IL104056A - Process for the preparation of L-phosphinothricin and its derivatives - Google Patents
Process for the preparation of L-phosphinothricin and its derivativesInfo
- Publication number
- IL104056A IL104056A IL10405692A IL10405692A IL104056A IL 104056 A IL104056 A IL 104056A IL 10405692 A IL10405692 A IL 10405692A IL 10405692 A IL10405692 A IL 10405692A IL 104056 A IL104056 A IL 104056A
- Authority
- IL
- Israel
- Prior art keywords
- denotes
- subst
- alkoxy
- alkyl
- formula
- Prior art date
Links
- IAJOBQBIJHVGMQ-BYPYZUCNSA-N glufosinate-P Chemical compound CP(O)(=O)CC[C@H](N)C(O)=O IAJOBQBIJHVGMQ-BYPYZUCNSA-N 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 2
- 125000004191 (C1-C6) alkoxy group Chemical group 0.000 abstract 3
- 150000001875 compounds Chemical class 0.000 abstract 3
- 125000004169 (C1-C6) alkyl group Chemical group 0.000 abstract 2
- 125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 abstract 2
- 150000003839 salts Chemical class 0.000 abstract 2
- 125000004178 (C1-C4) alkyl group Chemical group 0.000 abstract 1
- 125000004765 (C1-C4) haloalkyl group Chemical group 0.000 abstract 1
- 125000004739 (C1-C6) alkylsulfonyl group Chemical group 0.000 abstract 1
- 125000005913 (C3-C6) cycloalkyl group Chemical group 0.000 abstract 1
- RQVLGLPAZTUBKX-VKHMYHEASA-N L-vinylglycine Chemical class C=C[C@H](N)C(O)=O RQVLGLPAZTUBKX-VKHMYHEASA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 150000007513 acids Chemical class 0.000 abstract 1
- 238000007098 aminolysis reaction Methods 0.000 abstract 1
- 125000001584 benzyloxycarbonyl group Chemical group C(=O)(OCC1=CC=CC=C1)* 0.000 abstract 1
- 230000003197 catalytic effect Effects 0.000 abstract 1
- 229940125890 compound Ia Drugs 0.000 abstract 1
- 125000002485 formyl group Chemical group [H]C(*)=O 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 abstract 1
- 230000007062 hydrolysis Effects 0.000 abstract 1
- 238000006460 hydrolysis reaction Methods 0.000 abstract 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 abstract 1
- PMVVRSKJCGEFIY-UHFFFAOYSA-N methylphosphonous acid Chemical compound CP(O)O PMVVRSKJCGEFIY-UHFFFAOYSA-N 0.000 abstract 1
- UYWQUFXKFGHYNT-UHFFFAOYSA-N phenylmethyl ester of formic acid Natural products O=COCC1=CC=CC=C1 UYWQUFXKFGHYNT-UHFFFAOYSA-N 0.000 abstract 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 abstract 1
- 150000003254 radicals Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/30—Phosphinic acids [R2P(=O)(OH)]; Thiophosphinic acids ; [R2P(=X1)(X2H) (X1, X2 are each independently O, S or Se)]
- C07F9/301—Acyclic saturated acids which can have further substituents on alkyl
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/30—Phosphinic acids [R2P(=O)(OH)]; Thiophosphinic acids ; [R2P(=X1)(X2H) (X1, X2 are each independently O, S or Se)]
- C07F9/32—Esters thereof
- C07F9/3205—Esters thereof the acid moiety containing a substituent or a structure which is considered as characteristic
- C07F9/3211—Esters of acyclic saturated acids which can have further substituents on alkyl
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Steroid Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Saccharide Compounds (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE4141042 | 1991-12-13 |
Publications (2)
Publication Number | Publication Date |
---|---|
IL104056A0 IL104056A0 (en) | 1993-05-13 |
IL104056A true IL104056A (en) | 1997-02-18 |
Family
ID=6446916
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
IL10405692A IL104056A (en) | 1991-12-13 | 1992-12-10 | Process for the preparation of L-phosphinothricin and its derivatives |
Country Status (10)
Country | Link |
---|---|
US (1) | US5420329A (ja) |
EP (1) | EP0546566B1 (ja) |
JP (1) | JP3294647B2 (ja) |
AT (1) | ATE142219T1 (ja) |
AU (1) | AU662779B2 (ja) |
CA (1) | CA2085145A1 (ja) |
DE (1) | DE59207049D1 (ja) |
HU (2) | HU213525B (ja) |
IL (1) | IL104056A (ja) |
MX (1) | MX9207180A (ja) |
Families Citing this family (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE4407197A1 (de) * | 1994-03-04 | 1995-09-07 | Hoechst Schering Agrevo Gmbh | Verfahren zur Herstellung von /L/-Homoalanin-4-yl-(methyl)phosphinsäure und deren Salze durch Racematspaltung |
JP2003502866A (ja) * | 1999-06-17 | 2003-01-21 | インフィネオン テクノロジーズ アクチエンゲゼルシャフト | 軟質ボンディング部を有する電子部品およびこのような部品を製造するための方法 |
