FR3123070B1 - Procede d’extraction et de transformation par transesterification de phtalates contenus dans des plastiques pvc - Google Patents

Procede d’extraction et de transformation par transesterification de phtalates contenus dans des plastiques pvc Download PDF

Info

Publication number
FR3123070B1
FR3123070B1 FR2105300A FR2105300A FR3123070B1 FR 3123070 B1 FR3123070 B1 FR 3123070B1 FR 2105300 A FR2105300 A FR 2105300A FR 2105300 A FR2105300 A FR 2105300A FR 3123070 B1 FR3123070 B1 FR 3123070B1
Authority
FR
France
Prior art keywords
liquid
phthalate
solid
pvc
dialkylphthalate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR2105300A
Other languages
English (en)
French (fr)
Other versions
FR3123070A1 (fr
Inventor
Nicolas Cadran
Alexandra Chaumonnot
Vincent Coupard
Damien Delcroix
Marc Jacquin
David Pasquier
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
IFP Energies Nouvelles IFPEN
Original Assignee
IFP Energies Nouvelles IFPEN
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to FR2105300A priority Critical patent/FR3123070B1/fr
Application filed by IFP Energies Nouvelles IFPEN filed Critical IFP Energies Nouvelles IFPEN
Priority to AU2022275987A priority patent/AU2022275987A1/en
Priority to CA3213694A priority patent/CA3213694A1/fr
Priority to JP2023571658A priority patent/JP2024518623A/ja
Priority to BR112023020502A priority patent/BR112023020502A2/pt
Priority to MX2023013269A priority patent/MX2023013269A/es
Priority to CN202280036046.1A priority patent/CN117321126A/zh
Priority to PCT/EP2022/062082 priority patent/WO2022243043A1/fr
Priority to KR1020237044000A priority patent/KR20240010498A/ko
Priority to US18/561,764 priority patent/US20240239983A1/en
Priority to EP22727177.2A priority patent/EP4341332A1/fr
Priority to TW111118530A priority patent/TW202311391A/zh
Publication of FR3123070A1 publication Critical patent/FR3123070A1/fr
Application granted granted Critical
Publication of FR3123070B1 publication Critical patent/FR3123070B1/fr
Priority to CONC2023/0015466A priority patent/CO2023015466A2/es
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J11/00—Recovery or working-up of waste materials
    • C08J11/02—Recovery or working-up of waste materials of solvents, plasticisers or unreacted monomers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B17/00—Recovery of plastics or other constituents of waste material containing plastics
    • B29B17/02—Separating plastics from other materials
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/02—Preparation of carboxylic acid esters by interreacting ester groups, i.e. transesterification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/58—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J11/00—Recovery or working-up of waste materials
    • C08J11/04—Recovery or working-up of waste materials of polymers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B17/00—Recovery of plastics or other constituents of waste material containing plastics
    • B29B17/04—Disintegrating plastics, e.g. by milling
    • B29B17/0412—Disintegrating plastics, e.g. by milling to large particles, e.g. beads, granules, flakes, slices
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B17/00—Recovery of plastics or other constituents of waste material containing plastics
    • B29B17/02—Separating plastics from other materials
    • B29B2017/0213—Specific separating techniques
    • B29B2017/0293—Dissolving the materials in gases or liquids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B17/00—Recovery of plastics or other constituents of waste material containing plastics
    • B29B17/02—Separating plastics from other materials
    • B29B2017/0213—Specific separating techniques
    • B29B2017/0293—Dissolving the materials in gases or liquids
    • B29B2017/0296—Dissolving the materials in aqueous alkaline solutions, e.g. NaOH or KOH
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2027/00—Use of polyvinylhalogenides or derivatives thereof as moulding material
    • B29K2027/06—PVC, i.e. polyvinylchloride
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2105/00—Condition, form or state of moulded material or of the material to be shaped
    • B29K2105/0005—Condition, form or state of moulded material or of the material to be shaped containing compounding ingredients
    • B29K2105/0038—Plasticisers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2327/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers
    • C08J2327/02—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers not modified by chemical after-treatment
    • C08J2327/04—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers not modified by chemical after-treatment containing chlorine atoms
    • C08J2327/06—Homopolymers or copolymers of vinyl chloride
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/141—Feedstock
    • Y02P20/143—Feedstock the feedstock being recycled material, e.g. plastics
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00—Technologies for solid waste management
    • Y02W30/50—Reuse, recycling or recovery technologies
    • Y02W30/62—Plastics recycling; Rubber recycling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Polymers & Plastics (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Sustainable Development (AREA)
  • Environmental & Geological Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Separation, Recovery Or Treatment Of Waste Materials Containing Plastics (AREA)
FR2105300A 2021-05-20 2021-05-20 Procede d’extraction et de transformation par transesterification de phtalates contenus dans des plastiques pvc Active FR3123070B1 (fr)

Priority Applications (13)

