GB1351949A - Process for hydrating a nitrile to the corresponding amide - Google Patents
Process for hydrating a nitrile to the corresponding amideInfo
- Publication number
- GB1351949A GB1351949A GB2853271A GB2853271A GB1351949A GB 1351949 A GB1351949 A GB 1351949A GB 2853271 A GB2853271 A GB 2853271A GB 2853271 A GB2853271 A GB 2853271A GB 1351949 A GB1351949 A GB 1351949A
- Authority
- GB
- United Kingdom
- Prior art keywords
- nitrile
- mixture
- oxide
- copper oxide
- nitriles
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000002825 nitriles Chemical class 0.000 title abstract 5
- 150000001408 amides Chemical class 0.000 title abstract 2
- 230000000887 hydrating effect Effects 0.000 title 1
- QPLDLSVMHZLSFG-UHFFFAOYSA-N Copper oxide Chemical compound [Cu]=O QPLDLSVMHZLSFG-UHFFFAOYSA-N 0.000 abstract 3
- 239000005751 Copper oxide Substances 0.000 abstract 3
- 229910000431 copper oxide Inorganic materials 0.000 abstract 3
- 239000000203 mixture Substances 0.000 abstract 3
- 239000003054 catalyst Substances 0.000 abstract 2
- IHXNSHZBFXGOJM-HWKANZROSA-N (e)-2-methylbut-2-enenitrile Chemical compound C\C=C(/C)C#N IHXNSHZBFXGOJM-HWKANZROSA-N 0.000 abstract 1
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 abstract 1
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 abstract 1
- 229910052684 Cerium Inorganic materials 0.000 abstract 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 abstract 1
- 229910052692 Dysprosium Inorganic materials 0.000 abstract 1
- 229910052691 Erbium Inorganic materials 0.000 abstract 1
- 229910052693 Europium Inorganic materials 0.000 abstract 1
- 229910052688 Gadolinium Inorganic materials 0.000 abstract 1
- 229910052689 Holmium Inorganic materials 0.000 abstract 1
- 229910052779 Neodymium Inorganic materials 0.000 abstract 1
- 229910052781 Neptunium Inorganic materials 0.000 abstract 1
- 229910052777 Praseodymium Inorganic materials 0.000 abstract 1
- 229910052774 Proactinium Inorganic materials 0.000 abstract 1
- 229910052772 Samarium Inorganic materials 0.000 abstract 1
- 229910052771 Terbium Inorganic materials 0.000 abstract 1
- 229910052776 Thorium Inorganic materials 0.000 abstract 1
- 229910052775 Thulium Inorganic materials 0.000 abstract 1
- 229910052770 Uranium Inorganic materials 0.000 abstract 1
- 229910052769 Ytterbium Inorganic materials 0.000 abstract 1
- 125000005605 benzo group Chemical group 0.000 abstract 1
- 229910052790 beryllium Inorganic materials 0.000 abstract 1
- 229910052793 cadmium Inorganic materials 0.000 abstract 1
- 229910052791 calcium Inorganic materials 0.000 abstract 1
- 239000003638 chemical reducing agent Substances 0.000 abstract 1
- 229910052802 copper Inorganic materials 0.000 abstract 1
- 239000010949 copper Substances 0.000 abstract 1
- NKKMVIVFRUYPLQ-NSCUHMNNSA-N crotononitrile Chemical compound C\C=C\C#N NKKMVIVFRUYPLQ-NSCUHMNNSA-N 0.000 abstract 1
- 229910052733 gallium Inorganic materials 0.000 abstract 1
- 229910052732 germanium Inorganic materials 0.000 abstract 1
- 229910052735 hafnium Inorganic materials 0.000 abstract 1
- 229910052738 indium Inorganic materials 0.000 abstract 1
- 229910052741 iridium Inorganic materials 0.000 abstract 1
- 229910052742 iron Inorganic materials 0.000 abstract 1
- 229910052746 lanthanum Inorganic materials 0.000 abstract 1
- 229910052745 lead Inorganic materials 0.000 abstract 1
- 229910052749 magnesium Inorganic materials 0.000 abstract 1
- 229910052748 manganese Inorganic materials 0.000 abstract 1
