FR2425291A1 - Procede de preparation de nitrure metallique en poudre - Google Patents

Procede de preparation de nitrure metallique en poudre

Info

Publication number
FR2425291A1
FR2425291A1 FR7909151A FR7909151A FR2425291A1 FR 2425291 A1 FR2425291 A1 FR 2425291A1 FR 7909151 A FR7909151 A FR 7909151A FR 7909151 A FR7909151 A FR 7909151A FR 2425291 A1 FR2425291 A1 FR 2425291A1
Authority
FR
France
Prior art keywords
metal nitride
preparing metal
liquid ammonia
nitride powder
reaction temperature
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7909151A
Other languages
English (en)
Other versions
FR2425291B1 (fr
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ube Corp
Original Assignee
Ube Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ube Industries Ltd filed Critical Ube Industries Ltd
Publication of FR2425291A1 publication Critical patent/FR2425291A1/fr
Application granted granted Critical
Publication of FR2425291B1 publication Critical patent/FR2425291B1/fr
Granted legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/06—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/06—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron
    • C01B21/0615—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron with transition metals other than titanium, zirconium or hafnium
    • C01B21/0617—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron with transition metals other than titanium, zirconium or hafnium with vanadium, niobium or tantalum
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/06—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron
    • C01B21/0635—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron with germanium, tin or lead
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/06—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron
    • C01B21/064—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron with boron
    • C01B21/0643—Preparation from boron halides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/06—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron
    • C01B21/068—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron with silicon
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/06—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron
    • C01B21/076—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron with titanium or zirconium or hafnium
    • C01B21/0763—Preparation from titanium, zirconium or hafnium halides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/80—Compositional purity

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Nanotechnology (AREA)
  • Composite Materials (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Materials Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Ceramic Products (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

L'INVENTION A POUR OBJET UN PROCEDE DE PREPARATION DE NITRURE METALLIQUE SOUS FORME D'UNE POUDRE FINE DE HAUTE PURETE QUI PERMET DE RESOUDRE LES PROBLEMES DE COLMATAGE, ET DE REGLAGE DE LA TEMPERATURE DE REACTION. CE PROCEDE CONSISTE A FAIRE REAGIR UN HALOGENURE METALLIQUE AVEC DE L'AMMONIAC LIQUIDE DANS UN REACTEUR EN PRESENCE D'UN SOLVANT ORGANIQUE AYANT UN POIDS SPECIFIQUE SUPERIEUR A CELUI DE L'AMMONIAC LIQUIDE ET SEULEMENT LEGEREMENT MISCIBLE OU NON MISCIBLE AVEC L'AMMONIAC LIQUIDE A LA TEMPERATURE DE REACTION, L'INTRODUCTION DE L'HALOGENURE METALLIQUE ETANT REALISEE DANS LA COUCHE INFERIEURE DE SOLVANT DU SYSTEME REACTIONNEL.
FR7909151A 1978-05-08 1979-04-11 Procede de preparation de nitrure metallique en poudre Granted FR2425291A1 (fr)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP5371378A JPS54145400A (en) 1978-05-08 1978-05-08 Production of metal nitride powder

Publications (2)

Publication Number Publication Date
FR2425291A1 true FR2425291A1 (fr) 1979-12-07
FR2425291B1 FR2425291B1 (fr) 1982-11-26

Family

ID=12950464

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7909151A Granted FR2425291A1 (fr) 1978-05-08 1979-04-11 Procede de preparation de nitrure metallique en poudre

Country Status (6)

Country Link
US (1) US4196178A (fr)
JP (1) JPS54145400A (fr)
DE (1) DE2915023C2 (fr)
FR (1) FR2425291A1 (fr)
GB (1) GB2020264B (fr)
SE (1) SE438146B (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2446252A1 (fr) * 1979-01-10 1980-08-08 Toyo Soda Mfg Co Ltd Nitrure de silicium de haute purete et procede pour la preparation de celui-ci

