IE53413B1 - Process for the preparation of magnesium nitrate hexahydrate - Google Patents
Process for the preparation of magnesium nitrate hexahydrateInfo
- Publication number
- IE53413B1 IE53413B1 IE2257/82A IE225782A IE53413B1 IE 53413 B1 IE53413 B1 IE 53413B1 IE 2257/82 A IE2257/82 A IE 2257/82A IE 225782 A IE225782 A IE 225782A IE 53413 B1 IE53413 B1 IE 53413B1
- Authority
- IE
- Ireland
- Prior art keywords
- nitrate hexahydrate
- magnesium oxide
- magnesium nitrate
- nitric acid
- added
- Prior art date
Links
- MFUVDXOKPBAHMC-UHFFFAOYSA-N magnesium;dinitrate;hexahydrate Chemical compound O.O.O.O.O.O.[Mg+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O MFUVDXOKPBAHMC-UHFFFAOYSA-N 0.000 title claims abstract description 58
- 238000000034 method Methods 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims description 7
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims abstract description 38
- 239000000395 magnesium oxide Substances 0.000 claims abstract description 35
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 claims abstract description 32
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims abstract description 26
- 229910017604 nitric acid Inorganic materials 0.000 claims abstract description 26
- 239000000047 product Substances 0.000 claims abstract description 19
- 239000007788 liquid Substances 0.000 claims abstract description 18
- 238000006243 chemical reaction Methods 0.000 claims abstract description 12
- 238000003756 stirring Methods 0.000 claims abstract description 9
- 239000000706 filtrate Substances 0.000 claims abstract description 7
- 239000011541 reaction mixture Substances 0.000 claims abstract description 6
- 239000000203 mixture Substances 0.000 claims description 22
- 239000000725 suspension Substances 0.000 claims description 13
- 229910001868 water Inorganic materials 0.000 claims description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- 239000002253 acid Substances 0.000 claims description 8
- 239000002245 particle Substances 0.000 claims description 4
- 230000015572 biosynthetic process Effects 0.000 claims description 2
- 239000000376 reactant Substances 0.000 claims description 2
- 235000012245 magnesium oxide Nutrition 0.000 abstract description 27
- PAWQVTBBRAZDMG-UHFFFAOYSA-N 2-(3-bromo-2-fluorophenyl)acetic acid Chemical compound OC(=O)CC1=CC=CC(Br)=C1F PAWQVTBBRAZDMG-UHFFFAOYSA-N 0.000 abstract description 8
- 238000001914 filtration Methods 0.000 abstract description 5
- 230000006641 stabilisation Effects 0.000 abstract description 4
- 238000011105 stabilization Methods 0.000 abstract description 4
- 238000007599 discharging Methods 0.000 abstract description 2
- 229960000869 magnesium oxide Drugs 0.000 abstract 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 6
- YIXJRHPUWRPCBB-UHFFFAOYSA-N magnesium nitrate Chemical compound [Mg+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O YIXJRHPUWRPCBB-UHFFFAOYSA-N 0.000 description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- 150000004677 hydrates Chemical class 0.000 description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 238000002425 crystallisation Methods 0.000 description 3
- 230000008025 crystallization Effects 0.000 description 3
- 238000001704 evaporation Methods 0.000 description 3
- 230000008020 evaporation Effects 0.000 description 3
- 239000008187 granular material Substances 0.000 description 3
- 239000012535 impurity Substances 0.000 description 3
- 239000011777 magnesium Substances 0.000 description 3
- 229910002651 NO3 Inorganic materials 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 239000003337 fertilizer Substances 0.000 description 2
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 2
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 2
- 150000001447 alkali salts Chemical class 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 229910000514 dolomite Inorganic materials 0.000 description 1
- 239000010459 dolomite Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000001095 magnesium carbonate Substances 0.000 description 1
- 235000014380 magnesium carbonate Nutrition 0.000 description 1
- ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 description 1
- 229910000021 magnesium carbonate Inorganic materials 0.000 description 1
- 150000002681 magnesium compounds Chemical class 0.000 description 1
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 description 1
- 239000000347 magnesium hydroxide Substances 0.000 description 1
- 235000012254 magnesium hydroxide Nutrition 0.000 description 1
- 229910001862 magnesium hydroxide Inorganic materials 0.000 description 1
- YISKQXFNIWWETM-UHFFFAOYSA-N magnesium;dinitrate;hydrate Chemical compound O.[Mg+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O YISKQXFNIWWETM-UHFFFAOYSA-N 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- OQUOOEBLAKQCOP-UHFFFAOYSA-N nitric acid;hexahydrate Chemical compound O.O.O.O.O.O.O[N+]([O-])=O OQUOOEBLAKQCOP-UHFFFAOYSA-N 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000013535 sea water Substances 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
- C01C1/00—Ammonia; Compounds thereof
- C01C1/18—Nitrates of ammonium
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
- C01C1/00—Ammonia; Compounds thereof
- C01C1/18—Nitrates of ammonium
