HUP0001071A2 - Eljárás alkilén-oxidok poliaddíciós reakciótermékeinek előállítására és diszperziós reaktorok az eljárás megvalósításához - Google Patents
Eljárás alkilén-oxidok poliaddíciós reakciótermékeinek előállítására és diszperziós reaktorok az eljárás megvalósításáhozInfo
- Publication number
- HUP0001071A2 HUP0001071A2 HU0001071A HUP0001071A HUP0001071A2 HU P0001071 A2 HUP0001071 A2 HU P0001071A2 HU 0001071 A HU0001071 A HU 0001071A HU P0001071 A HUP0001071 A HU P0001071A HU P0001071 A2 HUP0001071 A2 HU P0001071A2
- Authority
- HU
- Hungary
- Prior art keywords
- reactor
- temperature
- mixture
- reactors
- production
- Prior art date
Links
- 125000002947 alkylene group Chemical group 0.000 title abstract 4
- 238000000034 method Methods 0.000 title abstract 4
- 239000006185 dispersion Substances 0.000 title 1
- 239000003999 initiator Substances 0.000 abstract 3
- 239000000203 mixture Substances 0.000 abstract 3
- 239000007795 chemical reaction product Substances 0.000 abstract 2
- 239000004575 stone Substances 0.000 abstract 2
- 239000004721 Polyphenylene oxide Substances 0.000 abstract 1
- 239000012467 final product Substances 0.000 abstract 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 abstract 1
- 229920000570 polyether Polymers 0.000 abstract 1
- 229920005862 polyol Polymers 0.000 abstract 1
- 150000003077 polyols Chemical class 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
- 239000004094 surface-active agent Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2/00—Processes of polymerisation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2696—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the process or apparatus used
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J10/00—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
- B01J10/002—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor carried out in foam, aerosol or bubbles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
- B01J19/2455—Stationary reactors without moving elements inside provoking a loop type movement of the reactants
- B01J19/2465—Stationary reactors without moving elements inside provoking a loop type movement of the reactants externally, i.e. the mixture leaving the vessel and subsequently re-entering it
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/26—Nozzle-type reactors, i.e. the distribution of the initial reactants within the reactor is effected by their introduction or injection through nozzles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/0009—Coils
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00103—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor in a heat exchanger separate from the reactor
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Dispersion Chemistry (AREA)
- Polyethers (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Gas Separation By Absorption (AREA)
Abstract
A találmány új, félfőlyamatős eljárásra és berendezésekre vőnatkőzik,amelyek alkalmasak alkilén-őxidők pőliaddíciós reakciótermékeinekelőállítására az adőtt alkilén-őxidnak legalább egy aktív hidrőgénnelrendelkező láncinicátőrra való addiciőnáltatása útján. Ezeket atermékeket főleg nemiőnős felületaktív anyagként és pőliéter-pőliőlként alkalmazzák. A találmány szerinti eljárás sőrán - őlyan,két különböző átmérővel rendelkező reaktőrt készítenek elő, amelynyílásőkkal, valamint reaktőr felső részének teljes belső felszínénelhelyezett pőrlasztókkal van ellátva; - előre meghatárőzőttmennyiségű, a lánciniciátőrt magában főglaló főlyadékőt töltenek areaktőrba, - főlyadékőt vezetnek el és hőmérsékletét az előremeghatárőzőtt reakcióhőmérsékletre állítják be, - őlyan közbensőhőmérsékletre állítják be, -őlyan közbenső cseppfőlyós reakcióterméketállítanak elő, amely a cseppfőlyós lánciniciátőrral elegyet képez, és- az így kapőtt, előzőleg az előre meghatárőzőtt reakcióhőmérsékletreismét beállítőtt hőmérsékletű elegyet főlyamatősan visszavezetik areaktőr felső részébe és a bepőrlasztőtt elegy tővábbi alkilén-őxid-mennyiséggel való reagáltatásával a kívánt lánchősszúságú végterméketállítják elő. Az ismertetett reaktőrőkat önmagűkban vagy tővábbi -akár hagyőmányős - reaktőrőkkal sőrba vagy párhűzamősan kapcsőlvaalkalmazzák. ŕ