Families Citing this family (49)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4321163A (en) * 1978-11-21 1982-03-23 Max-Planck-Gesellschaft Lithium nitride of increased conductivity, method for its preparation, and its use
JPS589764B2 (ja) * 1980-04-18 1983-02-22 宇部興産株式会社 金属炭窒化物の製法
JPS593925B2 (ja) * 1980-06-20 1984-01-26 宇部興産株式会社 金属炭窒化物の製法
US4396587A (en) * 1980-08-29 1983-08-02 Asahi-Dow Limited Method for manufacture of silicon nitride
US5445776A (en) * 1980-10-20 1995-08-29 Kabushiki Kaisha Kobe Seiko Sho Method for producing high density sintered silicon nitride (Si3 N.sub.4
DE3141590C2 (de) * 1980-10-20 1985-01-03 Kobe Steel, Ltd., Kobe, Hyogo Verfahren zur Herstellung von hochdichtem gesintertem Siliziumnitrid
JPS57175711A (en) * 1981-04-21 1982-10-28 Asahi Glass Co Ltd Synthesis of silicon nitride
US4851206A (en) * 1981-07-15 1989-07-25 The Board Of Trustees Of The Leland Stanford Junior University, Stanford University Methods and compostions involving high specific surface area carbides and nitrides
JPS5815013A (ja) * 1981-07-21 1983-01-28 Asahi Glass Co Ltd 珪素の窒化物の合成方法
JPS5888110A (ja) * 1981-11-17 1983-05-26 Ube Ind Ltd 窒化ケイ素質粉末の製法
JPS5891018A (ja) * 1981-11-26 1983-05-30 Denki Kagaku Kogyo Kk 窒化物微粉末の製造方法
JPS5921506A (ja) * 1982-07-27 1984-02-03 Ube Ind Ltd 結晶質窒化ケイ素粉末の製法
JPS60145903A (ja) * 1983-12-29 1985-08-01 Toa Nenryo Kogyo Kk 無機ポリシラザン及びその合成方法
DE3578581D1 (de) * 1985-12-09 1990-08-09 Toa Nenryo Kogyo Kk Verfahren zur herstellung von siliciumimid und dessen weiterberarbeitung zu siliciumnitrid.
US4686095A (en) * 1985-12-23 1987-08-11 Ford Motor Company Method of making ultrapure silicon nitride precursor
US4800183A (en) * 1986-04-09 1989-01-24 The United States Of America As Represented By The United States Department Of Energy Method for producing refractory nitrides
US4732746A (en) * 1986-04-18 1988-03-22 Ford Motor Company Method of making high purity silicon nitride precursor
US4746501A (en) * 1986-12-09 1988-05-24 United States Department Of Energy Process for preparing transition metal nitrides and transition metal carbonitrides and their reaction intermediates
US5023213A (en) * 1986-12-09 1991-06-11 United States Department Of Energy Precursors in the preparation of transition metal nitrides and transition metal carbonitrides and their reaction intermediates
DE3717284A1 (de) * 1987-05-22 1988-12-01 Basf Ag Verfahren zur herstellung von pulverfoermigem siliciumnitrid
DE3720572A1 (de) * 1987-06-22 1989-01-05 Basf Ag Amorphes pulverfoermiges siliciumnitrid
US4929433A (en) * 1987-10-22 1990-05-29 Alfred University Method for the preparation of sinterable nitrides
US4914063A (en) * 1988-04-04 1990-04-03 The United States Of America As Represented By The United States Department Of Energy Process for producing organic products containing silicon, hydrogen, nitrogen, and carbon by the direct reaction between elemental silicon and organic amines
DE3829503A1 (de) * 1988-08-31 1990-03-01 Bayer Ag Siliciumnitridpulver mit geringem sauerstoffgehalt
US4929432A (en) * 1988-10-19 1990-05-29 Union Carbide Corporation Process for producing crystalline silicon nitride powder
JP2659807B2 (ja) * 1989-01-26 1997-09-30 万鎔工業株式会社 直接製錬方法
US5244647A (en) * 1990-08-29 1993-09-14 Tanaka Kinkinzoku Kogyo K.K. Process of preparing hexaamminerhodium trihydroxide, hexaammineplatinum (IV) tetrahydroxide, tetraammineplatinum (II) dihydroxide and tetraamminepalladium dihydroxide
DE4031070A1 (de) * 1990-10-02 1992-04-09 Bayer Ag Siliciumdiimid, verfahren zu dessen herstellung sowie daraus erhaltenes siliciumnitrid
US5171557A (en) * 1991-05-28 1992-12-15 Ford Motor Company Method for silicon nitride precursor solids recovery
DE4241287A1 (de) * 1992-12-08 1994-06-09 Bayer Ag Siliciumaluminiumnitridkeramik und Vorläuferverbindungen, Verfahren zu ihrer Herstellung sowie deren Verwendung
US5618509A (en) * 1993-07-09 1997-04-08 Showa Denko K.K. Method for producing cubic boron nitride
DE19651731B4 (de) * 1995-12-12 2012-08-16 Ube Industries, Ltd. Verfahren zur Herstellung einer Stickstoff enthaltenden Silanverbindung
US5968594A (en) * 1996-06-28 1999-10-19 Lam Research Corporation Direct liquid injection of liquid ammonia solutions in chemical vapor deposition
JP2005097022A (ja) * 2003-09-22 2005-04-14 Japan Science & Technology Agency Ｉｉｉｂ族窒化物の合成方法
JP4585043B1 (ja) * 2009-11-12 2010-11-24 太平洋セメント株式会社 金属窒化物の製造方法
KR101746562B1 (ko) 2009-11-12 2017-06-13 다이헤이요 세멘토 가부시키가이샤 알칼리금속 질화물 또는 알칼리토금속 질화물의 제조방법
JP5627099B2 (ja) * 2010-02-08 2014-11-19 太平洋セメント株式会社 アルカリ金属窒化物の製造方法
JP5627105B2 (ja) * 2010-02-08 2014-11-19 太平洋セメント株式会社 アルカリ土類金属窒化物の製造方法
JP5651493B2 (ja) * 2010-02-08 2015-01-14 太平洋セメント株式会社 多種アルカリ土類金属窒化物複合体の製造方法
JP5567880B2 (ja) * 2010-03-30 2014-08-06 太平洋セメント株式会社 反応制御方法
JP5849961B2 (ja) * 2010-10-20 2016-02-03 三菱化学株式会社 共沈原料を用いた窒化物蛍光体の製造方法、窒化物蛍光体、及びその原料
KR20120061343A (ko) * 2010-12-03 2012-06-13 삼성엘이디 주식회사 형광체 제조방법 및 발광 장치
JP6089032B2 (ja) 2011-06-27 2017-03-01 シックスポイント マテリアルズ， インコーポレイテッド 遷移金属窒化物および遷移金属窒化物の合成方法
WO2013042721A1 (fr) * 2011-09-22 2013-03-28 戸田工業株式会社 Procédé de fabrication d'une poudre ferromagnétique de nitrure de fer, aimant anisotrope, aimant aggloméré et aimant en poudre comprimée
CN105236363B (zh) * 2015-10-12 2018-01-16 陕西阳乐陶瓷材料科技有限公司 一种制备微米纳米级球形氮化硅粉的方法
WO2017169584A1 (fr) * 2016-03-31 2017-10-05 富士フイルム株式会社 Composition, film durci, filtre coloré, film de blocage de lumière, élément d'imagerie à semi-conducteurs et dispositif d'affichage d'image
CN115246632A (zh) * 2020-11-02 2022-10-28 刘辉 一种利用固态四氯化钛与低温液氨制备氮化钛型材的方法
CN113148966B (zh) * 2021-04-20 2022-04-29 安徽工业大学 氨解法制备高纯氮化硅粉体方法
CN116119627B (zh) * 2023-02-08 2024-07-23 华瓷聚力(厦门)新材料有限公司 一种高α相氮化硅粉末合成方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3591338A (en) * 1968-06-05 1971-07-06 Du Pont Preparation of metal nitrides
US3959446A (en) * 1974-03-01 1976-05-25 The United States Of America As Represented By The Secretary Of The Air Force Synthesis of high purity, alpha phase silicon nitride powder
DE2635167B1 (de) * 1976-08-05 1977-10-06 Rosenthal Ag Verfahren zur Verminderung der Gasdurchlaessigkeit von poroesen Koerpern aus reaktionsgesintertem Siliziumnitrid