Application Number Priority Date Filing Date Title
FR2105300A FR3123070B1 (fr) 2021-05-20 2021-05-20 Procede d’extraction et de transformation par transesterification de phtalates contenus dans des plastiques pvc
EP22727177.2A EP4341332A1 (fr) 2021-05-20 2022-05-05 Procede d'extraction et de transformation par transesterification de phtalates contenus dans des plastiques pvc
JP2023571658A JP2024518623A (ja) 2021-05-20 2022-05-05 Ｐｖｃプラスチック材料中に含有されるフタラートの抽出およびエステル交換による変換のための方法
BR112023020502A BR112023020502A2 (pt) 2021-05-20 2022-05-05 Método para extracção e transformação por transesterificação de ftalatos contidos em materiais plásticos de pvc
MX2023013269A MX2023013269A (es) 2021-05-20 2022-05-05 Metodo de extraccion y transformacion por transesterificacion de los ftalatos contenidos en los materiales de plastico de cloruro de polivinilo (pvc).
CN202280036046.1A CN117321126A (zh) 2021-05-20 2022-05-05 提取和通过酯交换转化pvc塑料材料中所含邻苯二甲酸酯的方法
AU2022275987A AU2022275987A1 (en) 2021-05-20 2022-05-05 Method for extraction and transformation by transesterification of phthalates contained in pvc plastics materials
KR1020237044000A KR20240010498A (ko) 2021-05-20 2022-05-05 Pvc 플라스틱 재료에 함유된 프탈레이트의 에스테르 교환반응에 의한 추출 및 변환 방법
US18/561,764 US20240239983A1 (en) 2021-05-20 2022-05-05 Method for extraction and transformation by transesterification of phthalates contained in pvc plastics materials
CA3213694A CA3213694A1 (fr) 2021-05-20 2022-05-05 Procede d'extraction et de transformation par transesterification de phtalates contenus dans des plastiques pvc
PCT/EP2022/062082 WO2022243043A1 (fr) 2021-05-20 2022-05-05 Procede d'extraction et de transformation par transesterification de phtalates contenus dans des plastiques pvc
TW111118530A TW202311391A (zh) 2021-05-20 2022-05-18 對ｐｖｃ塑料中包含之鄰苯二甲酸酯類進行萃取及轉酯化反應之轉化方法
CONC2023/0015466A CO2023015466A2 (es) 2021-05-20 2023-11-16 Método de extracción y transformación mediante transesterificación de ftalatos contenidos en materiales plásticos de pvc

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR2105300A FR3123070B1 (fr) 2021-05-20 2021-05-20 Procede d’extraction et de transformation par transesterification de phtalates contenus dans des plastiques pvc
FR2105300 2021-05-20

Publications (2)

Publication Number Publication Date
FR3123070A1 FR3123070A1 (fr) 2022-11-25
FR3123070B1 true FR3123070B1 (fr) 2023-06-02

Family

ID=77021478

Family Applications (1)

Application Number Title Priority Date Filing Date
FR2105300A Active FR3123070B1 (fr) 2021-05-20 2021-05-20 Procede d’extraction et de transformation par transesterification de phtalates contenus dans des plastiques pvc

Country Status (13)

Country Link
US (1) US20240239983A1 (https=)
EP (1) EP4341332A1 (https=)
JP (1) JP2024518623A (https=)
KR (1) KR20240010498A (https=)
CN (1) CN117321126A (https=)
AU (1) AU2022275987A1 (https=)
BR (1) BR112023020502A2 (https=)
CA (1) CA3213694A1 (https=)
CO (1) CO2023015466A2 (https=)
FR (1) FR3123070B1 (https=)
MX (1) MX2023013269A (https=)
TW (1) TW202311391A (https=)
WO (1) WO2022243043A1 (https=)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2025120154A1 (en) 2023-12-07 2025-06-12 Inovyn Europe Limited Process for purifying pvc
EP4671317A1 (en) * 2024-03-04 2025-12-31 LG Chem, Ltd. METHOD FOR PREPARING A RECYCLED POLYMER