DE10016132A1 (de) * | 2000-03-31 | 2001-10-18 | Infineon Technologies Ag | Elektronisches Bauelement mit flexiblen Kontaktierungsstellen und Verfahren zu dessen Herstellung |
DE10116069C2 (de) * | 2001-04-02 | 2003-02-20 | Infineon Technologies Ag | Elektronisches Bauteil mit einem Halbleiterchip und Verfahren zu seiner Herstellung |
DE102008056339A1 (de) * | 2008-11-07 | 2010-05-12 | Clariant International Limited | Verfahren zur Herstellung von mono-aminofunktionalisierten Dialkylphosphinsäuren, -estern und -salzen und ihre Verwendung |
US9850263B2 (en) * | 2014-05-13 | 2017-12-26 | Bayer Cropscience Aktiengesellschaft | Process for preparing phosphorus containing cyanohydrins |
TW201840578A (zh) | 2017-02-22 | 2018-11-16 | 以色列商亞當阿甘公司 | 製備甲基膦酸丁基酯的方法 |
EP3392237B1 (de) | 2017-04-21 | 2019-10-02 | Evonik Degussa GmbH | Verfahren zur herstellung von acroleincyanhydrinen |
JP2020527567A (ja) | 2017-07-18 | 2020-09-10 | アグリメティス,エルエルシー | L−グルホシネートの精製方法 |
CN111793085B (zh) * | 2019-04-04 | 2023-02-24 | 利尔化学股份有限公司 | 一种制备l-草铵膦的方法 |
BR112021018995A2 (pt) | 2019-04-16 | 2021-11-30 | Basf Se | Método para preparar monoidrato de l-glufosinato de amônio cristalino e enzimas d-aminoácido oxidase mutantes |
BR112022009782A2 (pt) | 2019-11-20 | 2022-08-09 | Eureka! Agresearch Pty Ltd | Composição herbicida de glufosinato |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2717440C2 (de) * | 1976-05-17 | 1984-04-05 | Hoechst Ag, 6230 Frankfurt | Unkrautbekämpfung mit [(3-Amino-3-carboxy)-propyl-1]-methylphosphinsäure-Derivaten |
GB2011416B (en) * | 1977-12-28 | 1982-10-20 | Meiji Seika Kaisha | Herbicidal compositions |
WO1979001114A1 (en) * | 1978-05-25 | 1979-12-13 | Meiji Seika Kaisha | Dialkyl 4-methylphosphinobutyrates and process for producing same |
DE2849003A1 (de) * | 1978-11-11 | 1980-08-21 | Hoechst Ag | Phosphorhaltige cyanhydrinderivate und verfahren zu ihrer herstellung |
JPS59219297A (ja) * | 1983-05-27 | 1984-12-10 | Meiji Seika Kaisha Ltd | 光学活性な〔(3−アミノ−3−カルボキシ)プロピル−1〕−ホスフイン酸誘導体の製造法 |
DE3525267A1 (de) * | 1984-09-08 | 1986-03-20 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von weitgehend reinen enantiomeren von (3-amino-3-carboxy-propyl)-alkyl-phosphinsaeurederivaten, neue pyrazinderivate und ihre verwendung als herbizide und bioregulatoren |
DE3542645A1 (de) * | 1985-12-03 | 1987-06-04 | Hoechst Ag | Verfahren zur herstellung von l-homoalanin-4-yl(methyl)-phosphinsaeure sowie ihrer alkylester |
DE3609818A1 (de) * | 1986-03-22 | 1987-09-24 | Hoechst Ag | Verfahren zur herstellung von l-phosphinothricin(derivaten) sowie ihrer alkylester |
NL8801370A (nl) * | 1988-05-27 | 1989-12-18 | Leer Koninklijke Emballage | Vat uit thermoplastisch materiaal. |
DE3817956A1 (de) * | 1988-05-27 | 1989-12-07 | Hoechst Ag | Verfahren zur herstellung phosphorhaltiger l-aminosaeuren sowie ihrer ester und n-derivate |
-
1992
- 1992-12-10 IL IL10405692A patent/IL104056A/xx not_active IP Right Cessation
- 1992-12-10 JP JP33072292A patent/JP3294647B2/ja not_active Expired - Fee Related
- 1992-12-11 DE DE59207049T patent/DE59207049D1/de not_active Expired - Fee Related
- 1992-12-11 HU HU9203933A patent/HU213525B/hu not_active IP Right Cessation
- 1992-12-11 MX MX9207180A patent/MX9207180A/es unknown
- 1992-12-11 HU HU9203933A patent/HU9203933D0/hu unknown
- 1992-12-11 AT AT92121154T patent/ATE142219T1/de not_active IP Right Cessation
- 1992-12-11 AU AU30172/92A patent/AU662779B2/en not_active Ceased
- 1992-12-11 EP EP92121154A patent/EP0546566B1/de not_active Expired - Lifetime
- 1992-12-11 CA CA002085145A patent/CA2085145A1/en not_active Abandoned
-
1994
- 1994-07-25 US US08/279,709 patent/US5420329A/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
CA2085145A1 (en) | 1993-06-14 |
IL104056A0 (en) | 1993-05-13 |
EP0546566A1 (de) | 1993-06-16 |
AU3017292A (en) | 1993-06-17 |
JPH05262781A (ja) | 1993-10-12 |
HU9203933D0 (en) | 1993-03-29 |
AU662779B2 (en) | 1995-09-14 |
DE59207049D1 (de) | 1996-10-10 |
MX9207180A (es) | 1993-06-01 |
HU213525B (en) | 1997-07-28 |
HUT64078A (en) | 1993-11-29 |
JP3294647B2 (ja) | 2002-06-24 |
US5420329A (en) | 1995-05-30 |
EP0546566B1 (de) | 1996-09-04 |
ATE142219T1 (de) | 1996-09-15 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FF | Patent granted | ||
KB | Patent renewed | ||
KB | Patent renewed | ||
KB | Patent renewed | ||
MM9K | Patent not in force due to non-payment of renewal fees |