JP2005522541A5 - - Google Patents
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- Publication number
- JP2005522541A5 JP2005522541A5 JP2003584134A JP2003584134A JP2005522541A5 JP 2005522541 A5 JP2005522541 A5 JP 2005522541A5 JP 2003584134 A JP2003584134 A JP 2003584134A JP 2003584134 A JP2003584134 A JP 2003584134A JP 2005522541 A5 JP2005522541 A5 JP 2005522541A5
- Authority
- JP
- Japan
- Prior art keywords
- fluoropolymer
- dispersion
- perfluorovinyl ether
- poly
- group
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
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- 238000000034 method Methods 0.000 claims 11
- 239000006185 dispersion Substances 0.000 claims 9
- 229920002313 fluoropolymer Polymers 0.000 claims 9
- 239000004811 fluoropolymer Substances 0.000 claims 9
- RRZIJNVZMJUGTK-UHFFFAOYSA-N 1,1,2-trifluoro-2-(1,2,2-trifluoroethenoxy)ethene Chemical compound FC(F)=C(F)OC(F)=C(F)F RRZIJNVZMJUGTK-UHFFFAOYSA-N 0.000 claims 7
- 239000000178 monomer Substances 0.000 claims 6
- 125000004432 carbon atom Chemical group C* 0.000 claims 5
- 239000000203 mixture Substances 0.000 claims 4
- 239000002245 particle Substances 0.000 claims 4
- 239000003995 emulsifying agent Substances 0.000 claims 3
- 238000006116 polymerization reaction Methods 0.000 claims 3
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims 2
- 239000005977 Ethylene Substances 0.000 claims 2
- 229910052799 carbon Inorganic materials 0.000 claims 2
- -1 dichlorodifluoroethylene, trifluoroethylene Chemical group 0.000 claims 2
- 229920001519 homopolymer Polymers 0.000 claims 2
- 229910052739 hydrogen Inorganic materials 0.000 claims 2
- 239000001257 hydrogen Substances 0.000 claims 2
- 239000004615 ingredient Substances 0.000 claims 2
- 239000000463 material Substances 0.000 claims 2
- 125000005010 perfluoroalkyl group Chemical group 0.000 claims 2
- 239000003505 polymerization initiator Substances 0.000 claims 2
- 230000000379 polymerizing effect Effects 0.000 claims 2
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 claims 2
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 claims 2
- 239000000758 substrate Substances 0.000 claims 2
- BQCIDUSAKPWEOX-UHFFFAOYSA-N 1,1-Difluoroethene Chemical compound FC(F)=C BQCIDUSAKPWEOX-UHFFFAOYSA-N 0.000 claims 1
- YTCHAEAIYHLXBK-UHFFFAOYSA-N 2-chloro-1,1,3,3,3-pentafluoroprop-1-ene Chemical compound FC(F)=C(Cl)C(F)(F)F YTCHAEAIYHLXBK-UHFFFAOYSA-N 0.000 claims 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 1
- XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical group ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 125000000129 anionic group Chemical group 0.000 claims 1
- 125000004429 atom Chemical group 0.000 claims 1
- 125000002091 cationic group Chemical group 0.000 claims 1
- 150000001768 cations Chemical class 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 claims 1
- UUAGAQFQZIEFAH-UHFFFAOYSA-N chlorotrifluoroethylene Chemical group FC(F)=C(F)Cl UUAGAQFQZIEFAH-UHFFFAOYSA-N 0.000 claims 1
- 125000004122 cyclic group Chemical group 0.000 claims 1
- 230000001804 emulsifying effect Effects 0.000 claims 1
