GB2398567B - Continuous process and system for production of glycidyl nitrate from glycerin, nitric acid and caustic and conversion of glycidyl nitrate to poly(glycidyl ni - Google Patents

Continuous process and system for production of glycidyl nitrate from glycerin, nitric acid and caustic and conversion of glycidyl nitrate to poly(glycidyl ni

Info

Publication number
GB2398567B
GB2398567B GB0330032A GB0330032A GB2398567B GB 2398567 B GB2398567 B GB 2398567B GB 0330032 A GB0330032 A GB 0330032A GB 0330032 A GB0330032 A GB 0330032A GB 2398567 B GB2398567 B GB 2398567B
Authority
GB
United Kingdom
Prior art keywords
glycidyl
nitrate
caustic
glycerin
poly
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
GB0330032A
Other languages
English (en)
Other versions
GB2398567A (en
GB0330032D0 (en
Inventor
Thomas K Highsmith
Harold E Johnston
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Northrop Grumman Innovation Systems LLC
Original Assignee
Alliant Techsystems Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Alliant Techsystems Inc filed Critical Alliant Techsystems Inc
Publication of GB0330032D0 publication Critical patent/GB0330032D0/en
Publication of GB2398567A publication Critical patent/GB2398567A/en
Application granted granted Critical
Publication of GB2398567B publication Critical patent/GB2398567B/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02—Compounds containing oxirane rings
    • C07D303/08—Compounds containing oxirane rings with hydrocarbon radicals, substituted by halogen atoms, nitro radicals or nitroso radicals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02—Compounds containing oxirane rings
    • C07D303/12—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
    • C07D303/16—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by esterified hydroxyl radicals

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Epoxy Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polyethers (AREA)
GB0330032A 2003-01-10 2003-12-24 Continuous process and system for production of glycidyl nitrate from glycerin, nitric acid and caustic and conversion of glycidyl nitrate to poly(glycidyl ni Expired - Fee Related GB2398567B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US10/340,167 US6870061B2 (en) 2003-01-10 2003-01-10 Continuous process and system for production of glycidyl nitrate from glycerin, nitric acid and caustic and conversion of glycidyl nitrate to poly(glycidyl nitrate)

Publications (3)

Publication Number Publication Date
GB0330032D0 GB0330032D0 (en) 2004-01-28
GB2398567A GB2398567A (en) 2004-08-25
GB2398567B true GB2398567B (en) 2007-08-01

Family

ID=31188249

Family Applications (1)

Application Number Title Priority Date Filing Date
GB0330032A Expired - Fee Related GB2398567B (en) 2003-01-10 2003-12-24 Continuous process and system for production of glycidyl nitrate from glycerin, nitric acid and caustic and conversion of glycidyl nitrate to poly(glycidyl ni

Country Status (4)

Country Link
US (1) US6870061B2 (enExample)
JP (1) JP2004238393A (enExample)
FR (1) FR2851770B1 (enExample)
GB (1) GB2398567B (enExample)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10350672B4 (de) * 2003-10-30 2009-10-29 Südzucker Aktiengesellschaft Verfahren zur Reduzierung des Kalkverbrauches bei der Zuckerrübensaft-Reinigung
US20070135380A1 (en) * 2005-08-12 2007-06-14 Radiorx, Inc. O-nitro compounds, pharmaceutical compositions thereof and uses thereof
CN101417966A (zh) * 2007-10-25 2009-04-29 北京天擎化工有限责任公司 3-异噻唑啉酮衍生物的连续式生产方法
US8471041B2 (en) * 2010-02-09 2013-06-25 Alliant Techsystems Inc. Methods of synthesizing and isolating N-(bromoacetyl)-3,3-dinitroazetidine and a composition including the same
WO2014047319A1 (en) * 2012-09-20 2014-03-27 M-I L.L.C. Oil based flocculation mixing and dispersion system
KR20190040931A (ko) 2016-01-11 2019-04-19 에피센트알엑스, 인코포레이티드 2-브로모-1-(3,3-디니트로아제티딘-1-일)에타논의 정맥내 투여를 위한 조성물 및 방법
US11510901B2 (en) 2018-01-08 2022-11-29 Epicentrx, Inc. Methods and compositions utilizing RRx-001 combination therapy for radioprotection
US10562873B1 (en) 2018-12-07 2020-02-18 Northrop Grumman Innovation Systems, Inc. Methods of producing glycidyl nitrate
US20230183198A1 (en) * 2021-12-10 2023-06-15 Northrop Grumman Systems Corporation Methods of producing glycidyl nitrate and related systems
CN119746792B (zh) * 2024-12-17 2025-10-03 中国石油大学(华东) 一种基于氯闭环循环利用的环氧烷烃氯醇法清洁生产装置

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001029111A1 (en) * 1999-10-19 2001-04-26 Alliant Techsystems Inc. Polymerization of poly(glycidyl nitrate) from high purity glycidyl nitrate synthesized from glycerol

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB8817545D0 (en) * 1988-07-22 1988-08-24 Secr Defence Preparation of epoxy nitrates
DE68914992T2 (de) * 1988-07-22 1994-08-11 Secr Defence Brit Herstellung von durch nitratoalkyl substituierten cyclischen äthern.
US5120827A (en) * 1990-08-02 1992-06-09 Thiokol Corporation Process for producing improved poly(glycidyl nitrate)

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001029111A1 (en) * 1999-10-19 2001-04-26 Alliant Techsystems Inc. Polymerization of poly(glycidyl nitrate) from high purity glycidyl nitrate synthesized from glycerol
EP1240234B1 (en) * 1999-10-19 2004-12-29 Alliant Techsystems Inc. Polymerization of poly(glycidyl nitrate) from high purity glycidyl nitrate synthesized from glycerol

Also Published As

Publication number Publication date
US6870061B2 (en) 2005-03-22
GB2398567A (en) 2004-08-25
US20040138481A1 (en) 2004-07-15
GB0330032D0 (en) 2004-01-28
JP2004238393A (ja) 2004-08-26
FR2851770A1 (fr) 2004-09-03
FR2851770B1 (fr) 2007-08-03

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Legal Events

Date Code Title Description
PCNP Patent ceased through non-payment of renewal fee

Effective date: 20111224