FR2446252A1 - Nitrure de silicium de haute purete et procede pour la preparation de celui-ci - Google Patents
Nitrure de silicium de haute purete et procede pour la preparation de celui-ciInfo
- Publication number
- FR2446252A1 FR2446252A1 FR8000391A FR8000391A FR2446252A1 FR 2446252 A1 FR2446252 A1 FR 2446252A1 FR 8000391 A FR8000391 A FR 8000391A FR 8000391 A FR8000391 A FR 8000391A FR 2446252 A1 FR2446252 A1 FR 2446252A1
- Authority
- FR
- France
- Prior art keywords
- preparation
- silicon nitride
- purity silicon
- weight
- nitride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/06—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron
- C01B21/068—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron with silicon
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/087—Compounds containing nitrogen and non-metals and optionally metals containing one or more hydrogen atoms
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
- C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/03—Particle morphology depicted by an image obtained by SEM
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Ceramic Products (AREA)
Abstract
Ce procédé est caractérisé en ce qu'on effectue le traitement thermique de silanes azotés en présence d'ammoniac. Le nitrure est caractérisé en ce qu'il a une teneur en chlore inférieure à 0,05 % en poids et une teneur en azote supérieure à 38 % en poids. L'invention trouve une application avantageuse dans le domaine des matériaux céramiques, notamment pour turbines à gaz.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP75179A JPS5595605A (en) | 1979-01-10 | 1979-01-10 | High purity silicon nitride and production thereof |
Publications (2)
Publication Number | Publication Date |
---|---|
FR2446252A1 true FR2446252A1 (fr) | 1980-08-08 |
FR2446252B1 FR2446252B1 (fr) | 1985-07-12 |
Family
ID=11482394
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR8000391A Expired FR2446252B1 (fr) | 1979-01-10 | 1980-01-09 | Nitrure de silicium de haute purete et procede pour la preparation de celui-ci |
Country Status (5)
Country | Link |
---|---|
US (1) | US4387079A (fr) |
JP (1) | JPS5595605A (fr) |
DE (1) | DE3000463A1 (fr) |
FR (1) | FR2446252B1 (fr) |
GB (1) | GB2040902B (fr) |
Families Citing this family (20)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5913442B2 (ja) * | 1980-01-11 | 1984-03-29 | 東ソー株式会社 | 高純度の型窒化珪素の製造法 |
JPS5855316A (ja) * | 1981-09-24 | 1983-04-01 | Toyo Soda Mfg Co Ltd | 窒化珪素粉末の製造法 |
JPS5891018A (ja) * | 1981-11-26 | 1983-05-30 | Denki Kagaku Kogyo Kk | 窒化物微粉末の製造方法 |
JPS59107908A (ja) * | 1982-12-08 | 1984-06-22 | Toyo Soda Mfg Co Ltd | 焼結性に優れた窒化珪素粉末の製造法 |
JPS60145903A (ja) * | 1983-12-29 | 1985-08-01 | Toa Nenryo Kogyo Kk | 無機ポリシラザン及びその合成方法 |
US4582696A (en) * | 1985-04-15 | 1986-04-15 | Ford Motor Company | Method of making a special purity silicon nitride powder |
DE3578581D1 (de) * | 1985-12-09 | 1990-08-09 | Toa Nenryo Kogyo Kk | Verfahren zur herstellung von siliciumimid und dessen weiterberarbeitung zu siliciumnitrid. |
JPS62148309A (ja) * | 1985-12-23 | 1987-07-02 | Toyo Soda Mfg Co Ltd | 高α型窒化珪素粉末の製造法 |
US4732746A (en) * | 1986-04-18 | 1988-03-22 | Ford Motor Company | Method of making high purity silicon nitride precursor |
US4795622A (en) * | 1986-04-24 | 1989-01-03 | Toa Nenryo Kogyo Kabushiki Kaisha | Method for producing silicon-imide |