- 239000000839 emulsion Substances 0.000 claims 1
- 125000001153 fluoro group Chemical group F* 0.000 claims 1
- 125000005843 halogen group Chemical group 0.000 claims 1
- HCDGVLDPFQMKDK-UHFFFAOYSA-N hexafluoropropylene Chemical compound FC(F)=C(F)C(F)(F)F HCDGVLDPFQMKDK-UHFFFAOYSA-N 0.000 claims 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 claims 1
- 125000000962 organic group Chemical group 0.000 claims 1
- 125000004430 oxygen atom Chemical group O* 0.000 claims 1
- 125000006551 perfluoro alkylene group Chemical group 0.000 claims 1
- 229920005548 perfluoropolymer Polymers 0.000 claims 1
- 239000007870 radical polymerization initiator Substances 0.000 claims 1
- 239000002689 soil Substances 0.000 claims 1
- 150000003460 sulfonic acids Chemical class 0.000 claims 1
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10/117,714 US6822059B2 (en) | 2002-04-05 | 2002-04-05 | Dispersions containing bicomponent fluoropolymer particles and use thereof |
| PCT/US2003/004070 WO2003087179A1 (en) | 2002-04-05 | 2003-02-12 | Dispersions containing bicomponent fluoropolymer particles and use thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2005522541A JP2005522541A (ja) | 2005-07-28 |
| JP2005522541A5 true JP2005522541A5 (US07829477-20101109-C00007.png) | 2006-03-30 |
Family
ID=28789861
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2003584134A Withdrawn JP2005522541A (ja) | 2002-04-05 | 2003-02-12 | 二成分フルオロポリマー粒子を含む分散体およびその使用 |
Country Status (12)
Families Citing this family (45)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7045571B2 (en) * | 2001-05-21 | 2006-05-16 | 3M Innovative Properties Company | Emulsion polymerization of fluorinated monomers |
| US7279522B2 (en) | 2001-09-05 | 2007-10-09 | 3M Innovative Properties Company | Fluoropolymer dispersions containing no or little low molecular weight fluorinated surfactant |
| US6822059B2 (en) * | 2002-04-05 | 2004-11-23 | 3M Innovative Properties Company | Dispersions containing bicomponent fluoropolymer particles and use thereof |
| US6833418B2 (en) * | 2002-04-05 | 2004-12-21 | 3M Innovative Properties Company | Dispersions containing perfluorovinyl ether homopolymers and use thereof |
| CA2554293A1 (en) | 2004-01-30 | 2005-08-18 | Great Lakes Chemical Corporation | Production processes and systems, compositions, surfactants, monomer units, metal complexes, phosphate esters, glycols, aqueous film forming foams, and foam stabilizers |
| EP1570917B1 (en) * | 2004-03-01 | 2009-06-10 | 3M Innovative Properties Company | Method of coating a substrate with a fluoropolymer dispersion |
| US8814861B2 (en) | 2005-05-12 | 2014-08-26 | Innovatech, Llc | Electrosurgical electrode and method of manufacturing same |
| US7147634B2 (en) | 2005-05-12 | 2006-12-12 | Orion Industries, Ltd. | Electrosurgical electrode and method of manufacturing same |
| GB2427170A (en) * | 2005-06-17 | 2006-12-20 | 3M Innovative Properties Co | Fluoropolymer film having glass microspheres |
| GB0514398D0 (en) | 2005-07-15 | 2005-08-17 | 3M Innovative Properties Co | Aqueous emulsion polymerization of fluorinated monomers using a fluorinated surfactant |
