FR3090393B1 - Procédé de traitement d’une charge alcool pour la production d’oléfines - Google Patents

Procédé de traitement d’une charge alcool pour la production d’oléfines Download PDF

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Publication number
FR3090393B1
FR3090393B1 FR1873651A FR1873651A FR3090393B1 FR 3090393 B1 FR3090393 B1 FR 3090393B1 FR 1873651 A FR1873651 A FR 1873651A FR 1873651 A FR1873651 A FR 1873651A FR 3090393 B1 FR3090393 B1 FR 3090393B1
Authority
FR
France
Prior art keywords
treating
stream
olefins
production
alcohol feed
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR1873651A
Other languages
English (en)
Other versions
FR3090393A1 (fr
Inventor
Nicolas Aribert
Ludovic Chahen
Arnaud Lanoue
Vincent Coupard
Nikolai Nesterenko
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
TotalEnergies One Tech Belgium SA
IFP Energies Nouvelles IFPEN
Original Assignee
Total Research and Technology Feluy SA
IFP Energies Nouvelles IFPEN
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to FR1873651A priority Critical patent/FR3090393B1/fr
Application filed by Total Research and Technology Feluy SA, IFP Energies Nouvelles IFPEN filed Critical Total Research and Technology Feluy SA
Priority to US17/415,910 priority patent/US20220064088A1/en
Priority to PCT/EP2019/082776 priority patent/WO2020126374A1/fr
Priority to EP19806300.0A priority patent/EP3897897A1/fr
Priority to JP2021535588A priority patent/JP2022514360A/ja
Priority to BR112021010648-0A priority patent/BR112021010648A2/pt
Priority to CN201980083283.1A priority patent/CN113453775B/zh
Priority to CA3121907A priority patent/CA3121907A1/fr
Publication of FR3090393A1 publication Critical patent/FR3090393A1/fr
Application granted granted Critical
Publication of FR3090393B1 publication Critical patent/FR3090393B1/fr
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/001—Processes specially adapted for distillation or rectification of fermented solutions
    • B01D3/002—Processes specially adapted for distillation or rectification of fermented solutions by continuous methods
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/001—Processes specially adapted for distillation or rectification of fermented solutions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/007—Energy recuperation; Heat pumps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/06—Flash distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B01D3/148—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step in combination with at least one evaporator
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/40—Extractive distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/88—Separation; Purification; Use of additives, e.g. for stabilisation by treatment giving rise to a chemical modification of at least one compound

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)

Abstract

L’invention concerne un procédé de traitement d’une charge alcoolique comprenant : a) une étape de préchauffe de ladite charge alcoolique à une température comprise entre 70°C et 200°C ; b) une étape de prétraitement sur un solide acide, opérant à une température comprise entre 70°C et 200°C, pour produire une charge alcoolique prétraitée ; c) une étape de vaporisation partielle pour produire un flux vaporisé et un flux liquide ; et d) une étape de purification du flux liquide issu de l’étape c), en un flux riche en eau, un flux riche en mono-alcool et un flux riche en impuretés. Figure 1 à publier
FR1873651A 2018-12-20 2018-12-20 Procédé de traitement d’une charge alcool pour la production d’oléfines Active FR3090393B1 (fr)

Priority Applications (8)

Application Number Priority Date Filing Date Title
FR1873651A FR3090393B1 (fr) 2018-12-20 2018-12-20 Procédé de traitement d’une charge alcool pour la production d’oléfines
PCT/EP2019/082776 WO2020126374A1 (fr) 2018-12-20 2019-11-27 Procede de traitement d'une charge alcool pour la production d'olefines
EP19806300.0A EP3897897A1 (fr) 2018-12-20 2019-11-27 Procede de traitement d'une charge alcool pour la production d'olefines
JP2021535588A JP2022514360A (ja) 2018-12-20 2019-11-27 オレフィンの製造のためのアルコール供給原料の処理方法
US17/415,910 US20220064088A1 (en) 2018-12-20 2019-11-27 Method for treating an alcohol feedstock for the production of olefins
BR112021010648-0A BR112021010648A2 (pt) 2018-12-20 2019-11-27 processo de tratamento de uma carga de álcool para produção de olefinas
CN201980083283.1A CN113453775B (zh) 2018-12-20 2019-11-27 处理生产烯烃用的醇原料的方法
CA3121907A CA3121907A1 (fr) 2018-12-20 2019-11-27 Procede de traitement d'une charge alcool pour la production d'olefines

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR1873651A FR3090393B1 (fr) 2018-12-20 2018-12-20 Procédé de traitement d’une charge alcool pour la production d’oléfines

Publications (2)

Publication Number Publication Date
FR3090393A1 FR3090393A1 (fr) 2020-06-26
FR3090393B1 true FR3090393B1 (fr) 2021-04-23

Family

ID=66676736

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1873651A Active FR3090393B1 (fr) 2018-12-20 2018-12-20 Procédé de traitement d’une charge alcool pour la production d’oléfines

Country Status (8)

Country Link
US (1) US20220064088A1 (fr)
EP (1) EP3897897A1 (fr)
JP (1) JP2022514360A (fr)
CN (1) CN113453775B (fr)
BR (1) BR112021010648A2 (fr)
CA (1) CA3121907A1 (fr)
FR (1) FR3090393B1 (fr)
WO (1) WO2020126374A1 (fr)

