JP2008302580A - 光学フィルム用粘着シート、その製造方法、粘着型光学フィルムおよび画像表示装置 - Google Patents
光学フィルム用粘着シート、その製造方法、粘着型光学フィルムおよび画像表示装置 Download PDFInfo
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- JP2008302580A JP2008302580A JP2007151611A JP2007151611A JP2008302580A JP 2008302580 A JP2008302580 A JP 2008302580A JP 2007151611 A JP2007151611 A JP 2007151611A JP 2007151611 A JP2007151611 A JP 2007151611A JP 2008302580 A JP2008302580 A JP 2008302580A
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- HTEAGOMAXMOFFS-UHFFFAOYSA-N methyl 2-methylprop-2-enoate;prop-2-enoic acid Chemical compound OC(=O)C=C.COC(=O)C(C)=C HTEAGOMAXMOFFS-UHFFFAOYSA-N 0.000 description 1
- 229920000609 methyl cellulose Polymers 0.000 description 1
- 239000001923 methylcellulose Substances 0.000 description 1
- 235000010981 methylcellulose Nutrition 0.000 description 1
- LVHBHZANLOWSRM-UHFFFAOYSA-N methylenebutanedioic acid Natural products OC(=O)CC(=C)C(O)=O LVHBHZANLOWSRM-UHFFFAOYSA-N 0.000 description 1
- 239000010445 mica Substances 0.000 description 1
- 229910052618 mica group Inorganic materials 0.000 description 1
- 239000011859 microparticle Substances 0.000 description 1
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- CWQXQMHSOZUFJS-UHFFFAOYSA-N molybdenum disulfide Chemical compound S=[Mo]=S CWQXQMHSOZUFJS-UHFFFAOYSA-N 0.000 description 1
- PHQOGHDTIVQXHL-UHFFFAOYSA-N n'-(3-trimethoxysilylpropyl)ethane-1,2-diamine Chemical compound CO[Si](OC)(OC)CCCNCCN PHQOGHDTIVQXHL-UHFFFAOYSA-N 0.000 description 1
- SJPFBRJHYRBAGV-UHFFFAOYSA-N n-[[3-[[bis(oxiran-2-ylmethyl)amino]methyl]phenyl]methyl]-1-(oxiran-2-yl)-n-(oxiran-2-ylmethyl)methanamine Chemical compound C1OC1CN(CC=1C=C(CN(CC2OC2)CC2OC2)C=CC=1)CC1CO1 SJPFBRJHYRBAGV-UHFFFAOYSA-N 0.000 description 1
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- ZQXSMRAEXCEDJD-UHFFFAOYSA-N n-ethenylformamide Chemical compound C=CNC=O ZQXSMRAEXCEDJD-UHFFFAOYSA-N 0.000 description 1
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- 125000002560 nitrile group Chemical group 0.000 description 1
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- 125000001400 nonyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
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- SRSFOMHQIATOFV-UHFFFAOYSA-N octanoyl octaneperoxoate Chemical compound CCCCCCCC(=O)OOC(=O)CCCCCCC SRSFOMHQIATOFV-UHFFFAOYSA-N 0.000 description 1
- 125000002347 octyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 239000011368 organic material Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- VTRUBDSFZJNXHI-UHFFFAOYSA-N oxoantimony Chemical compound [Sb]=O VTRUBDSFZJNXHI-UHFFFAOYSA-N 0.000 description 1
- 125000004430 oxygen atom Chemical group O* 0.000 description 1
- 229910052763 palladium Inorganic materials 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 125000001147 pentyl group Chemical group C(CCCC)* 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 125000002080 perylenyl group Chemical group C1(=CC=C2C=CC=C3C4=CC=CC5=CC=CC(C1=C23)=C45)* 0.000 description 1
- 238000009832 plasma treatment Methods 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 229920002037 poly(vinyl butyral) polymer Polymers 0.000 description 1
- 229920006122 polyamide resin Polymers 0.000 description 1