| GB0525978D0 (en) * | 2005-12-21 | 2006-02-01 | 3M Innovative Properties Co | Fluorinated Surfactants For Making Fluoropolymers |
| US7795332B2 (en) | 2005-07-15 | 2010-09-14 | 3M Innovative Properties Company | Method of removing fluorinated carboxylic acid from aqueous liquid |
| GB0514387D0 (en) * | 2005-07-15 | 2005-08-17 | 3M Innovative Properties Co | Aqueous emulsion polymerization of fluorinated monomers using a perfluoropolyether surfactant |
| US20080015304A1 (en) | 2006-07-13 | 2008-01-17 | Klaus Hintzer | Aqueous emulsion polymerization process for producing fluoropolymers |
| GB0523853D0 (en) * | 2005-11-24 | 2006-01-04 | 3M Innovative Properties Co | Fluorinated surfactants for use in making a fluoropolymer |
| US7728087B2 (en) * | 2005-12-23 | 2010-06-01 | 3M Innovative Properties Company | Fluoropolymer dispersion and method for making the same |
| US9029477B2 (en) * | 2006-03-03 | 2015-05-12 | 3M Innovative Properties Company | Compositions comprising melt-processable thermoplastic fluoropolymers and methods of making the same |
| US7754795B2 (en) | 2006-05-25 | 2010-07-13 | 3M Innovative Properties Company | Coating composition |
| US20070276103A1 (en) * | 2006-05-25 | 2007-11-29 | 3M Innovative Properties Company | Fluorinated Surfactants |
| US8119750B2 (en) | 2006-07-13 | 2012-02-21 | 3M Innovative Properties Company | Explosion taming surfactants for the production of perfluoropolymers |
| KR20100017848A (ko) | 2007-05-23 | 2010-02-16 | 쓰리엠 이노베이티브 프로퍼티즈 컴파니 | 플루오르화 계면활성제의 수성 조성물 및 그의 사용 방법 |
| EP2160421A1 (en) | 2007-06-06 | 2010-03-10 | 3M Innovative Properties Company | Fluorinated ether compositions and methods of using the same |
| US8318656B2 (en) | 2007-07-03 | 2012-11-27 | E. I. Du Pont De Nemours And Company | Production processes and systems, compositions, surfactants, monomer units, metal complexes, phosphate esters, glycols, aqueous film forming foams, and foam stabilizers |
| GB0716421D0 (en) * | 2007-08-23 | 2007-10-03 | 3M Innovative Properties Co | Method of preparing fluoropolymers by aqueous emulsion polymerization |
| US9650479B2 (en) | 2007-10-04 | 2017-05-16 | W. L. Gore & Associates, Inc. | Dense articles formed from tetrafluoroethylene core shell copolymers and methods of making the same |
| US8637144B2 (en) | 2007-10-04 | 2014-01-28 | W. L. Gore & Associates, Inc. | Expandable TFE copolymers, method of making, and porous, expended articles thereof |
| US9040646B2 (en) | 2007-10-04 | 2015-05-26 | W. L. Gore & Associates, Inc. | Expandable TFE copolymers, methods of making, and porous, expanded articles thereof |
| ES2389274T3 (es) * | 2008-07-17 | 2012-10-24 | W.L. Gore & Associates Gmbh | Recubrimiento de polímeros que contienen un complejo de un fluoropolieter iónico y un agente contraiónico |
| CN102149674A (zh) | 2008-07-18 | 2011-08-10 | 3M创新有限公司 | 氟化醚化合物及其使用方法 |
| US20100036053A1 (en) * | 2008-08-08 | 2010-02-11 | E.I. Du Pont De Nemours And Company | Aqueous Polymerization Process for the Manufacture of Fluoropolymer Comprising Repeating Units Arising from a Perfluoromonomer and a Monomer Having a Functional Group and a Polymerizable Carbon-Carbon Double Bond |
