FR2997317B1 - Adsorbant de tamis moleculaire de 5 a et procede pour la preparation de celui-ci - Google Patents

Adsorbant de tamis moleculaire de 5 a et procede pour la preparation de celui-ci Download PDF

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Publication number
FR2997317B1
FR2997317B1 FR1360564A FR1360564A FR2997317B1 FR 2997317 B1 FR2997317 B1 FR 2997317B1 FR 1360564 A FR1360564 A FR 1360564A FR 1360564 A FR1360564 A FR 1360564A FR 2997317 B1 FR2997317 B1 FR 2997317B1
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FR
France
Prior art keywords
preparation
molecular sieve
sieve adsorbent
adsorbent
molecular
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Active
Application number
FR1360564A
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English (en)
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FR2997317A1 (fr
Inventor
Changzhi TU
Shihua CHEN
Yunlong DING
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Petroleum and Chemical Corp
Sinopec Catalyst Co
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China Petroleum and Chemical Corp
Sinopec Catalyst Co
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Publication of FR2997317A1 publication Critical patent/FR2997317A1/fr
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3071—Washing or leaching
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/16—Alumino-silicates
    • B01J20/18—Synthetic zeolitic molecular sieves
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/16—Alumino-silicates
    • B01J20/18—Synthetic zeolitic molecular sieves
    • B01J20/183—Physical conditioning without chemical treatment, e.g. drying, granulating, coating, irradiation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28002—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their physical properties
    • B01J20/28004—Sorbent size or size distribution, e.g. particle size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28002—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their physical properties
    • B01J20/28011—Other properties, e.g. density, crush strength
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28016—Particle form
    • B01J20/28019—Spherical, ellipsoidal or cylindrical
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28069—Pore volume, e.g. total pore volume, mesopore volume, micropore volume
    • B01J20/28071—Pore volume, e.g. total pore volume, mesopore volume, micropore volume being less than 0.5 ml/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28078—Pore diameter
    • B01J20/2808—Pore diameter being less than 2 nm, i.e. micropores or nanopores
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3042—Use of binding agents; addition of materials ameliorating the mechanical properties of the produced sorbent
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7003—A-type
    • B01J35/40—
    • B01J35/633—
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
FR1360564A 2012-10-29 2013-10-29 Adsorbant de tamis moleculaire de 5 a et procede pour la preparation de celui-ci Active FR2997317B1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CN201210421121 2012-10-29
CN201210421121.4 2012-10-29

Publications (2)

Publication Number Publication Date
FR2997317A1 FR2997317A1 (fr) 2014-05-02
FR2997317B1 true FR2997317B1 (fr) 2018-06-29

Family

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FR1360564A Active FR2997317B1 (fr) 2012-10-29 2013-10-29 Adsorbant de tamis moleculaire de 5 a et procede pour la preparation de celui-ci

Country Status (5)