- 229920002857 polybutadiene Polymers 0.000 description 1
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- 229920000570 polyether Polymers 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920013716 polyethylene resin Polymers 0.000 description 1
- 239000009719 polyimide resin Substances 0.000 description 1
- 229920001195 polyisoprene Polymers 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 229920006380 polyphenylene oxide Polymers 0.000 description 1
- 229920000069 polyphenylene sulfide Polymers 0.000 description 1
- 229920001451 polypropylene glycol Polymers 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 229920005990 polystyrene resin Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- UIIIBRHUICCMAI-UHFFFAOYSA-N prop-2-ene-1-sulfonic acid Chemical compound OS(=O)(=O)CC=C UIIIBRHUICCMAI-UHFFFAOYSA-N 0.000 description 1
- AAYRWMCIKCRHIN-UHFFFAOYSA-N propane-1-sulfonic acid;prop-2-enamide Chemical compound NC(=O)C=C.CCCS(O)(=O)=O AAYRWMCIKCRHIN-UHFFFAOYSA-N 0.000 description 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
- 239000007870 radical polymerization initiator Substances 0.000 description 1
- 238000010526 radical polymerization reaction Methods 0.000 description 1
- 229920005604 random copolymer Polymers 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 238000007142 ring opening reaction Methods 0.000 description 1
- 238000005488 sandblasting Methods 0.000 description 1
- 238000007127 saponification reaction Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 229920006300 shrink film Polymers 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 229910052814 silicon oxide Inorganic materials 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 239000002356 single layer Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 125000004079 stearyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000010558 suspension polymerization method Methods 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 239000000057 synthetic resin Substances 0.000 description 1
- 229920006027 ternary co-polymer Polymers 0.000 description 1
- OPQYOFWUFGEMRZ-UHFFFAOYSA-N tert-butyl 2,2-dimethylpropaneperoxoate Chemical compound CC(C)(C)OOC(=O)C(C)(C)C OPQYOFWUFGEMRZ-UHFFFAOYSA-N 0.000 description 1
- NMOALOSNPWTWRH-UHFFFAOYSA-N tert-butyl 7,7-dimethyloctaneperoxoate Chemical compound CC(C)(C)CCCCCC(=O)OOC(C)(C)C NMOALOSNPWTWRH-UHFFFAOYSA-N 0.000 description 1
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 description 1
- 229920002803 thermoplastic polyurethane Polymers 0.000 description 1
- 229920001187 thermosetting polymer Polymers 0.000 description 1
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 description 1
- 229910001887 tin oxide Inorganic materials 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- DVKJHBMWWAPEIU-UHFFFAOYSA-N toluene 2,4-diisocyanate Chemical compound CC1=CC=C(N=C=O)C=C1N=C=O DVKJHBMWWAPEIU-UHFFFAOYSA-N 0.000 description 1
- 150000004992 toluidines Chemical class 0.000 description 1
- LDHQCZJRKDOVOX-UHFFFAOYSA-N trans-crotonic acid Natural products CC=CC(O)=O LDHQCZJRKDOVOX-UHFFFAOYSA-N 0.000 description 1
- NBXZNTLFQLUFES-UHFFFAOYSA-N triethoxy(propyl)silane Chemical compound CCC[Si](OCC)(OCC)OCC NBXZNTLFQLUFES-UHFFFAOYSA-N 0.000 description 1