Family Cites Families (33)

* Cited by examiner, † Cited by third party
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US2910412A (en) * 1955-10-17 1959-10-27 Nat Petro Chem Alcohol purification process
GB2091260A (en) * 1981-01-10 1982-07-28 Bp Chem Int Ltd Purification of fermentation alcohol
JPH1143452A (ja) 1997-07-28 1999-02-16 Mitsubishi Chem Corp アルコールの品質改善法
DE102006003492A1 (de) * 2006-01-25 2007-07-26 Oxeno Olefinchemie Gmbh Verfahren zur Entwässerung von Ethanol
KR101512860B1 (ko) * 2006-09-26 2015-04-16 미쓰비시 가가꾸 가부시키가이샤 프로필렌의 제조 방법
CA2565433C (fr) * 2006-10-25 2014-02-11 Iogen Energy Corporation Recuperation de sel inorganique pendant la transformation de matieres premieres lignocellulosiques
US8496831B2 (en) * 2007-08-30 2013-07-30 Membrane Technology And Research, Inc. Dehydration processes using membranes with hydrophobic coating
CN101664611A (zh) * 2008-09-03 2010-03-10 上海市长宁区少年科技指导站 一种有机溶剂回收利用方法
EA020426B1 (ru) 2008-11-28 2014-11-28 Тотал Петрокемикалз Ресерч Фелюи Очистка спиртов перед их применением в присутствии кислотного катализатора
CN101955418B (zh) * 2009-12-16 2013-10-16 华东理工大学 一种耦合分离纯化制备etbe的方法
RU2426716C1 (ru) * 2010-04-06 2011-08-20 Общество с ограниченной ответственностью "Научно-производственное объединение "БиоХимСервис" Способ обезвоживания спиртосодержащей смеси
FR2959750B1 (fr) * 2010-05-06 2013-02-15 Inst Francais Du Petrole Procede de production de kerosene a partir de bio-ethanol.
BR112012028710B1 (pt) * 2010-05-10 2018-09-18 Catalytic Distillation Tech produção de combustível para aviação e outros combustíveis pesados a partir de isobutanol
US8846988B2 (en) * 2010-07-09 2014-09-30 Celanese International Corporation Liquid esterification for the production of alcohols
US9056807B2 (en) * 2010-08-03 2015-06-16 Total Research & Technology Feluy Process to make olefins from isobutanol
FR2978146B1 (fr) 2011-07-21 2013-08-30 IFP Energies Nouvelles Procede de deshydratation de l'ethanol en ethylene a basse consommation energetique
EP2788096A2 (fr) * 2011-12-09 2014-10-15 Butamax Advanced Biofuels LLC Procédé pour éliminer des alcools en produit d'un bouillon de fermentation
TWI622577B (zh) * 2012-09-14 2018-05-01 Technip E&C Limited 醇類的處理
KR20140042402A (ko) * 2012-09-28 2014-04-07 주식회사 엘지화학 올레핀으로부터 알코올의 제조장치 및 제조방법
CN103772102B (zh) * 2012-10-17 2015-08-12 中国石油化工股份有限公司 乙醇脱水制乙烯的分离精制方法
EP2914566A1 (fr) * 2012-10-31 2015-09-09 Shell Internationale Research Maatschappij B.V. Procédés de préparation d'un produit oléfinique
FR2998567B1 (fr) * 2012-11-27 2014-12-26 IFP Energies Nouvelles Procede de deshydratation d'ethanol en ethylene mettant en oeuvre un pretraitement de la charge
FR2998568B1 (fr) 2012-11-27 2015-01-23 IFP Energies Nouvelles Procede de deshydratation de l'ethanol en ethylene a basse consommation
FR3001968B1 (fr) * 2013-02-12 2015-02-27 IFP Energies Nouvelles Procede de production d'oxyde d'ethylene a partir d'un flux d'ethanol thermo-mecaniquement integre
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FR3013707B1 (fr) 2013-11-27 2016-07-29 Ifp Energies Now Procede de deshydratation d'un melange contenant de l'ethanol et de l'isopropanol
FR3013708B1 (fr) * 2013-11-27 2016-07-29 Ifp Energies Now Procede de deshydratation d'un melange contenant de l'ethanol et du n-propanol
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FR3026406B1 (fr) 2014-09-26 2016-12-09 Ifp Energies Now Procede de deshydratation isomerisante d'une charge alcool primaire substitue en position 2 par un groupement alkyl sur un catalyseur comprenant une zeolithe de type fer
CN107074677B (zh) * 2014-12-12 2021-03-09 维尔萨利斯股份公司 用于从1,3-丁二醇产生1,3-丁二烯的工艺
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CN106631801B (zh) * 2015-10-31 2019-07-05 湖南中创化工股份有限公司 一种用甲醇作为共沸剂分离乙酸仲丁酯中杂质的方法及装置

Also Published As

Publication number Publication date
CA3121907A1 (fr) 2020-06-25
BR112021010648A2 (pt) 2021-08-17
JP2022514360A (ja) 2022-02-10
EP3897897A1 (fr) 2021-10-27
CN113453775A (zh) 2021-09-28
FR3090393A1 (fr) 2020-06-26
WO2020126374A1 (fr) 2020-06-25
US20220064088A1 (en) 2022-03-03
CN113453775B (zh) 2023-06-06

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