IL162002A0 - A process for preparing 2-oxo imidazolidine derivatives - Google Patents
A process for preparing 2-oxo imidazolidine derivativesInfo
- Publication number
- IL162002A0 IL162002A0 IL16200202A IL16200202A IL162002A0 IL 162002 A0 IL162002 A0 IL 162002A0 IL 16200202 A IL16200202 A IL 16200202A IL 16200202 A IL16200202 A IL 16200202A IL 162002 A0 IL162002 A0 IL 162002A0
- Authority
- IL
- Israel
- Prior art keywords
- substituent
- magnesium
- zinc
- atom
- formula
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- YAMHXTCMCPHKLN-UHFFFAOYSA-N imidazolidin-2-one Chemical class O=C1NCCN1 YAMHXTCMCPHKLN-UHFFFAOYSA-N 0.000 title 1
- 125000001424 substituent group Chemical group 0.000 abstract 5
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical group [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 abstract 3
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical group [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 abstract 3
- 239000011777 magnesium Chemical group 0.000 abstract 3
- 229910052749 magnesium Chemical group 0.000 abstract 3
- 229910052725 zinc Inorganic materials 0.000 abstract 3
- 239000011701 zinc Substances 0.000 abstract 3
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 abstract 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 abstract 2
- CPELXLSAUQHCOX-UHFFFAOYSA-N Hydrogen bromide Chemical compound Br CPELXLSAUQHCOX-UHFFFAOYSA-N 0.000 abstract 2
- 125000004429 atom Chemical group 0.000 abstract 2
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 abstract 2
- 229910052794 bromium Inorganic materials 0.000 abstract 2
- 239000000460 chlorine Substances 0.000 abstract 2
- 229910052801 chlorine Inorganic materials 0.000 abstract 2
- 150000001875 compounds Chemical class 0.000 abstract 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 1
- 125000003342 alkenyl group Chemical group 0.000 abstract 1
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- 125000003118 aryl group Chemical group 0.000 abstract 1
- 125000005842 heteroatom Chemical group 0.000 abstract 1
- 125000000623 heterocyclic group Chemical group 0.000 abstract 1
- 229910000042 hydrogen bromide Inorganic materials 0.000 abstract 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 abstract 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 abstract 1
- PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical compound II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 abstract 1
- 229910052751 metal Inorganic materials 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 229910052757 nitrogen Inorganic materials 0.000 abstract 1
- 125000004433 nitrogen atom Chemical group N* 0.000 abstract 1
- 125000004430 oxygen atom Chemical group O* 0.000 abstract 1
- 229910052717 sulfur Inorganic materials 0.000 abstract 1
- 125000004434 sulfur atom Chemical group 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F3/00—Compounds containing elements of Groups 2 or 12 of the Periodic Table
- C07F3/06—Zinc compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
- C07D233/04—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member
- C07D233/28—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D233/30—Oxygen or sulfur atoms
- C07D233/32—One oxygen atom