- C01C1/185—Preparation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F5/00—Compounds of magnesium
- C01F5/38—Magnesium nitrates
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C1/00—Ammonium nitrate fertilisers
- C05C1/02—Granulation; Pelletisation; Stabilisation; Colouring
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
- Detergent Compositions (AREA)
- Lubricants (AREA)
- Separation Of Suspended Particles By Flocculating Agents (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL8104284A NL8104284A (nl) | 1981-09-17 | 1981-09-17 | Werkwijze voor het bereiden van magnesiumnitraathexahydraat, alsmede voor het thermisch stabiliseren van ammoniumnitraat onder toepassing van een zo verkregen magnesiumnitraathexahydraat. |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| IE822257L IE822257L (en) | 1983-03-17 |
| IE53413B1 true IE53413B1 (en) | 1988-11-09 |
Family
ID=19838077
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IE2257/82A IE53413B1 (en) | 1981-09-17 | 1982-09-16 | Process for the preparation of magnesium nitrate hexahydrate |
Country Status (12)
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3373644D1 (en) * | 1982-10-01 | 1987-10-22 | Stamicarbon | Production of magnesium nitrate solutions |
| NL8503443A (nl) * | 1985-12-13 | 1987-07-01 | Nl Stikstof | Werkwijze voor de bereiding van een magnesiumnitraat bevattende oplossing, die geschikt is voor toepassing bij de vervaardiging van technisch stabiele ammoniumnitraat bevattende meststofkorrels. |
| US5012019A (en) * | 1990-01-26 | 1991-04-30 | Olin Corporation | Process for purifying aromatic nitration products |
| RU2285667C1 (ru) * | 2005-01-11 | 2006-10-20 | Открытое акционерное общество "Азот" | Способ получения гексагидрата нитрата магния высокой чистоты из технического раствора нитрата магния |
| RU2395457C1 (ru) * | 2008-12-22 | 2010-07-27 | Закрытое акционерное общество "Завод "БИНИТ" | Способ получения гексагидрата нитрата магния путем комплексной переработки серпентинита |
| US20100301288A1 (en) * | 2009-06-01 | 2010-12-02 | Los Alamos National Security, Llc | Preparation of nuclear fuel composition and recycling |
| CN104086235B (zh) * | 2014-07-22 | 2016-02-24 | 路永宽 | 一种利用钢带造粒机生产全水溶性硝酸铵镁的方法 |
| CN104098115B (zh) * | 2014-07-22 | 2016-03-30 | 路永宽 | 一种利用钢带造粒机生产全水溶性片状硝酸镁的方法 |
| EP3418267A1 (en) * | 2017-06-23 | 2018-12-26 | YARA International ASA | Improvement of anti-caking properties of ammonium nitrate particles that are stored in a closed container |
| WO2022051671A1 (en) * | 2020-09-04 | 2022-03-10 | Lyme Revive Foundation | Mineral cation complex compositions, formulations therof, and methods of use therof |
| CN115155493B (zh) * | 2022-07-05 | 2024-07-26 | 山西金兰化工股份有限公司 | 一种硝酸镁连续中和装置及制备工艺 |
| CN119954186B (zh) * | 2025-04-11 | 2025-07-01 | 山东海化骊潍新材料有限公司 | 一种硝酸镁制备过程中的反应热利用方法 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA534723A (en) | 1956-12-18 | Slot Willem | Treatment of impure calcium nitrate | |
| BE344123A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1926-10-16 | |||
| US1844862A (en) * | 1927-10-01 | 1932-02-09 | Hercules Powder Co Ltd | Method of producing hydrated metal nitrates |
| GB300632A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1927-11-18 | 1929-08-15 | Kali-Industrie Aktiengesellschaft | |
| US1865303A (en) | 1929-04-03 | 1932-06-28 | App Et Evaporateurs Kestner Sa | Production of nitrate of lime |
| BE425447A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1936-12-31 | |||
| US3173756A (en) * | 1960-11-16 | 1965-03-16 | Monsanto Co | Double nitrate salts and methods for their preparation |
| NL173387C (nl) * | 1979-03-15 | 1984-01-16 | Azote Sa Cie Neerlandaise | Werkwijze voor het maken van stabiele, ammoniumnitraat bevattende meststofkorrels. |
-
1981
- 1981-09-17 NL NL8104284A patent/NL8104284A/nl not_active Application Discontinuation
-
1982
- 1982-09-09 DE DE8282201113T patent/DE3266703D1/de not_active Expired
- 1982-09-09 EP EP82201113A patent/EP0075354B1/en not_active Expired
- 1982-09-09 AT AT82201113T patent/ATE15876T1/de active
- 1982-09-09 ES ES515594A patent/ES8306681A1/es not_active Expired
- 1982-09-15 ZA ZA826769A patent/ZA826769B/xx unknown
- 1982-09-15 US US06/418,547 patent/US4438083A/en not_active Expired - Fee Related
- 1982-09-15 MX MX8210283U patent/MX7369E/es unknown
- 1982-09-15 FI FI823193A patent/FI69442C/fi not_active IP Right Cessation
- 1982-09-16 IE IE2257/82A patent/IE53413B1/en unknown
- 1982-09-16 NO NO823142A patent/NO160072C/no unknown
- 1982-09-17 IN IN1080/CAL/82A patent/IN157872B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| ATE15876T1 (de) | 1985-10-15 |
| MX7369E (es) | 1988-08-09 |
| EP0075354A1 (en) | 1983-03-30 |
| US4438083A (en) | 1984-03-20 |
| ES515594A0 (es) | 1983-06-01 |
| IN157872B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1986-07-12 |
| ZA826769B (en) | 1983-07-27 |
| FI823193L (fi) | 1983-03-18 |
| NO823142L (no) | 1983-03-18 |
| NO160072C (no) | 1989-03-08 |
| IE822257L (en) | 1983-03-17 |
| FI69442C (fi) | 1986-02-10 |
| NO160072B (no) | 1988-11-28 |
| DE3266703D1 (en) | 1985-11-07 |
| FI69442B (fi) | 1985-10-31 |
| FI823193A0 (fi) | 1982-09-15 |
| NL8104284A (nl) | 1983-04-18 |
| EP0075354B1 (en) | 1985-10-02 |
| ES8306681A1 (es) | 1983-06-01 |
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