- WEAPVABOECTMGR-UHFFFAOYSA-N triethyl 2-acetyloxypropane-1,2,3-tricarboxylate Chemical compound CCOC(=O)CC(C(=O)OCC)(OC(C)=O)CC(=O)OCC WEAPVABOECTMGR-UHFFFAOYSA-N 0.000 description 1
- BPSIOYPQMFLKFR-UHFFFAOYSA-N trimethoxy-[3-(oxiran-2-ylmethoxy)propyl]silane Chemical compound CO[Si](OC)(OC)CCCOCC1CO1 BPSIOYPQMFLKFR-UHFFFAOYSA-N 0.000 description 1
- YUYCVXFAYWRXLS-UHFFFAOYSA-N trimethoxysilane Chemical compound CO[SiH](OC)OC YUYCVXFAYWRXLS-UHFFFAOYSA-N 0.000 description 1
- 125000006617 triphenylamine group Chemical group 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- 239000004711 α-olefin Substances 0.000 description 1
- PAPBSGBWRJIAAV-UHFFFAOYSA-N ε-Caprolactone Chemical class O=C1CCCCCO1 PAPBSGBWRJIAAV-UHFFFAOYSA-N 0.000 description 1
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- C09J7/00—Adhesives in the form of films or foils
- C09J7/40—Adhesives in the form of films or foils characterised by release liners
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- B32B7/00—Layered products characterised by the relation between layers; Layered products characterised by the relative orientation of features between layers, or by the relative values of a measurable parameter between layers, i.e. products comprising layers having different physical, chemical or physicochemical properties; Layered products characterised by the interconnection of layers
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- C09J7/00—Adhesives in the form of films or foils
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- C09J7/22—Plastics; Metallised plastics
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- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J7/00—Adhesives in the form of films or foils
- C09J7/40—Adhesives in the form of films or foils characterised by release liners
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- G02F1/01—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour
- G02F1/13—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour based on liquid crystals, e.g. single liquid crystal display cells
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Abstract
【解決手段】離型シート上に粘着剤層を有する光学フィルム用粘着シートであって、離型シート上の粘着剤層表面の表面粗さ(Ra)が、2〜150nmである。当該光学フィルム用粘着シートは、離型シート上に粘着剤塗工液を塗工する工程、前記粘着剤塗工液に、温度30〜80℃、風速0.5〜15m/秒の第1乾燥工程、および、温度90〜160℃、風速0.1〜25m/秒の第2乾燥工程、を施すことにより粘着剤層を形成する工程を、有する製造方法により得られる。
【選択図】図1
Description
離型シート上の粘着剤層表面の表面粗さ(Ra)が、2〜150nmであることを特徴とする光学フィルム用粘着シート、に関する。
前記粘着剤塗工液に、温度30〜80℃、風速0.5〜15m/秒の第1乾燥工程、および、温度90〜160℃、風速0.1〜25m/秒の第2乾燥工程、を施すことにより粘着剤層を形成する工程を、有することを特徴とする光学フィルム用粘着シートの製造方法、に関する。
光学フィルム用粘着シートが、請求項1記載の光学フィルム用粘着シートであり、表面粗さ(Ra)2〜150nmの粘着剤層表面に、光学フィルムを貼り合わせていること特徴とする粘着型光学フィルム、に関する。
<アクリル系粘着剤の調製>
窒素導入管、冷却管を備えた4つ口フラスコに、ブチルアクリレート96.5部、アクリル酸3部、2−ヒドロキシエチルアクリレート0.5部、2,2´‐アゾビスイソブチロニトリル0.15部および酢酸エチル100重量部を投入し、十分に窒素置換した後、窒素気流下で撹拌しながら、60℃で8時間反応して、重量平均分子量165万のアクリル系ポリマー溶液を得た。上記アクリル系ポリマー溶液の固形分100部に対して、イソシアネート系架橋剤(日本ポリウレタン(株)製,コロネートL)0.5部を配合し、粘着剤塗工液(固形分12%)を調製した。
<アクリル系粘着剤の調製>
窒素導入管、冷却管を備えた4つ口フラスコに、ブチルアクリレート99.5部、4−ヒドロキシブチルアクリレート0.5部、2,2´‐アゾビスイソブチロニトリル0.15部および酢酸エチル100重量部を投入し、十分に窒素置換した後、窒素気流下で撹拌しながら、60℃で8時間反応して、重量平均分子量165万のアクリル系ポリマー溶液を得た。上記アクリル系ポリマー溶液の固形分100部に対して、架橋剤として、イソシアネート系架橋剤(日本ポリウレタン(株)製,コロネートL)0.2部配合し、粘着剤塗工液(固形分11.5%)を調製した。
<アクリル系粘着剤の調製>