| WO2010080473A1 (en) | 2008-12-18 | 2010-07-15 | 3M Innovative Properties Company | Method of contacting hydrocarbon-bearing formations with fluorinated ether compositions |
| US8835547B2 (en) * | 2008-12-23 | 2014-09-16 | E I Du Pont De Nemours And Company | Fluoropolymer particles having a nucleus of fluorinated ionomer |
| US8436054B2 (en) * | 2008-12-23 | 2013-05-07 | E I Du Pont De Nemours And Company | Fluorinated ionomer produced by aqueous polymerization using dispersed particulate of fluorinated ionomer produced in situ |
| US8436053B2 (en) * | 2008-12-23 | 2013-05-07 | E.I. Du Pont De Nemours And Company | Fluorinated ionomer produced by aqueous polymerization using dispersed particulate of fluorinated ionomer |
| CN102337677B (zh) * | 2010-07-14 | 2014-03-19 | 杜邦公司 | 表面涂覆过的聚酯纤维基质及其制备方法 |
| JPWO2012020806A1 (ja) * | 2010-08-11 | 2013-10-28 | 旭硝子株式会社 | 撥水撥油剤組成物および物品 |
| EP2927247B1 (en) | 2012-11-30 | 2017-07-19 | Daikin Industries, Ltd. | Polytetrafluoroethylene aqueous dispersion, and polytetrafluoroethylene fine powder |
| EP2918613B1 (en) * | 2012-11-30 | 2020-06-03 | Daikin Industries, Ltd. | Production method for polytetrafluoroethylene aqueous dispersion |
| JP2016520732A (ja) * | 2013-06-04 | 2016-07-14 | ソルベイ スペシャルティ ポリマーズ イタリー エス．ピー．エー． | フルオロポリマー複合体の製造方法 |
| CN103709306A (zh) * | 2013-12-30 | 2014-04-09 | 江苏梅兰化工有限公司 | 一种过氧化物硫化氟橡胶的纳米乳液及其聚合方法 |
| CN103709305B (zh) * | 2013-12-30 | 2016-09-07 | 江苏梅兰化工有限公司 | 一种氟橡胶的制备方法 |
| US11111405B2 (en) * | 2014-09-09 | 2021-09-07 | Honeywell International Inc. | Low VOC and high solid fluoropolymer for coating applications |
| US9644054B2 (en) | 2014-12-19 | 2017-05-09 | W. L. Gore & Associates, Inc. | Dense articles formed from tetrafluoroethylene core shell copolymers and methods of making the same |
| WO2018228871A1 (en) * | 2017-06-14 | 2018-12-20 | Solvay Specialty Polymers Italy S.P.A. | Ferroelectric fluoropolymer |
| CN111836870B (zh) * | 2018-03-08 | 2023-03-24 | Ａｇｃ株式会社 | 拒水拒油剂组合物的制造方法及拒水拒油性物品的制造方法 |
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|---|---|---|---|---|
| US2567011A (en) | 1949-01-10 | 1951-09-04 | Minnesota Mining & Mfg | Fluorocarbon acids and derivatives |
| US2732398A (en) | 1953-01-29 | 1956-01-24 | cafiicfzsojk | |
| US2809990A (en) | 1955-12-29 | 1957-10-15 | Minnesota Mining & Mfg | Fluorocarbon acids and derivatives |
| US3136745A (en) | 1961-06-23 | 1964-06-09 | Du Pont | Elastomeric copolymers of vinylidene fluoride and perfluoroalkyl perfluorovinyl ethers |
| US3132124A (en) | 1961-07-06 | 1964-05-05 | Du Pont | Copolymerization of tetrafluoroethylene and hexafluoropropylene |
| US3450684A (en) | 1963-07-24 | 1969-06-17 | Du Pont | Fluorocarbon polyethers |
| GB1196760A (en) | 1967-11-10 | 1970-07-01 | Roger Boudart | Method for Processing Papaw Latex, and Product Obtained. |
| DE1720799A1 (de) | 1968-03-09 | 1970-05-14 | Hoechst Ag | Verfahren zur Herstellung von polymeren Fluoralkyl-vinyl-aethern |
| US4029867A (en) | 1971-02-22 | 1977-06-14 | The United States Of America As Represented By The Secretary Of Agriculture | Terpolymers of fluoroalkyl ethers and maleic anhydride |