- C07D233/34—Ethylene-urea
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D495/00—Heterocyclic compounds containing in the condensed system at least one hetero ring having sulfur atoms as the only ring hetero atoms
- C07D495/02—Heterocyclic compounds containing in the condensed system at least one hetero ring having sulfur atoms as the only ring hetero atoms in which the condensed system contains two hetero rings
- C07D495/04—Ortho-condensed systems
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F3/00—Compounds containing elements of Groups 2 or 12 of the Periodic Table
- C07F3/02—Magnesium compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2001369479 | 2001-12-04 | ||
| JP2002209121 | 2002-07-18 | ||
| PCT/JP2002/012694 WO2003048131A1 (en) | 2001-12-04 | 2002-12-04 | Intermediate for biotin and process for producing the same |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| IL162002A0 true IL162002A0 (en) | 2005-11-20 |
Family
ID=26624858
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IL16200202A IL162002A0 (en) | 2001-12-04 | 2002-12-04 | A process for preparing 2-oxo imidazolidine derivatives |
Country Status (12)
| Country | Link |
|---|---|
| US (2) | US7335778B2 (de) |
| EP (2) | EP2098528A3 (de) |
| JP (1) | JP4046693B2 (de) |
| KR (2) | KR100589550B1 (de) |
| CN (1) | CN1273453C (de) |
| AT (1) | ATE443050T1 (de) |
| AU (1) | AU2002349398A1 (de) |
| DE (1) | DE60233754D1 (de) |
| ES (1) | ES2330624T3 (de) |
| IL (1) | IL162002A0 (de) |
| TW (1) | TW200300676A (de) |
| WO (1) | WO2003048131A1 (de) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100560598C (zh) * | 2005-07-26 | 2009-11-18 | 上海奥锐特国际贸易有限公司 | 氟替卡松丙酸酯的合成方法 |
| CN101328148B (zh) * | 2007-06-20 | 2012-05-23 | 浙江医药股份有限公司新昌制药厂 | 酯交换法合成1,3-二苄基-5-羟甲基-4-烷氧羰基-咪唑啉2-酮的方法 |
| CN101429204B (zh) * | 2007-11-08 | 2010-12-29 | 浙江医药股份有限公司新昌制药厂 | (3aS,4S,6aR)-4-(5'-氧代己基)-四氢噻酚-[3,6-并]咪唑啉-2-酮及其合成方法 |
| CN103724358B (zh) * | 2014-01-20 | 2015-10-28 | 新发药业有限公司 | （3aS,6aR）-1,3-二苄基四氢-4H-噻吩并[3,4-d]咪唑-2,4-（1H）-二酮的制备方法 |
| CN103936759B (zh) * | 2014-03-11 | 2016-01-13 | 新发药业有限公司 | （3aS,6aR）-1,3-二苄基-四氢-4H-噻吩并[3,4-d]咪唑-2,4-（1H）-二酮的简便制备方法 |
| CN103880859B (zh) * | 2014-03-11 | 2015-12-09 | 新发药业有限公司 | （3aS,6aR）-1,3-二苄基四氢-4H-噻吩并[3,4-d]咪唑-2,4-（1H）-二酮的制备方法 |
| CN104530076B (zh) * | 2014-12-17 | 2016-08-17 | 新发药业有限公司 | （3aS,6aR）-1,3-二苄基四氢-4H-噻吩并[3,4-d]咪唑-2,4-（1H）-二酮的合成方法 |
| CN104592146A (zh) * | 2015-01-19 | 2015-05-06 | 烟台腾辉化工有限公司 | 一种l-2-氧代噻唑烷-4-羧酸的制备工艺 |
| WO2021224295A1 (en) * | 2020-05-07 | 2021-11-11 | Dsm Ip Assets B.V. | A process for producing d-biotin intermediates |
| CN113200996B (zh) * | 2021-04-08 | 2022-10-11 | 复旦大学 | 一种戊酸酯的连续流合成方法 |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE759512A (fr) | 1969-11-29 | 1971-05-27 | Hoffmann La Roche | Lactone |
| BE759513A (fr) | 1969-11-29 | 1971-05-27 | Hoffmann La Roche | Thiolactone |
| FR2105655A5 (de) * | 1970-09-16 | 1972-04-28 | Rhone Poulenc Sa | |
| JPS4932551A (de) | 1972-07-25 | 1974-03-25 | ||
| JPS5327279A (en) | 1976-08-25 | 1978-03-14 | Yutaka Terashita | Electric source device for electronic flash |
| JPS58190395A (ja) | 1982-04-28 | 1983-11-07 | Sumitomo Chem Co Ltd | 光学活性なシス−イミダゾリジンジカルボン酸誘導体の製造法 |
| JPS58192886A (ja) | 1982-04-30 | 1983-11-10 | Sumitomo Chem Co Ltd | 光学活性なラクトンの製造方法 |
