GB584977A - Improvements in or relating to the electro-deposition of nickel and nickel alloys - Google Patents
Improvements in or relating to the electro-deposition of nickel and nickel alloysInfo
- Publication number
- GB584977A GB584977A GB18720/44A GB1872044A GB584977A GB 584977 A GB584977 A GB 584977A GB 18720/44 A GB18720/44 A GB 18720/44A GB 1872044 A GB1872044 A GB 1872044A GB 584977 A GB584977 A GB 584977A
- Authority
- GB
- United Kingdom
- Prior art keywords
- nickel
- gms
- sodium
- per litre
- cobalt
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical group [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 title abstract 6
- 229910000990 Ni alloy Inorganic materials 0.000 title abstract 3
- 229910052759 nickel Inorganic materials 0.000 title abstract 3
- 238000004070 electrodeposition Methods 0.000 title abstract 2
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical class C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 abstract 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 abstract 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 abstract 2
- 229910017052 cobalt Inorganic materials 0.000 abstract 2
- 239000010941 cobalt Substances 0.000 abstract 2
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 abstract 2
- PUZPDOWCWNUUKD-UHFFFAOYSA-M sodium fluoride Chemical compound [F-].[Na+] PUZPDOWCWNUUKD-UHFFFAOYSA-M 0.000 abstract 2
- 239000000080 wetting agent Substances 0.000 abstract 2
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 abstract 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 1
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 abstract 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 abstract 1
- 239000004327 boric acid Substances 0.000 abstract 1
- 229910052793 cadmium Inorganic materials 0.000 abstract 1
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 abstract 1
- CXKCTMHTOKXKQT-UHFFFAOYSA-N cadmium oxide Inorganic materials [Cd]=O CXKCTMHTOKXKQT-UHFFFAOYSA-N 0.000 abstract 1
- CFEAAQFZALKQPA-UHFFFAOYSA-N cadmium(2+);oxygen(2-) Chemical compound [O-2].[Cd+2] CFEAAQFZALKQPA-UHFFFAOYSA-N 0.000 abstract 1
- KTVIXTQDYHMGHF-UHFFFAOYSA-L cobalt(2+) sulfate Chemical compound [Co+2].[O-]S([O-])(=O)=O KTVIXTQDYHMGHF-UHFFFAOYSA-L 0.000 abstract 1
- 239000000470 constituent Substances 0.000 abstract 1
- 239000000356 contaminant Substances 0.000 abstract 1
- 238000000151 deposition Methods 0.000 abstract 1
- 230000008021 deposition Effects 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- LGQLOGILCSXPEA-UHFFFAOYSA-L nickel sulfate Chemical compound [Ni+2].[O-]S([O-])(=O)=O LGQLOGILCSXPEA-UHFFFAOYSA-L 0.000 abstract 1
- 239000004848 polyfunctional curative Substances 0.000 abstract 1
- 239000012286 potassium permanganate Substances 0.000 abstract 1
- 229910052708 sodium Inorganic materials 0.000 abstract 1
- 239000011734 sodium Substances 0.000 abstract 1
- 239000011780 sodium chloride Substances 0.000 abstract 1
- 239000011775 sodium fluoride Substances 0.000 abstract 1
- 235000013024 sodium fluoride Nutrition 0.000 abstract 1
- 229910052938 sodium sulfate Inorganic materials 0.000 abstract 1
- 235000011152 sodium sulphate Nutrition 0.000 abstract 1
- RHZZVWTVJHZKAH-UHFFFAOYSA-K trisodium;naphthalene-1,2,3-trisulfonate Chemical compound [Na+].[Na+].[Na+].C1=CC=C2C(S([O-])(=O)=O)=C(S([O-])(=O)=O)C(S(=O)(=O)[O-])=CC2=C1 RHZZVWTVJHZKAH-UHFFFAOYSA-K 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D3/00—Electroplating: Baths therefor
- C25D3/02—Electroplating: Baths therefor from solutions
- C25D3/56—Electroplating: Baths therefor from solutions of alloys
- C25D3/562—Electroplating: Baths therefor from solutions of alloys containing more than 50% by weight of iron or nickel or cobalt
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D3/00—Electroplating: Baths therefor
- C25D3/02—Electroplating: Baths therefor from solutions
- C25D3/12—Electroplating: Baths therefor from solutions of nickel or cobalt
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Electroplating And Plating Baths Therefor (AREA)
- Pyrrole Compounds (AREA)
- Secondary Cells (AREA)
- Paints Or Removers (AREA)
Abstract
584,977. Electrodeposition of nickel and nickel alloys. LONDON & SCANDINAVIAN METALLURGICAL CO., Ltd., SPIRO, P., and WOHLGEMUTH, F. Sept. 29, 1944, No. 18720. [Class 41] Nickel or a nickel alloy is deposited from a bath containing a fluoride and cobalt with the addition of an organic hardener having a sodium naphthalene trisulphonate base and a wetting agent consisting of a sulphonated aliphatic alcohol containing sodium sulphate. The deposit may contain an appreciable quantity of cobalt or a trace only according to conditions. Cadmium may be added to the bath to give a deposit not subject to embrittlement by heat treatment. A suitable basic bath constitution is nickel sulphate 220-340, cobalt sulphate 6.28-22, boric acid 25.2-37.7, sodium fluoride 6.28-15.7, sodium chloride 1.57-12.56 gms. per litre of solution. Cadmium oxide may be added in the proportion 0.044-0.22 gms. per litre of solution. The constituents are dissolved and the solution oxidized by means of potassium permanganate or otherwise to remove organic contaminants and filtered. There are then added 1-5 gms. per litre of 1-3-6 sodium napthalene trisulphonate and 1-3 gms. of the wetting agent known as "Claytavon W.M." (containing ¢-1¢ gm.s. of sulphonated aliphatic alcohol) per litre. Deposition may be effected on non- conducting bodies provided with a conductive layer.