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP96830658A EP0850954A1 (en) | 1996-12-27 | 1996-12-27 | A method for the production of polyadducts of alkylene oxides with a liquid in a gas dispersion reactor |
Publications (2)
Publication Number | Publication Date |
---|---|
HUP0001071A2 true HUP0001071A2 (hu) | 2000-08-28 |
HUP0001071A3 HUP0001071A3 (en) | 2001-02-28 |
Family
ID=8226098
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
HU0001071A HUP0001071A3 (en) | 1996-12-27 | 1997-12-23 | A method for the production of polyadducts of alkylene oxides and dispersion reactors for making this method |
Country Status (18)
Country | Link |
---|---|
US (1) | US6319999B1 (hu) |
EP (2) | EP0850954A1 (hu) |
JP (1) | JP4510153B2 (hu) |
KR (1) | KR20000069727A (hu) |
CN (1) | CN1111543C (hu) |
AT (1) | ATE233789T1 (hu) |
AU (1) | AU720858B2 (hu) |
BG (1) | BG64216B1 (hu) |
BR (1) | BR9713637A (hu) |
CA (1) | CA2276357A1 (hu) |
DE (1) | DE69719553T2 (hu) |
ES (1) | ES2192278T3 (hu) |
HU (1) | HUP0001071A3 (hu) |
ID (1) | ID23523A (hu) |
RO (1) | RO120544B1 (hu) |
RU (1) | RU2193041C2 (hu) |
TR (1) | TR199901966T2 (hu) |
WO (1) | WO1998029458A1 (hu) |
Families Citing this family (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19937911A1 (de) | 1999-08-11 | 2001-02-15 | Cognis Deutschland Gmbh | Verfahren zum Herstellen von Estern aus ungesättigten Carbonsäuren und mehrwertigen Alkoholen |
DE10008629A1 (de) | 2000-02-24 | 2001-09-06 | Basf Ag | Verfahren zur Herstellung von Polyetherpolyolen in Gegenwart eines Multimetallcyanidkomplex-Katalysators |
DE10008635A1 (de) * | 2000-02-24 | 2001-09-06 | Basf Ag | Verfahren zur Herstellung von Polyetherpolyolen |
DE10008630A1 (de) | 2000-02-24 | 2001-09-06 | Basf Ag | Verfahren zur Herstellung von Polyetherpolyolen in Gegenwart eines Multimetallcyanidkomplex-Katalysators |
US20060147853A1 (en) * | 2005-01-06 | 2006-07-06 | Lipp Charles W | Feed nozzle assembly and burner apparatus for gas/liquid reactions |
CN1883786B (zh) * | 2005-06-24 | 2010-07-28 | 鸿富锦精密工业(深圳)有限公司 | 纳米颗粒合成方法 |
JP5734633B2 (ja) * | 2010-12-09 | 2015-06-17 | 三井化学株式会社 | アルキレンオキサイド付加物の製造方法 |
CN102814157B (zh) * | 2012-08-27 | 2014-06-11 | 江苏远洋药业股份有限公司 | 化工产品瞬间反应用的装置 |
CN102847492A (zh) * | 2012-10-16 | 2013-01-02 | 四川国光农化股份有限公司 | 一种适用于气液反应的制备装置 |
CN104987503A (zh) * | 2015-06-25 | 2015-10-21 | 淄博德信联邦化学工业有限公司 | 硬泡聚醚多元醇的制备方法 |
CN107413291A (zh) * | 2017-06-22 | 2017-12-01 | 江苏凌飞科技股份有限公司 | 一种乙氧基化反应器 |
FR3068620B1 (fr) * | 2017-07-10 | 2020-06-26 | IFP Energies Nouvelles | Procede d’oligomerisation mettant en oeuvre un dispositf reactionnel comprenant un moyen de dispersion |
BR112020015471A2 (pt) * | 2018-01-31 | 2020-12-08 | Basf Se | Processo para a preparação de uma composição de polímero. |
CN110358070B (zh) * | 2019-06-12 | 2021-11-09 | 佳化化学科技发展(上海)有限公司 | 一种低气味聚醚多元醇的生产工艺及系统 |
CN110773085B (zh) * | 2019-11-07 | 2021-10-26 | 浙江工业大学 | 一种气液反应器 |
CN112619577A (zh) * | 2020-11-26 | 2021-04-09 | 瑞昌荣联环保科技有限公司 | 一种高效的亚克力板材反应系统 |
CN112844250B (zh) * | 2021-01-15 | 2022-09-13 | 上海宏韵新型建材有限公司 | 一种混凝土用减水剂的制备工艺 |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB736991A (en) * | 1951-04-09 | 1955-09-21 | Oxirane Ltd | The manufacture of polyoxyalkylene glycols and their mono-ethers |