Country Link
US (1) US9656241B2 (fr)
CN (1) CN103933932B (fr)
ES (1) ES2457917B1 (fr)
FR (1) FR2997317B1 (fr)
IT (1) ITUD20130141A1 (fr)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105749859B (zh) * 2014-12-17 2018-05-04 中国石油天然气股份有限公司 用于甲基丙烯酸甲酯脱酸吸附剂的制备方法
CN106423047B (zh) * 2015-08-10 2019-12-27 中国石油化工股份有限公司 一种球形正构烷烃吸附剂及其制备方法
CN106475048B (zh) * 2015-08-28 2019-05-21 中国石油化工股份有限公司 一种无粘结剂的5a分子筛球形吸附剂及制备方法
CN107961759B (zh) * 2016-10-19 2020-08-11 中国石油化工股份有限公司 一种5a分子筛吸附剂及其制备方法和应用
CN107376835B (zh) * 2017-08-18 2020-12-01 洛阳建龙微纳新材料股份有限公司 一种高效制氢吸附剂及其制备方法
CN109772261B (zh) * 2017-11-13 2021-11-26 中国石油化工股份有限公司 5a分子筛吸附剂及其制备方法和应用
CN108485314A (zh) * 2018-04-10 2018-09-04 宁波卡利特新材料有限公司 一种具有吸附功能的橡塑增强剂制备方法
CN111097379A (zh) * 2018-10-29 2020-05-05 中国石油化工股份有限公司 一种5a分子筛及其制备方法和应用
CN111097378A (zh) * 2018-10-29 2020-05-05 中国石油化工股份有限公司 一种改性分子筛吸附剂及其制备方法和应用
CN111097375A (zh) * 2018-10-29 2020-05-05 中国石油化工股份有限公司 一种改性分子筛及其制备方法和应用
CN111111609B (zh) * 2018-10-30 2022-02-22 中国石油化工股份有限公司 5a分子筛吸附剂及其制备方法和应用
CN109289764B (zh) * 2018-11-02 2021-04-06 太原理工大学 一种tut-5a的合成方法及其在丙炔丙烯高效分离中的应用
CN112755966A (zh) * 2019-10-21 2021-05-07 中国石油化工股份有限公司 5a分子筛吸附剂及其制备方法和应用
CN112717877A (zh) * 2019-10-28 2021-04-30 中国石油化工股份有限公司 一种吸附材料及其制备方法和应用
CN114054484A (zh) * 2020-07-31 2022-02-18 中国石油化工股份有限公司 一种可渗透反应墙及其修复污染地下水的方法
CN114426283B (zh) * 2020-10-29 2023-08-08 中国石油化工股份有限公司 5a分子筛及其制备方法和应用以及分离汽油中的正构烷烃和异构烷烃的方法
CN114433016B (zh) * 2020-10-31 2023-07-28 中国石油化工股份有限公司 一种5a分子筛吸附剂及其制备方法
CN114433013B (zh) * 2020-11-06 2023-12-19 中国石油化工股份有限公司 分子筛吸附剂的成型方法及其应用
CN113697824B (zh) * 2021-08-26 2023-08-25 中国地质科学院郑州矿产综合利用研究所 一种改性3a分子筛的制备工艺及其应用
CN114572995B (zh) * 2022-03-16 2024-02-20 南京宇清环境科技有限公司 一种高效吸附脱附分子筛制备方法及设备
CN115385355B (zh) * 2022-08-30 2023-11-17 江苏洁欧康科技有限公司 一种提高4a无粘连大球分子筛强度的方法

Family Cites Families (10)

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Publication number Priority date Publication date Assignee Title
DE3718673A1 (de) 1987-06-04 1988-12-15 Bayer Ag Zeolith a-granulat fuer sauerstoffanreicherung
CN1010301B (zh) 1987-08-03 1990-11-07 金凌石油化工公司南京炼油厂 无粘结剂球状a型分子筛制备方法
CN1248487A (zh) 1998-09-24 2000-03-29 广州经济技术开发区商业服务总公司 二次成孔分子筛吸附剂及其制备方法
CN1121051C (zh) 1999-12-06 2003-09-10 赵惠玲 按键板
US7404846B2 (en) * 2005-04-26 2008-07-29 Air Products And Chemicals, Inc. Adsorbents for rapid cycle pressure swing adsorption processes
KR101448271B1 (ko) * 2007-02-21 2014-10-07 토소가부시키가이샤 할로겐계 가스의 제해제 및 그것을 사용하는 할로겐계가스의 제해방법
CN101497022B (zh) 2008-01-31 2011-06-15 中国石油化工股份有限公司 聚结型沸石吸附剂及其制备方法
WO2012024896A1 (fr) 2010-08-23 2012-03-01 中国石油化工股份有限公司 Catalyseur à tamis moléculaire sans adhésif et procédé de préparation de celui-ci
CN102451664B (zh) 2010-10-21 2013-09-18 中国石油化工股份有限公司 用于全流程石脑油吸附分离的吸附剂制备方法
CN102464324A (zh) 2010-11-17 2012-05-23 中国石油化工股份有限公司 分子筛的成型方法

Also Published As

Publication number Publication date
US9656241B2 (en) 2017-05-23
US20150018196A1 (en) 2015-01-15
CN103933932A (zh) 2014-07-23
CN103933932B (zh) 2016-04-27
ES2457917R1 (es) 2015-03-17
ES2457917A2 (es) 2014-04-29
FR2997317A1 (fr) 2014-05-02
ITUD20130141A1 (it) 2014-04-30
ES2457917B1 (es) 2015-09-22

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