窒素導入管、冷却管を備えた4つ口フラスコに、ブチルアクリレート90部、アクリル酸4部、アクリロイルモルホリン5部、4−ヒドロキシエチルアクリレート1部、2,2´‐アゾビスイソブチロニトリル0.15部および酢酸エチル100重量部を投入し、十分に窒素置換した後、窒素気流下で撹拌しながら、60℃で8時間反応して、重量平均分子量165万のアクリル系ポリマー溶液を得た。上記アクリル系ポリマー溶液の固形分100部に対して、架橋剤として、イソシアネート系架橋剤(日本ポリウレタン(株)製,コロネートL)0.3部配合し、粘着剤塗工液(固形分11.5%)を調製した。
厚さ80μmのポリビニルアルコールフィルムをヨウ素水溶液中で5倍に延伸した後に乾燥させて偏光子を得た。当該偏光子の両側に、透明保護フィルム(トリアセチルセルロースフィルム,厚さ80μm)をポリビニルアルコール系接着剤により、貼り合わせて偏光板を得た。
離型処理を施したポリエステルフィルム(離型シート,三菱化学ポリエステル社製、商品名ダイヤホイルMRF#38,厚さ38μm)の離型処理面(表面粗さ21nm)上に、製造例1で得られた粘着剤塗工液を、乾燥厚さが25μmになるように、ダイコーターにより塗工した後、70℃のオーブン中にて、風速14m/秒の風を1分間送ることにより第1乾燥工程を施した。次いで、温度155℃、風速15m/秒の風を2分間送ることにより第2乾燥工程を施して、粘着剤層を形成して、光学フィルム用粘着シートを得た。
実施例1において、粘着剤塗工液の種類、第1乾燥工程の条件、第2乾燥工程の条件を表1に示すように変えたこと以外は実施例1と同様にして光学フィルム用粘着シートを得た。
得られた光学フィルム用粘着シートの粘着剤層に、別の離型シート(離型処理を施したポリエステルフィルム,三菱化学ポリエステル社製、商品名ダイヤホイルMRF#38,厚さ38μm)を貼り合わせた。その後、元から貼られていた離型シートを剥離し、ガラス(マツナミガラス社製,MICROSLIDE GLASS)に貼り付けたものをサンプルとした。当該サンプルについて、後で貼り合わせた離型シートが上になるように置き、WYKO NT3300(非接触三次元粗さ測定装置,日本ビーコ社製)を用いて、表面粗さを測定した。測定は、20mm×20mmの範囲で観察し、粘着剤層の塗工方向と垂直な方向に5mmおきに3点、表面粗さを算出した。表1には、表面粗さの平均値ととともに、3点の測定値(かっこ内)を示す。なお、表面粗さ(Ra)JISB0601に準拠して測定される値である。
離型シート側の粘着剤層のRaは、離型シートの離型処理面のRaを写し取ったものである。従って、離型シート側の粘着剤層のRaは、微細形状測定器(三次元表面形状測定器)ET4000(小坂研究所製)を用いて、離型シートの離型処理面の表面粗さを測定した。測定は、20mm×20mmの範囲で観察し、粘着剤層の塗工方向と垂直な方向に測定した。なお、表面粗さ(Ra)JISB0601に準拠して測定される値である。
得られた光学フィルム用粘着シートの粘着剤層を、偏光板に転写して、粘着型偏光板を作成した。当該粘着型偏光板から、離型シートを剥離した後、シャープ(株)製の携帯用パネルに貼り合わせ、目視で、下記基準により、正面および斜め45°の2方向から視認性の観察を行った。
◎:視認性に問題なし。
○:多少のムラは確認させるが問題ないレベル。
×:視認性に問題あり。
2 粘着剤層
2a 表面粗さ(Ra)が、2〜150nmの粘着剤層表面
3 光学フィルム
Claims (4)
- 離型シート上に粘着剤層を有する光学フィルム用粘着シートであって、
離型シート上の粘着剤層表面の表面粗さ(Ra)が、2〜150nmであることを特徴とする光学フィルム用粘着シート。 - 請求項1記載の光学フィルム用粘着シートの製造方法であって、
離型シート上に粘着剤塗工液を塗工する工程、
前記粘着剤塗工液に、温度30〜80℃、風速0.5〜15m/秒の第1乾燥工程、および、温度90〜160℃、風速0.1〜25m/秒の第2乾燥工程、を施すことにより粘着剤層を形成する工程を、有することを特徴とする光学フィルム用粘着シートの製造方法。 - 離型シート上に粘着剤層を有する光学フィルム用粘着シートの粘着剤層表面に、光学フィルムを貼り合わせている粘着型光学フィルムであって、
光学フィルム用粘着シートが、請求項1記載の光学フィルム用粘着シートであり、表面粗さ(Ra)2〜150nmの粘着剤層表面に、光学フィルムを貼り合わせていること特徴とする粘着型光学フィルム。 - 請求項3記載の粘着型光学フィルムから、離型シートが剥離された粘着型光学フィルムを少なくとも1枚用いた画像表示装置。
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PCT/JP2008/060272 WO2008149890A1 (ja) | 2007-06-07 | 2008-06-04 | 光学フィルム用粘着シート、その製造方法、粘着型光学フィルムおよび画像表示装置 |
KR1020127019708A KR101667087B1 (ko) | 2007-06-07 | 2008-06-04 | 광학 필름용 점착 시트, 그 제조 방법, 점착형 광학 필름 및 화상 표시 장치 |
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CN201210381996.6A CN102909903B (zh) | 2007-06-07 | 2008-06-04 | 光学薄膜用粘合片、其制造方法、粘合型光学薄膜及图像显示装置 |
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CN2008800146415A CN101674933B (zh) | 2007-06-07 | 2008-06-04 | 光学薄膜用粘合片、其制造方法、粘合型光学薄膜及图像显示装置 |
TW097121342A TWI392591B (zh) | 2007-06-07 | 2008-06-06 | An adhesive film for an optical film, a method for manufacturing the same, an adhesive type optical film, and an image display device |
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CN102909903A (zh) | 2013-02-06 |
KR20120091469A (ko) | 2012-08-17 |
KR101912493B1 (ko) | 2018-10-26 |
CN101674933B (zh) | 2013-03-27 |
WO2008149890A1 (ja) | 2008-12-11 |
TWI392591B (zh) | 2013-04-11 |
KR20100013337A (ko) | 2010-02-09 |
CN101674933A (zh) | 2010-03-17 |
KR20150055625A (ko) | 2015-05-21 |
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JP4673344B2 (ja) | 2011-04-20 |
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