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2207791A (en) * 1938-03-18 1940-07-16 Fernelius Willis Conard Manufacture of sulphur nitride
US3032397A (en) * 1957-01-25 1962-05-01 Du Pont Preparation of metal nitride pigment flakes

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3591338A (en) * 1968-06-05 1971-07-06 Du Pont Preparation of metal nitrides
US3959446A (en) * 1974-03-01 1976-05-25 The United States Of America As Represented By The Secretary Of The Air Force Synthesis of high purity, alpha phase silicon nitride powder
DE2635167B1 (de) * 1976-08-05 1977-10-06 Rosenthal Ag Verfahren zur Verminderung der Gasdurchlaessigkeit von poroesen Koerpern aus reaktionsgesintertem Siliziumnitrid

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
CA1974 *
CA1975 *
EXBK/59 *
EXBK/69 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2446252A1 (fr) * 1979-01-10 1980-08-08 Toyo Soda Mfg Co Ltd Nitrure de silicium de haute purete et procede pour la preparation de celui-ci

Also Published As

Publication number Publication date
JPS5644006B2 (fr) 1981-10-16
FR2425291B1 (fr) 1982-11-26
SE7903031L (sv) 1979-11-09
DE2915023C2 (de) 1984-11-08
JPS54145400A (en) 1979-11-13
SE438146B (sv) 1985-04-01
DE2915023A1 (de) 1979-11-22
US4196178A (en) 1980-04-01
GB2020264B (en) 1982-09-08
GB2020264A (en) 1979-11-14

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