Priority Applications (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB18720/44A GB584977A (en) | 1944-09-29 | 1944-09-29 | Improvements in or relating to the electro-deposition of nickel and nickel alloys |
| US619904A US2519858A (en) | 1944-09-29 | 1945-10-02 | Electrodeposition of nickel and nickel alloys |
| FR944048D FR944048A (en) | 1944-09-29 | 1945-10-22 | Improvements in electrical precipitation processes for nickel and nickel alloys |
| DEP459A DE804278C (en) | 1944-09-29 | 1948-11-13 | Electrolyte for the galvanic production of coatings from nickel and nickel alloys on metal and non-conductors |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB18720/44A GB584977A (en) | 1944-09-29 | 1944-09-29 | Improvements in or relating to the electro-deposition of nickel and nickel alloys |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB584977A true GB584977A (en) | 1947-01-28 |
Family
ID=10117250
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB18720/44A Expired GB584977A (en) | 1944-09-29 | 1944-09-29 | Improvements in or relating to the electro-deposition of nickel and nickel alloys |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US2519858A (en) |
| DE (1) | DE804278C (en) |
| FR (1) | FR944048A (en) |
| GB (1) | GB584977A (en) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL101173C (en) * | 1952-04-22 | |||
| BE526094A (en) * | 1953-09-19 | |||
| GB765958A (en) * | 1953-12-10 | 1957-01-16 | Vickers Ltd Sa | Improvements in or relating to the electro-deposition of nickel and nickel alloys |
| US3274079A (en) * | 1962-07-19 | 1966-09-20 | M & T Chemicals Inc | Bath and process for the electrodeposition of nickel and nickel-cobalt alloys |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US998085A (en) * | 1909-02-23 | 1911-07-18 | Frank Iorns Gibbs | Method of producing metallic vessels by electrodeposition. |
| DE688814C (en) * | 1935-02-14 | 1940-03-02 | Harshaw Chem Corp | free nickel deposits |
| US2119304A (en) * | 1935-08-01 | 1938-05-31 | Eaton Detroit Metal Company | Electroplating |
| US2228991A (en) * | 1936-01-20 | 1941-01-14 | Seymour Mfg Co | Production of bright nickel deposit |
| US2125229A (en) * | 1936-04-14 | 1938-07-26 | Harshaw Chem Corp | Electrodeposition of metals |
| US2147415A (en) * | 1937-05-11 | 1939-02-14 | Eastman Kodak Co | Electroplating |
| US2238861A (en) * | 1938-07-06 | 1941-04-15 | Harshaw Chem Corp | Electrodeposition of metals |
| US2313756A (en) * | 1939-03-01 | 1943-03-16 | Dow Chemical Co | Method of electroplating magnesium |
| US2191813A (en) * | 1939-12-01 | 1940-02-27 | Udylite Corp | Electrodeposition of nickel from an acid bath |
| US2198267A (en) * | 1939-12-14 | 1940-04-23 | Harshaw Chem Corp | Electrodeposition of metals |
| US2315802A (en) * | 1940-04-20 | 1943-04-06 | Harshaw Chem Corp | Nickel plating |
-
1944
- 1944-09-29 GB GB18720/44A patent/GB584977A/en not_active Expired
-
1945
- 1945-10-02 US US619904A patent/US2519858A/en not_active Expired - Lifetime
- 1945-10-22 FR FR944048D patent/FR944048A/en not_active Expired
-
1948
- 1948-11-13 DE DEP459A patent/DE804278C/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| DE804278C (en) | 1951-04-19 |
| US2519858A (en) | 1950-08-22 |
| FR944048A (en) | 1949-03-24 |
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