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS53142476A (en) * 1977-05-18 1978-12-12 Nippon Steel Corp Extraction of plasticizers from non-rigid vinyl chloride resin
JPS5738834A (en) * 1980-08-18 1982-03-03 Shimada Kankyo Kagaku Kenkyusho:Kk Treatment for reclaiming waste polyvinyl chloride
IT1178901B (it) * 1984-03-22 1987-09-16 Irfin S P A Procedimento per il recupero selettivo dei materiali costituenti cascami di cavi elettrici isolati
JPH1112386A (ja) * 1997-06-20 1999-01-19 Yazaki Corp 軟質ビニル製品からの再生原料の回収方法
FR2776664B1 (fr) 1998-03-26 2000-09-15 Ferrari S Tissage & Enduct Sa Procede de recyclage d'articles a base de polymeres du chlorure de vinyle
FR2806731B1 (fr) 2000-03-23 2002-06-14 Solvay Procede de recyclage d'une matiere plastique
DE10039363A1 (de) 2000-08-11 2002-03-07 Fraunhofer Ges Forschung Verfahren zur Trennung und Rückgewinnung von Zielpolymeren und deren Additiven aus einem polymerhaltigen Material
JP4685728B2 (ja) 2005-08-31 2011-05-18 日機装株式会社 鉛含有軟質ポリ塩化ビニル素材の原料回収方法
JP4473225B2 (ja) 2006-01-19 2010-06-02 株式会社神鋼環境ソリューション 再生ポリ塩化ビニルコンパウンド製造方法。
KR100788334B1 (ko) * 2007-01-19 2007-12-27 이종욱 폐폴리염화비닐의 재생방법
EP2119741A1 (en) 2008-05-09 2009-11-18 SOLVAY (Société Anonyme) Process for recycling articles based on a fibre reinforced polymer
CN104236994A (zh) * 2014-09-26 2014-12-24 中华人民共和国台州出入境检验检疫局 一种玩具中邻苯二甲酸酯类化合物的萃取方法

Also Published As

Publication number Publication date
CN117321126A (zh) 2023-12-29
EP4341332A1 (fr) 2024-03-27
KR20240010498A (ko) 2024-01-23
WO2022243043A1 (fr) 2022-11-24
MX2023013269A (es) 2023-11-30
JP2024518623A (ja) 2024-05-01
AU2022275987A1 (en) 2023-10-12
TW202311391A (zh) 2023-03-16
CO2023015466A2 (es) 2024-01-25
CA3213694A1 (fr) 2022-11-24
US20240239983A1 (en) 2024-07-18
FR3123070A1 (fr) 2022-11-25
BR112023020502A2 (pt) 2023-12-05

Similar Documents

Publication Publication Date Title
FR3123069B1 (fr) Procede d’extraction et de transformation par transesterification de phtalates contenus dans des plastiques pvc au moyen d’alcool
FR3123070B1 (fr) Procede d’extraction et de transformation par transesterification de phtalates contenus dans des plastiques pvc
ES2636456T3 (es) Procedimiento para la producción de mentol ópticamente activo y racémico
US8435387B2 (en) Small-scale method and apparatus for separating mixtures
JP6211707B2 (ja) 溶媒分離システムおよび方法
US20090131728A1 (en) Process for the separation of diastereomers
Arregoitia-Sarabia et al. Polyether-block-amide thin-film composite hollow fiber membranes for the recovery of butanol from ABE process by pervaporation
JPH07258129A (ja) １，３−ブチレングリコ−ルの精製方法
EP3802486A1 (fr) Procede de preparation de sel d'imides contenant un groupement fluorosulfonyle
WO2019229360A1 (fr) Procede de preparation d'un sel de lithium de bis(fluorosulfonyl)imide
Trusiano et al. Modification of photocurable epoxides by new perfluoropolyalkylether alcohols for obtaining self-cleaning coatings
Hasanoğlu et al. Pervaporation separation of organics from multicomponent aqueous mixtures
JP2004285064A (ja) ｔｅｒｔ−ブタノール／水−混合物から２−ブタノールを分離する方法
Hsueh et al. Separation of ethanol–water solution by poly (acrylonitrile-co-acrylic acid) membranes
Van Eygen et al. Comparison of distinctive polymeric membrane structures as support materials for membrane extraction of chiral amines
Seibert et al. Hydraulics and mass transfer efficiency of a commercial-scale membrane extractor
山口智彦 et al. Chiral crown ether-mediated transport of phenylglycine through an immobilized liquid membrane.
Scholes et al. Mass transfer correlations for membrane gas-solvent contactors undergoing carbon dioxide desorption
EP0129459A1 (fr) Procédé de purification d'un mélange eau-alcool en C1-C2-impuretés, issu d'un procédé de fabrication industriel d'alcool en C1-C2 au moyen d'un agent d'extraction
FR2909667B1 (fr) Elimination de l'acetonitrile dans la charge olefinique des procedes de production d'ethers par mise en oeuvre de liquides ioniques.
WO2015185835A1 (fr) Procédé d'élimination d'ions métalliques dans une solution organique visqueuse
Parmar et al. Molecular interaction analysis and transport properties of binary liquid mixtures containing 1-Amino-2-propanol and alkyl acetates at T= 298.15–318.15 K: Application of Graph theory and DFT studies
JPS63156738A (ja) １，３−ブチレングリコ−ルの精製法
CN101965340A (zh) 在1,3-二氧戊环-2-酮生产中分离高沸物的膜分离方法
Kitazume et al. Fluorination of carbinols with 2, 2-difluoro-1, 3-dimethylimidazolidine in ionic liquid

Legal Events

Date Code Title Description
PLFP Fee payment

Year of fee payment: 2

PLSC Publication of the preliminary search report

Effective date: 20221125

PLFP Fee payment

Year of fee payment: 3

PLFP Fee payment

Year of fee payment: 4

PLFP Fee payment

Year of fee payment: 5