| EP0242686B1 (de) | 1986-04-19 | 1992-01-29 | MERCK PATENT GmbH | Verfahren zur Herstellung von D-(+)-Biotin |
| JPH0772156B2 (ja) * | 1986-07-11 | 1995-08-02 | 東ソー株式会社 | 含フツ素α，β−不飽和カルボン酸の製法 |
| JPH0759222B2 (ja) | 1989-08-03 | 1995-06-28 | 三菱電機ホーム機器株式会社 | 炊飯器の制御回路 |
| JPH0672044B2 (ja) | 1991-08-02 | 1994-09-14 | 旭化成工業株式会社 | 高純度アルミナ焼結体の製造方法 |
| IT1289910B1 (it) * | 1997-01-17 | 1998-10-19 | Zambon Spa | Processo per la preparazione di eteroaril-zinco alogenuri |
| JP4406948B2 (ja) | 1998-12-28 | 2010-02-03 | 田辺三菱製薬株式会社 | ビオチン中間体の製法 |
| JP2001002679A (ja) | 1999-06-21 | 2001-01-09 | Tanabe Seiyaku Co Ltd | テトラヒドロチエノイミダゾール誘導体及びその製法 |
| US6291681B1 (en) | 2000-02-25 | 2001-09-18 | Roche Vitamins Inc. | Process for preparing biotin |
| DE10024776C1 (de) * | 2000-05-19 | 2001-09-06 | Goldschmidt Ag Th | Verwendung von Metallhydrid-behandeltem Zink in der metallorganischen Synthese |
| FR2826963B1 (fr) * | 2001-07-04 | 2006-01-27 | Rhodia Chimie Sa | Preparation d'organozinciques aromatiques et composition pour ce faire |
-
2002
- 2002-12-03 TW TW091135009A patent/TW200300676A/zh not_active IP Right Cessation
- 2002-12-04 AU AU2002349398A patent/AU2002349398A1/en not_active Abandoned
- 2002-12-04 US US10/496,660 patent/US7335778B2/en not_active Expired - Fee Related
- 2002-12-04 WO PCT/JP2002/012694 patent/WO2003048131A1/ja not_active Ceased
- 2002-12-04 EP EP09159038A patent/EP2098528A3/de not_active Withdrawn
- 2002-12-04 AT AT02783761T patent/ATE443050T1/de active
- 2002-12-04 EP EP02783761A patent/EP1462444B1/de not_active Expired - Lifetime
- 2002-12-04 KR KR1020067005582A patent/KR100589550B1/ko not_active Expired - Fee Related
- 2002-12-04 CN CNB028199111A patent/CN1273453C/zh not_active Expired - Fee Related
- 2002-12-04 DE DE60233754T patent/DE60233754D1/de not_active Expired - Lifetime
- 2002-12-04 JP JP2003549323A patent/JP4046693B2/ja not_active Expired - Fee Related
- 2002-12-04 IL IL16200202A patent/IL162002A0/xx not_active IP Right Cessation
- 2002-12-04 KR KR1020047008563A patent/KR100592016B1/ko not_active Expired - Fee Related
- 2002-12-04 ES ES02783761T patent/ES2330624T3/es not_active Expired - Lifetime
-
2008
- 2008-01-07 US US12/007,118 patent/US7799929B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN1273453C (zh) | 2006-09-06 |
| TWI310311B (de) | 2009-06-01 |
| AU2002349398A1 (en) | 2003-06-17 |
| CN1564813A (zh) | 2005-01-12 |
| KR20060029197A (ko) | 2006-04-04 |
| WO2003048131A1 (en) | 2003-06-12 |
| EP2098528A2 (de) | 2009-09-09 |
| US7799929B2 (en) | 2010-09-21 |
| EP1462444B1 (de) | 2009-09-16 |
| EP2098528A3 (de) | 2011-03-02 |
| US20050038260A1 (en) | 2005-02-17 |
| ES2330624T3 (es) | 2009-12-14 |
| KR100592016B1 (ko) | 2006-06-22 |
| US7335778B2 (en) | 2008-02-26 |
| KR100589550B1 (ko) | 2006-06-14 |
| US20080119655A1 (en) | 2008-05-22 |
| JPWO2003048131A1 (ja) | 2005-04-14 |
| KR20050044683A (ko) | 2005-05-12 |
| ATE443050T1 (de) | 2009-10-15 |
| JP4046693B2 (ja) | 2008-02-13 |
| TW200300676A (en) | 2003-06-16 |
| EP1462444A4 (de) | 2006-10-11 |
| EP1462444A1 (de) | 2004-09-29 |
| DE60233754D1 (de) | 2009-10-29 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MM9K | Patent not in force due to non-payment of renewal fees |