| CA950923A (en) | 1971-03-29 | 1974-07-09 | E. I. Du Pont De Nemours And Company | Polymers of perfluorovinyl ethers |
| US4035565A (en) | 1975-03-27 | 1977-07-12 | E. I. Du Pont De Nemours And Company | Fluoropolymer containing a small amount of bromine-containing olefin units |
| DE2949907A1 (de) | 1979-12-12 | 1981-06-19 | Hoechst Ag, 6230 Frankfurt | Fluorpolymere mit schalenmodifizierten teilchen und verfahren zu deren herstellung |
| US4316836A (en) * | 1980-04-23 | 1982-02-23 | E. I. Du Pont De Nemours And Company | Stabilized fluoroelastomer compositions |
| JPS5718710A (en) | 1980-07-08 | 1982-01-30 | Asahi Glass Co Ltd | Copolymer capable of giving elastomer containing fluorine having improved cold and oil resistance |
| JPS57109810A (en) | 1980-12-26 | 1982-07-08 | Asahi Glass Co Ltd | Copolymer giving fluorine-containing elastomer with cold and alcohol resistance |
| JPS5869213A (ja) | 1981-09-21 | 1983-04-25 | Daikin Ind Ltd | 含フツ素共重合体 |
| DE3575566D1 (de) * | 1984-12-19 | 1990-03-01 | Ausimont Usa | Terpolymer aus chlortrifluorethylen oder tetrafluorethylen, ethylen und perfluorisoalkoxyperfluoralkylethylen. |
| EP0186186B1 (en) | 1984-12-27 | 1991-07-24 | Asahi Glass Company Ltd. | Curable resin composition |
| JPS61201078A (ja) | 1985-02-28 | 1986-09-05 | ダイキン工業株式会社 | 新規な含浸物品 |
| US5110385A (en) | 1985-05-31 | 1992-05-05 | The Dow Chemical Company | Method for forming polymer composite films using a removable substrate |
| JPS6289713A (ja) | 1985-10-12 | 1987-04-24 | Daikin Ind Ltd | 新規フルオロエラストマー |
| IT1189092B (it) | 1986-04-29 | 1988-01-28 | Ausimont Spa | Processo di polimerizzazione in dispersione acquosa di monomeri fluorurati |
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| US4929471A (en) | 1989-04-13 | 1990-05-29 | The Balson-Hercules Group Ltd. | Method of treating polyester fabric |
| JP2729838B2 (ja) | 1989-07-21 | 1998-03-18 | 日本メクトロン株式会社 | パーフルオロ（ビニルエーテル）類の低重合法 |
| DE4124134A1 (de) | 1991-07-20 | 1993-01-21 | Hoechst Ag | Konzentrierte, waessrige dispersionen von tetrafluorethylen-polymeren, verfahren zu deren herstellung und deren verwendung |
| DE4213154C1 (US07829477-20101109-C00007.png) | 1992-04-22 | 1993-06-17 | Hoechst Ag, 6230 Frankfurt, De | |
| IT1264125B1 (it) | 1993-03-30 | 1996-09-16 | Ausimont Spa | Fluoroelastomeri dotati di elevata resistenza ai solventi polari ed alle basi |
| DE4402694A1 (de) | 1993-06-02 | 1995-08-03 | Hoechst Ag | Verfahren zur Rückgewinnung von fluorierten Carbonsäuren |
| CN1062873C (zh) * | 1993-10-12 | 2001-03-07 | 旭化成工业株式会社 | 含官能团的全氟化碳共聚物及其制备方法 |
| IT1269845B (it) * | 1994-05-27 | 1997-04-15 | Ausimont Spa | Composizioni fluoroelastomeriche vulcanizzabili |
| DE69511583T2 (de) | 1995-01-18 | 2000-01-13 | W.L. Gore & Associates, Inc. | Microemulsionspolymerisation-systeme für fluor-enthaltende monomere |
| EP0731081B1 (de) | 1995-03-09 | 1998-04-15 | Dyneon GmbH | Rückgewinnung hochfluorierter Carbonsäuren aus der Gasphase |
| DE19542501A1 (de) * | 1995-11-15 | 1997-05-22 | Bayer Ag | Peroxidisch vernetzbare Fluorkautschuke, ein Verfahren zu deren Herstellung und deren Verwendung |