US3182050A (en) * | 1962-10-19 | 1965-05-04 | Phillips Petroleum Co | Bulk polymerization |
DE1936046C3 (de) * | 1969-07-16 | 1982-09-02 | Hoechst Ag, 6000 Frankfurt | Verfahren zum Herstellen von Anlagerungsprodukten des Äthylenoxids an Verbindungen mit beweglichem Wasserstoff |
US3894093A (en) | 1969-07-16 | 1975-07-08 | Hoechst Ag | Process for the manufacture of addition products of ethylene oxide and compounds containing mobile hydrogen |
DD159262A3 (de) * | 1980-11-28 | 1983-03-02 | Habicher Wolf Dieter | Verfahren zur kontinuierlichen herstellung von polyetheralkoholen |
IT1226405B (it) | 1988-08-26 | 1991-01-15 | Pressind Spa | Processo per la preparazione di prodotti di addizione di ossidi alchidici su composti contenenti idrogeni mobili. |
IT1226406B (it) | 1988-08-26 | 1991-01-15 | Pressind Spa | Processo per la preparazione di prodotti ad alto peso molecolare per addizione di ossidi alchidici su composti contenenti idrogeni mobili. |
US5159092A (en) * | 1989-09-22 | 1992-10-27 | Buss Ag | Process for the safe and environmentally sound production of highly pure alkylene oxide adducts |
DE4300449C2 (de) * | 1993-01-11 | 1996-05-23 | Buna Sow Leuna Olefinverb Gmbh | Verfahren zur Verringerung der Alkenoxidemission bei der Herstellung von Alkenoxid-Anlagerungsprodukten |
EP0724556B1 (en) * | 1993-10-22 | 1998-12-23 | The Dow Chemical Company | Alkylene glycols having a higher primary hydroxyl content |
-
1996
- 1996-12-27 EP EP96830658A patent/EP0850954A1/en not_active Withdrawn
-
1997
- 1997-12-23 AT AT97953916T patent/ATE233789T1/de not_active IP Right Cessation
- 1997-12-23 CA CA002276357A patent/CA2276357A1/en not_active Abandoned
- 1997-12-23 JP JP52960398A patent/JP4510153B2/ja not_active Expired - Lifetime
- 1997-12-23 DE DE69719553T patent/DE69719553T2/de not_active Expired - Lifetime
- 1997-12-23 US US09/331,855 patent/US6319999B1/en not_active Expired - Lifetime
- 1997-12-23 WO PCT/EP1997/007272 patent/WO1998029458A1/en active IP Right Grant
- 1997-12-23 TR TR1999/01966T patent/TR199901966T2/xx unknown
- 1997-12-23 RO RO99-00716A patent/RO120544B1/ro unknown
- 1997-12-23 BR BR9713637-9A patent/BR9713637A/pt not_active IP Right Cessation
- 1997-12-23 AU AU57637/98A patent/AU720858B2/en not_active Ceased
- 1997-12-23 RU RU99115896/04A patent/RU2193041C2/ru active
- 1997-12-23 EP EP97953916A patent/EP0948546B1/en not_active Expired - Lifetime
- 1997-12-23 ID IDW990605D patent/ID23523A/id unknown
- 1997-12-23 CN CN97181062A patent/CN1111543C/zh not_active Expired - Lifetime
- 1997-12-23 HU HU0001071A patent/HUP0001071A3/hu unknown
- 1997-12-23 ES ES97953916T patent/ES2192278T3/es not_active Expired - Lifetime
- 1997-12-23 KR KR19997005814A patent/KR20000069727A/ko not_active Application Discontinuation
-
1999
- 1999-07-26 BG BG103601A patent/BG64216B1/bg unknown
Also Published As
Publication number | Publication date |
---|---|
BG103601A (en) | 2000-04-28 |
AU720858B2 (en) | 2000-06-15 |
HUP0001071A3 (en) | 2001-02-28 |
ID23523A (id) | 2000-04-27 |
JP2001507389A (ja) | 2001-06-05 |
DE69719553T2 (de) | 2004-02-19 |
US6319999B1 (en) | 2001-11-20 |
TR199901966T2 (xx) | 1999-10-21 |
JP4510153B2 (ja) | 2010-07-21 |
BG64216B1 (bg) | 2004-05-31 |
KR20000069727A (ko) | 2000-11-25 |
AU5763798A (en) | 1998-07-31 |
ATE233789T1 (de) | 2003-03-15 |
CN1242018A (zh) | 2000-01-19 |
DE69719553D1 (de) | 2003-04-10 |
EP0948546A1 (en) | 1999-10-13 |
MX9905998A (es) | 1999-11-01 |
RO120544B1 (ro) | 2006-03-30 |
BR9713637A (pt) | 2000-04-11 |
WO1998029458A1 (en) | 1998-07-09 |
EP0850954A1 (en) | 1998-07-01 |
EP0948546B1 (en) | 2003-03-05 |
ES2192278T3 (es) | 2003-10-01 |
CA2276357A1 (en) | 1998-07-09 |
RU2193041C2 (ru) | 2002-11-20 |
CN1111543C (zh) | 2003-06-18 |
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