- 229910052751 metal Inorganic materials 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 229910052759 nickel Inorganic materials 0.000 abstract 1
- 229910052758 niobium Inorganic materials 0.000 abstract 1
- WOVJAWMZNOWDII-UHFFFAOYSA-N non-2-enenitrile Chemical compound CCCCCCC=CC#N WOVJAWMZNOWDII-UHFFFAOYSA-N 0.000 abstract 1
- 229910052762 osmium Inorganic materials 0.000 abstract 1
- 229910052763 palladium Inorganic materials 0.000 abstract 1
- XQZYPMVTSDWCCE-UHFFFAOYSA-N phthalonitrile Chemical compound N#CC1=CC=CC=C1C#N XQZYPMVTSDWCCE-UHFFFAOYSA-N 0.000 abstract 1
- 229920006391 phthalonitrile polymer Polymers 0.000 abstract 1
- 229910052697 platinum Inorganic materials 0.000 abstract 1
- -1 propio- Chemical class 0.000 abstract 1
- 229910052702 rhenium Inorganic materials 0.000 abstract 1
- 229910052703 rhodium Inorganic materials 0.000 abstract 1
- 229910052707 ruthenium Inorganic materials 0.000 abstract 1
- 229910052710 silicon Inorganic materials 0.000 abstract 1
- 229910052712 strontium Inorganic materials 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- 229910052715 tantalum Inorganic materials 0.000 abstract 1
- 229910052716 thallium Inorganic materials 0.000 abstract 1
- 229910052718 tin Inorganic materials 0.000 abstract 1
- 229910052721 tungsten Inorganic materials 0.000 abstract 1
- 229910052720 vanadium Inorganic materials 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
- 229910052727 yttrium Inorganic materials 0.000 abstract 1
- 229910052725 zinc Inorganic materials 0.000 abstract 1
- 229910052726 zirconium Inorganic materials 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/16—Reducing
- B01J37/18—Reducing with gases containing free hydrogen
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/72—Copper
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US4716670A | 1970-06-17 | 1970-06-17 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1351949A true GB1351949A (en) | 1974-05-15 |
Family
ID=21947409
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB2853271A Expired GB1351949A (en) | 1970-06-17 | 1971-06-17 | Process for hydrating a nitrile to the corresponding amide |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US3696152A (enExample) |
| JP (1) | JPS5241241B1 (enExample) |
| BE (1) | BE768658A (enExample) |
| CA (1) | CA975005A (enExample) |
| DE (1) | DE2129423C3 (enExample) |
| FR (1) | FR2096309A5 (enExample) |
| GB (1) | GB1351949A (enExample) |
| NL (1) | NL170279C (enExample) |
| ZA (1) | ZA712602B (enExample) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0051984A1 (en) * | 1980-11-06 | 1982-05-19 | Sumitomo Chemical Company, Limited | A method for the production of acrylamide |
| US5894989A (en) * | 1996-04-25 | 1999-04-20 | Kao Corporation | Electrostatic powder coating gun |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4329500A (en) * | 1970-11-19 | 1982-05-11 | The Dow Chemical Company | Catalysts for the hydration of nitriles to amides |
| GB1404532A (en) * | 1972-09-02 | 1975-09-03 | Mitsubishi Chem Ind | Process for hydrating a nitrile to the corresponding amide |
| US3966810A (en) * | 1972-09-02 | 1976-06-29 | Tokuzo Kurata | Process for hydrating a nitrile to the corresponding amide |
| US3884975A (en) * | 1972-10-05 | 1975-05-20 | American Cyanamid Co | Rhodium catalyst for hydration of acrylonitrile |
| US3956387A (en) * | 1973-04-19 | 1976-05-11 | Basf Aktiengesellschaft | Manufacture of concentrated aqueous (meth)acrylamide solutions by catalytic addition of water to (meth)acrylonitrile |
| DE2320060C2 (de) * | 1973-04-19 | 1982-10-14 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Herstellung von Carbonsäureamiden |