| JP3671517B2 (ja) * | 1996-04-24 | 2005-07-13 | ユニマテック株式会社 | 含フッ素共重合体エラストマー、その製造法および組成物 |
| JPH10101740A (ja) | 1996-10-01 | 1998-04-21 | Nippon Mektron Ltd | フルオロエラストマーおよびその架橋性組成物 |
| DE19752677A1 (de) * | 1997-11-28 | 1999-06-02 | Basf Ag | Verfahren zur Herstellung von hochmolekularen Polymerisaten aus Maleinsäureanhydrid und Alkylvinylethern |
| DE19824615A1 (de) | 1998-06-02 | 1999-12-09 | Dyneon Gmbh | Verfahren zur Rückgewinnung von fluorierten Alkansäuren aus Abwässern |
| DE19824614A1 (de) | 1998-06-02 | 1999-12-09 | Dyneon Gmbh | Verfahren zur Rückgewinnung von fluorierten Alkansäuren aus Abwässern |
| ITMI981520A1 (it) | 1998-07-02 | 2000-01-02 | Ausimont Spa | Dispersioni di fluoropolimeri |
| CN1215085C (zh) | 1998-10-13 | 2005-08-17 | 大金工业株式会社 | 含氟聚合物的制造方法 |
| CA2362289A1 (en) | 1999-03-02 | 2000-09-08 | E. I. Du Pont De Nemours And Company | Free radical polymerization method for fluorinated copolymers |
| DE19932771A1 (de) | 1999-07-14 | 2001-01-18 | Dyneon Gmbh | Verfahren zur Eluierung fluorierter Emulgatoren |
| WO2001006054A1 (en) | 1999-07-19 | 2001-01-25 | Avantgarb, Llc | Nanoparticle-based permanent treatments for textiles |
| DE19964004A1 (de) | 1999-12-30 | 2001-07-12 | Dyneon Gmbh | Verfahren zur Polymerisation fluorierter Monomerer mit höheren Siedepunkten und geringer Wasserlöslichkeit |
| US6677414B2 (en) | 1999-12-30 | 2004-01-13 | 3M Innovative Properties Company | Aqueous emulsion polymerization process for the manufacturing of fluoropolymers |
| US6737489B2 (en) * | 2001-05-21 | 2004-05-18 | 3M Innovative Properties Company | Polymers containing perfluorovinyl ethers and applications for such polymers |
| US6833418B2 (en) | 2002-04-05 | 2004-12-21 | 3M Innovative Properties Company | Dispersions containing perfluorovinyl ether homopolymers and use thereof |
| US6822059B2 (en) | 2002-04-05 | 2004-11-23 | 3M Innovative Properties Company | Dispersions containing bicomponent fluoropolymer particles and use thereof |
-
2002
- 2002-04-05 US US10/117,714 patent/US6822059B2/en not_active Expired - Fee Related
-
2003
- 2003-02-12 CN CNB03807804XA patent/CN1290882C/zh not_active Expired - Fee Related
- 2003-02-12 DE DE60307251T patent/DE60307251T2/de not_active Expired - Lifetime
- 2003-02-12 MX MXPA04009505A patent/MXPA04009505A/es active IP Right Grant
- 2003-02-12 JP JP2003584134A patent/JP2005522541A/ja not_active Withdrawn
- 2003-02-12 KR KR10-2004-7015775A patent/KR20040106315A/ko not_active Application Discontinuation
- 2003-02-12 ES ES03713416T patent/ES2269995T3/es not_active Expired - Lifetime
- 2003-02-12 BR BR0308568-6A patent/BR0308568A/pt not_active IP Right Cessation
- 2003-02-12 WO PCT/US2003/004070 patent/WO2003087179A1/en active IP Right Grant
- 2003-02-12 EP EP03713416A patent/EP1492827B1/en not_active Expired - Lifetime
- 2003-02-12 AT AT03713416T patent/ATE335020T1/de not_active IP Right Cessation
- 2003-02-12 AU AU2003217372A patent/AU2003217372A1/en not_active Abandoned
-
2004
- 2004-11-01 US US10/978,848 patent/US7300989B2/en not_active Expired - Fee Related
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