12 2023-01-12 昭和電工株式会社 含フッ素有機化合物の製造方法

Also Published As

Publication number Publication date
US20070154368A1 (en) 2007-07-05
RU2446139C2 (ru) 2012-03-27
KR20080083036A (ko) 2008-09-12
US7731911B2 (en) 2010-06-08
KR101352471B1 (ko) 2014-01-17
US20070155996A1 (en) 2007-07-05
CN101365669B (zh) 2013-11-20
CN101365669A (zh) 2009-02-11
JP2014055152A (ja) 2014-03-27
WO2007089386A3 (en) 2007-09-20
EP1968921A2 (en) 2008-09-17
US7247759B1 (en) 2007-07-24
RU2008131767A (ru) 2010-02-10
WO2007089386A2 (en) 2007-08-09

Similar Documents

Publication Publication Date Title
KR102863123B1 (ko) 트라이플루오로요오도메탄 및 트라이플루오로아세틸 요오다이드의 제조 방법
JP5827628B2 (ja) （ｅ）−１−クロロ−３，３，３−トリフルオロプロペンを製造する統合プロセス及び方法
US20120123172A1 (en) Production Method Of Trans-1,3,3,3-Tetrafluoropropene
JP2014055152A (ja) 改善されたフッ素化反応器
EP2341040A1 (en) Process for producing 1,3,3,3-tetrafluoropropene
US8293953B2 (en) Method for producing 1, 1-dichloro-2,2,3,3,3-pentafluoropropane
JPWO2011162341A1 (ja) ２，３，３，３−テトラフルオロプロペンの製造方法
CA2152940C (en) A method of producing 1,1,1,3,3-pentafluoropropane, a method of producing 1,1,1,3,3-pentafluoro-2-halogeno-3-chloropropane, and a method of producing 1,1,1,2,3,3-hexachloropropene
US10988425B2 (en) One step process for manufacturing trifluoroiodomethane from trifluoroacetyl halide, hydrogen, and iodine
JP6780656B2 (ja) ハイドロフルオロオレフィンの製造方法
KR20210095215A (ko) 트라이플루오로요오도메탄을 제조하기 위한 촉매 및 통합된 방법
CN101646640B (zh) 含氯含氟化合物的制造方法
CN104496746B (zh) 一种同时制备1,1,1,2,2-五氯丙烷和2,3,3,3-四氯丙烯的方法
JP5712894B2 (ja) （ｚ）−１−クロロ−３，３，３−トリフルオロプロペンの製造方法
US20240425435A1 (en) An integrated process for producing trifluoroiodomethane
JP2002069014A (ja) オクタフルオロプロパンの製造方法及びその用途
Quan et al. Preparation and application of porous calcium fluoride—a novel fluorinating reagent and support of catalyst
JP3105321B2 (ja) フッ素含有エタン誘導体の製法
KR102914755B1 (ko) 트라이플루오로아세틸 할라이드, 수소, 및 요오드로부터 트라이플루오로요오도메탄을 제조하기 위한 1-단계 방법
CN113710636A (zh) 氢氯氟烃的制造方法、1-氯-2,3,3-三氟丙烯的制造方法、1-氯-2,3,3,4,4,5,5-七氟-1-戊烯的制造方法
CN114105728B (zh) 同时制备e-1,3,3,3-四氯丙烯和1,1,3,3-四氯丙烯的方法
JP2019151629A (ja) 化合物の製造方法
CN1054582A (zh) 卤素交换氟化反应
KR20000076122A (ko) 플루오르화 방법

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20091221

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20091221

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20120523

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20120619

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20120918

A602 Written permission of extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A602

Effective date: 20120925

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20121019

A02 Decision of refusal

Free format text: JAPANESE INTERMEDIATE CODE: A02

Effective date: 20130702

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20131105

A911 Transfer to examiner for re-examination before appeal (zenchi)

Free format text: JAPANESE INTERMEDIATE CODE: A911

Effective date: 20131112

A912 Re-examination (zenchi) completed and case transferred to appeal board

Free format text: JAPANESE INTERMEDIATE CODE: A912

Effective date: 20131213

A761 Written withdrawal of application

Free format text: JAPANESE INTERMEDIATE CODE: A761

Effective date: 20140410