US4914063A (en) * | 1988-04-04 | 1990-04-03 | The United States Of America As Represented By The United States Department Of Energy | Process for producing organic products containing silicon, hydrogen, nitrogen, and carbon by the direct reaction between elemental silicon and organic amines |
US5176893A (en) * | 1989-10-02 | 1993-01-05 | Phillips Petroleum Company | Silicon nitride products and method for their production |
DE4031070A1 (de) * | 1990-10-02 | 1992-04-09 | Bayer Ag | Siliciumdiimid, verfahren zu dessen herstellung sowie daraus erhaltenes siliciumnitrid |
US5171557A (en) * | 1991-05-28 | 1992-12-15 | Ford Motor Company | Method for silicon nitride precursor solids recovery |
US5453317A (en) * | 1993-08-31 | 1995-09-26 | Borg-Warner Automotive, Inc. | Friction material comprising powdered phenolic resin and method of making same |
KR100350332B1 (ko) * | 1993-09-23 | 2002-11-14 | 보그-워너 인코포레이티드 | 분말실리콘수지와분말페놀수지를포함하는불포화마찰재료및이의제조방법 |
US6264908B1 (en) | 1997-12-04 | 2001-07-24 | Thomas C. Maganas | Methods and systems for the catalytic formation of silicon nitride using a fluidized bed of silica |
EP1294639A1 (fr) * | 2000-06-17 | 2003-03-26 | Kunkel, Klaus | Procede d'obtention de nitrure de silicium |
CN101734632B (zh) * | 2009-12-10 | 2011-10-05 | 四川德诚金谷硅材料有限公司 | 纳米氮化硅粉的生产方法 |
KR101535379B1 (ko) * | 2014-04-14 | 2015-07-27 | 오씨아이 주식회사 | 수평형 반응기를 이용한 질화규소 분말 제조장치 및 이를 이용한 질화규소 분말 제조방법 |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3959446A (en) * | 1974-03-01 | 1976-05-25 | The United States Of America As Represented By The Secretary Of The Air Force | Synthesis of high purity, alpha phase silicon nitride powder |
FR2425291A1 (fr) * | 1978-05-08 | 1979-12-07 | Ube Industries | Procede de preparation de nitrure metallique en poudre |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA705317A (en) * | 1965-03-09 | F. Forsyth Paul | Process for producing ultrafine silicon nitride | |
GB970639A (en) * | 1960-03-24 | 1964-09-23 | Plessey Co Ltd | Method of producing high density silicon nitride |
JPS54124898A (en) * | 1978-03-22 | 1979-09-28 | Toyo Soda Mfg Co Ltd | Preparation of silicon nitride |
-
1979
- 1979-01-10 JP JP75179A patent/JPS5595605A/ja active Granted
-
1980
- 1980-01-08 DE DE19803000463 patent/DE3000463A1/de not_active Ceased
- 1980-01-09 GB GB8000688A patent/GB2040902B/en not_active Expired
- 1980-01-09 FR FR8000391A patent/FR2446252B1/fr not_active Expired
-
1981
- 1981-09-08 US US06/299,939 patent/US4387079A/en not_active Expired - Fee Related
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3959446A (en) * | 1974-03-01 | 1976-05-25 | The United States Of America As Represented By The Secretary Of The Air Force | Synthesis of high purity, alpha phase silicon nitride powder |
FR2425291A1 (fr) * | 1978-05-08 | 1979-12-07 | Ube Industries | Procede de preparation de nitrure metallique en poudre |
Non-Patent Citations (3)
Title |
---|
CA1979 * |
EXBK/59 * |
EXBK/75 * |
Also Published As
Publication number | Publication date |
---|---|
JPS5595605A (en) | 1980-07-21 |
US4387079A (en) | 1983-06-07 |
JPS6112844B2 (fr) | 1986-04-10 |
DE3000463A1 (de) | 1980-08-07 |
GB2040902A (en) | 1980-09-03 |
GB2040902B (en) | 1983-01-06 |
FR2446252B1 (fr) | 1985-07-12 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
ST | Notification of lapse |