| US3944609A (en) * | 1973-06-01 | 1976-03-16 | American Cyanamid Company | Catalyst preparation method |
| US3900516A (en) * | 1973-11-01 | 1975-08-19 | Nalco Chemical Co | Process for making acrylamide |
| US3929421A (en) * | 1973-12-26 | 1975-12-30 | Nalco Chemical Co | Tubular catalytic reactor with premixing means for multiple reactants of different densities |
| US4178310A (en) * | 1975-03-17 | 1979-12-11 | American Cyanamid Company | Catalyst for hydration of nitriles |
| US4096184A (en) * | 1976-01-19 | 1978-06-20 | Sumitomo Chemical Company, Limited | Process for preparing acid amides |
| US4250111A (en) * | 1976-07-12 | 1981-02-10 | Nalco Chemical Company | Mixed catalyst for the hydrolysis of nitriles to amides |
| US4322532A (en) * | 1980-11-17 | 1982-03-30 | Nalco Chemical Company | Solvents for the catalytic production of acrylamide from acrylonitrile and water |
| DE3767365D1 (de) * | 1986-05-21 | 1991-02-21 | Allied Colloids Ltd | Katalysatoren und ihre verwendung fuer die hydrolyse von nitrilen. |
| JPS62203093U (enExample) * | 1986-06-14 | 1987-12-24 | ||
| GB8727379D0 (en) * | 1987-11-23 | 1987-12-23 | Allied Colloids Ltd | Catalysts |
| TW316852B (enExample) * | 1994-08-02 | 1997-10-01 | Mitsui Toatsu Chemicals | |
| DE10161674A1 (de) * | 2001-12-14 | 2003-06-26 | Basf Ag | Katalysatoren zur Herstellung von Carbonsäuresalzen |
| CN111196763B (zh) * | 2018-11-16 | 2021-06-01 | 中国科学院大连化学物理研究所 | 一种3-羟基丙腈加氢生产3-氨基丙醇的催化剂及其制备方法 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB203812A (en) * | 1922-06-20 | 1923-09-20 | Basf Ag | An improved process for producing formic acid derivatives |
| DE1154086B (de) * | 1961-11-10 | 1963-09-12 | Basf Ag | Verfahren zur Herstellung von Glycidamid |
| US3381034A (en) * | 1965-06-30 | 1968-04-30 | Standard Oil Co | Process for hydrolyzing nitriles |
| US3597481A (en) * | 1969-01-16 | 1971-08-03 | Dow Chemical Co | Heterogeneous catalyst for the liquid phase hydrolysis of nitriles to amides |
-
1970
- 1970-06-17 US US47166A patent/US3696152A/en not_active Expired - Lifetime
-
1971
- 1971-04-20 CA CA110,870A patent/CA975005A/en not_active Expired
- 1971-04-22 ZA ZA712602A patent/ZA712602B/xx unknown
- 1971-05-07 NL NLAANVRAGE7106295,A patent/NL170279C/xx not_active IP Right Cessation
- 1971-06-14 FR FR7121554A patent/FR2096309A5/fr not_active Expired
- 1971-06-14 DE DE2129423A patent/DE2129423C3/de not_active Expired
- 1971-06-17 BE BE768658A patent/BE768658A/xx not_active IP Right Cessation
- 1971-06-17 GB GB2853271A patent/GB1351949A/en not_active Expired
- 1971-06-17 JP JP46043032A patent/JPS5241241B1/ja active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0051984A1 (en) * | 1980-11-06 | 1982-05-19 | Sumitomo Chemical Company, Limited | A method for the production of acrylamide |
| US5894989A (en) * | 1996-04-25 | 1999-04-20 | Kao Corporation | Electrostatic powder coating gun |
Also Published As
| Publication number | Publication date |
|---|---|
| US3696152A (en) | 1972-10-03 |
| FR2096309A5 (enExample) | 1972-02-11 |
| NL170279C (nl) | 1982-10-18 |
| BE768658A (fr) | 1971-12-17 |
| CA975005A (en) | 1975-09-23 |
| DE2129423B2 (de) | 1981-07-30 |
| ZA712602B (en) | 1972-01-26 |
| DE2129423C3 (de) | 1982-05-13 |
| NL7106295A (enExample) | 1971-12-21 |
| JPS5241241B1 (enExample) | 1977-10-17 |
| DE2129423A1 (de) | 1971-12-30 |
| NL170279B (nl) | 1982-05-17 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PCNP | Patent ceased through non-payment of renewal fee |