JP2004238393A5 - - Google Patents
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- Publication number
- JP2004238393A5 JP2004238393A5 JP2004005608A JP2004005608A JP2004238393A5 JP 2004238393 A5 JP2004238393 A5 JP 2004238393A5 JP 2004005608 A JP2004005608 A JP 2004005608A JP 2004005608 A JP2004005608 A JP 2004005608A JP 2004238393 A5 JP2004238393 A5 JP 2004238393A5
- Authority
- JP
- Japan
- Prior art keywords
- product
- dinitroglycerin
- reacting
- reaction vessel
- nitric acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000047 product Substances 0.000 claims description 63
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 54
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 40
- 238000000034 method Methods 0.000 claims description 36
- VSOJWGJCPFPODA-UHFFFAOYSA-N 1,3-dinitropropane-1,2,3-triol Chemical compound [O-][N+](=O)C(O)C(O)C(O)[N+]([O-])=O VSOJWGJCPFPODA-UHFFFAOYSA-N 0.000 claims description 35
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 29
- 229910017604 nitric acid Inorganic materials 0.000 claims description 29
- ADZAAKGRMMGJKM-UHFFFAOYSA-N oxiran-2-ylmethyl nitrate Chemical compound [O-][N+](=O)OCC1CO1 ADZAAKGRMMGJKM-UHFFFAOYSA-N 0.000 claims description 25
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 claims description 22
- 235000011187 glycerol Nutrition 0.000 claims description 20
- 238000000926 separation method Methods 0.000 claims description 20
- 239000003518 caustics Substances 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- 229910001868 water Inorganic materials 0.000 claims description 12
- 235000010344 sodium nitrate Nutrition 0.000 claims description 11
- 239000004317 sodium nitrate Substances 0.000 claims description 11
- 239000006227 byproduct Substances 0.000 claims description 8
- 239000002699 waste material Substances 0.000 claims description 6
- 239000002904 solvent Substances 0.000 claims description 5
- ASIGVDLTBLZXNC-UHFFFAOYSA-N 1,3-dinitroglycerol Chemical compound [O-][N+](=O)OCC(O)CO[N+]([O-])=O ASIGVDLTBLZXNC-UHFFFAOYSA-N 0.000 claims description 2
- 229910002651 NO3 Inorganic materials 0.000 claims description 2
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims description 2
- 238000007599 discharging Methods 0.000 claims description 2
- 125000003055 glycidyl group Chemical group C(C1CO1)* 0.000 claims description 2
- 230000003472 neutralizing effect Effects 0.000 claims description 2
- 230000000379 polymerizing effect Effects 0.000 claims description 2
- 238000003756 stirring Methods 0.000 claims description 2
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 6
- 239000012267 brine Substances 0.000 description 4
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 4
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10/340,167 US6870061B2 (en) | 2003-01-10 | 2003-01-10 | Continuous process and system for production of glycidyl nitrate from glycerin, nitric acid and caustic and conversion of glycidyl nitrate to poly(glycidyl nitrate) |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2004238393A JP2004238393A (ja) | 2004-08-26 |
| JP2004238393A5 true JP2004238393A5 (enExample) | 2006-03-30 |
Family
ID=31188249
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2004005608A Pending JP2004238393A (ja) | 2003-01-10 | 2004-01-13 | グリセリン、硝酸および苛性アルカリからグリシジルニトレートを製造するための連続法および装置系、並びにグリシジルニトレートのポリ・グリシジルニトレートへの転化 |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US6870061B2 (enExample) |
| JP (1) | JP2004238393A (enExample) |
| FR (1) | FR2851770B1 (enExample) |
| GB (1) | GB2398567B (enExample) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10350672B4 (de) * | 2003-10-30 | 2009-10-29 | Südzucker Aktiengesellschaft | Verfahren zur Reduzierung des Kalkverbrauches bei der Zuckerrübensaft-Reinigung |
| US20070135380A1 (en) * | 2005-08-12 | 2007-06-14 | Radiorx, Inc. | O-nitro compounds, pharmaceutical compositions thereof and uses thereof |
| CN101417966A (zh) * | 2007-10-25 | 2009-04-29 | 北京天擎化工有限责任公司 | 3-异噻唑啉酮衍生物的连续式生产方法 |
| US8471041B2 (en) * | 2010-02-09 | 2013-06-25 | Alliant Techsystems Inc. | Methods of synthesizing and isolating N-(bromoacetyl)-3,3-dinitroazetidine and a composition including the same |
| WO2014047319A1 (en) * | 2012-09-20 | 2014-03-27 | M-I L.L.C. | Oil based flocculation mixing and dispersion system |
| KR20190040931A (ko) | 2016-01-11 | 2019-04-19 | 에피센트알엑스, 인코포레이티드 | 2-브로모-1-(3,3-디니트로아제티딘-1-일)에타논의 정맥내 투여를 위한 조성물 및 방법 |
| US11510901B2 (en) | 2018-01-08 | 2022-11-29 | Epicentrx, Inc. | Methods and compositions utilizing RRx-001 combination therapy for radioprotection |
| US10562873B1 (en) | 2018-12-07 | 2020-02-18 | Northrop Grumman Innovation Systems, Inc. | Methods of producing glycidyl nitrate |
| US20230183198A1 (en) * | 2021-12-10 | 2023-06-15 | Northrop Grumman Systems Corporation | Methods of producing glycidyl nitrate and related systems |
| CN119746792B (zh) * | 2024-12-17 | 2025-10-03 | 中国石油大学(华东) | 一种基于氯闭环循环利用的环氧烷烃氯醇法清洁生产装置 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB8817545D0 (en) * | 1988-07-22 | 1988-08-24 | Secr Defence | Preparation of epoxy nitrates |
| DE68914992T2 (de) * | 1988-07-22 | 1994-08-11 | Secr Defence Brit | Herstellung von durch nitratoalkyl substituierten cyclischen äthern. |
| US5120827A (en) * | 1990-08-02 | 1992-06-09 | Thiokol Corporation | Process for producing improved poly(glycidyl nitrate) |
| EP1240234B1 (en) * | 1999-10-19 | 2004-12-29 | Alliant Techsystems Inc. | Polymerization of poly(glycidyl nitrate) from high purity glycidyl nitrate synthesized from glycerol |
-
2003
- 2003-01-10 US US10/340,167 patent/US6870061B2/en not_active Expired - Lifetime
- 2003-12-24 GB GB0330032A patent/GB2398567B/en not_active Expired - Fee Related
-
2004
- 2004-01-08 FR FR0400105A patent/FR2851770B1/fr not_active Expired - Fee Related
- 2004-01-13 JP JP2004005608A patent/JP2004238393A/ja active Pending
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