FR2391836A1 - Procede de preparation d'une membrane poreuse en fluorure de polyvinylidene - Google Patents
Procede de preparation d'une membrane poreuse en fluorure de polyvinylideneInfo
- Publication number
- FR2391836A1 FR2391836A1 FR7815593A FR7815593A FR2391836A1 FR 2391836 A1 FR2391836 A1 FR 2391836A1 FR 7815593 A FR7815593 A FR 7815593A FR 7815593 A FR7815593 A FR 7815593A FR 2391836 A1 FR2391836 A1 FR 2391836A1
- Authority
- FR
- France
- Prior art keywords
- solvent
- polymer
- forming bath
- membrane
- degrees
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D71/00—Semi-permeable membranes for separation processes or apparatus characterised by the material; Manufacturing processes specially adapted therefor
- B01D71/06—Organic material
- B01D71/30—Polyalkenyl halides
- B01D71/32—Polyalkenyl halides containing fluorine atoms
- B01D71/34—Polyvinylidene fluoride
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
- B01D67/0002—Organic membrane manufacture
- B01D67/0009—Organic membrane manufacture by phase separation, sol-gel transition, evaporation or solvent quenching
- B01D67/0011—Casting solutions therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C67/00—Shaping techniques not covered by groups B29C39/00 - B29C65/00, B29C70/00 or B29C73/00
- B29C67/20—Shaping techniques not covered by groups B29C39/00 - B29C65/00, B29C70/00 or B29C73/00 for porous or cellular articles, e.g. of foam plastics, coarse-pored
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Dispersion Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Mechanical Engineering (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
Abstract
L'invention a pour objet un procédé continu pour la préparation de membranes microporeuses et de membranes pour filtration moléculaire, consistant à appliquer une couche d'une solution d'un polymère de fluorure de polyvinylidène sur une face d'une bande d'appui supportée rigidement afin d'obtenir une pellicule, puis à faire passer la bande dans un bain de formation dans lequel la membrane est formée. Pour préparer la solution de polymère, on dissout le polymère dans un véhicule liquide qui dissout jusqu'à 25 % du poids du polymère à au moins 50 degrés C, mais qui dissout sensiblement moins du polymère à 20 degrés C environ. On prépare la solution à 50 degrés C ou plus et on maintient le bain de formation à peu près à la température ambiante. Le bain de formation est un mélange du véhicule liquide solvant avec un second liquide miscible avec le solvant mais qui n'est pas un solvant pour le polymère. On maintient la pellicule plongée dans le bain de formation jusqu'à sa transformation en une membrane poreuse dont la structure poreuse est essentiellement complètement formée, on élimine le solvant de la pellicule par lavage et on le remplace par le liquide non-solvant. Après quoi on extrait le solvant résiduel de la membrane poreuse et, après séparation de la membrane d'avec la bande d'appui, on sèche la membrane. Le système solvant-non-solvant préféré pour le bain de formation est un système acétone-eau. Il est préférable que le bain de formation contienne d'environ 70 à 80 % d'acétone, en volume.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US05/800,574 US4203848A (en) | 1977-05-25 | 1977-05-25 | Processes of making a porous membrane material from polyvinylidene fluoride, and products |
Publications (2)
Publication Number | Publication Date |
---|---|
FR2391836A1 true FR2391836A1 (fr) | 1978-12-22 |
FR2391836B1 FR2391836B1 (fr) | 1983-10-07 |
Family
ID=25178764
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR7815593A Granted FR2391836A1 (fr) | 1977-05-25 | 1978-05-25 | Procede de preparation d'une membrane poreuse en fluorure de polyvinylidene |
Country Status (6)
Country | Link |
---|---|
US (1) | US4203848A (fr) |
JP (1) | JPS5416382A (fr) |
CA (1) | CA1118560A (fr) |
DE (1) | DE2822266A1 (fr) |
FR (1) | FR2391836A1 (fr) |
GB (1) | GB1594640A (fr) |
Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2391837A1 (fr) * | 1977-05-25 | 1978-12-22 | Millipore Corp | Procede de preparation d'une membrane poreuse en matiere polymere |
EP0012557A1 (fr) * | 1978-12-06 | 1980-06-25 | Abcor, Inc. | Membranes hydrophiles polymères, procédé pour leur préparation, leur application en tant que membranes ultrafiltrantes et membranes précurseurs susceptibles d'y être converties |
EP0037836A1 (fr) * | 1979-10-15 | 1981-10-21 | Asahi Kasei Kogyo Kabushiki Kaisha | Microfiltre a filament creux en resine de fluorure de polyvinylidene et son procede de production |
EP0040670A2 (fr) * | 1980-03-28 | 1981-12-02 | Pennwalt Corporation | Membrane poreuse en polymère de fluorure de vinylidène et procédé pour sa fabrication |
FR2528361A1 (fr) * | 1982-03-16 | 1983-12-16 | Parker Pen Co | Instrument d'ecriture et son procede de fabrication |
EP0100552A2 (fr) * | 1982-08-02 | 1984-02-15 | Mitsubishi Rayon Co., Ltd. | Membrane à base d'un matériau poreux hydrophobe rendue hydrophile et son procédé de fabrication |
EP0175322A2 (fr) * | 1984-09-17 | 1986-03-26 | Mitsubishi Rayon Co., Ltd. | Membrane rendue hydrophile à base d'un matériau poreux hydrophobe et son procédé de fabrication |
EP0264333A2 (fr) * | 1986-10-17 | 1988-04-20 | Cytogen Corporation | Méthode de préparation de compositions de protéine, chélateur et ion métallique, convenant à l'injection |
EP0330072A2 (fr) * | 1988-02-26 | 1989-08-30 | SEPAREM S.p.A. | Membrane semi-perméable de séparation de fluides, son procédé de fabrication et son utilisation en microfiltration, distillation et pour des tissus spéciaux |
EP0335805A2 (fr) * | 1988-04-01 | 1989-10-04 | Terumo Kabushiki Kaisha | Procédé de préparation de membrane poreuse et membrane poreuse préparée par un tel procédé |
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JPS60232085A (ja) * | 1984-04-28 | 1985-11-18 | Kanegafuchi Chem Ind Co Ltd | 無菌的濾過方法 |
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- 1978-05-19 CA CA000303780A patent/CA1118560A/fr not_active Expired
- 1978-05-22 DE DE19782822266 patent/DE2822266A1/de active Granted
- 1978-05-25 FR FR7815593A patent/FR2391836A1/fr active Granted
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Cited By (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2391837A1 (fr) * | 1977-05-25 | 1978-12-22 | Millipore Corp | Procede de preparation d'une membrane poreuse en matiere polymere |
EP0012557A1 (fr) * | 1978-12-06 | 1980-06-25 | Abcor, Inc. | Membranes hydrophiles polymères, procédé pour leur préparation, leur application en tant que membranes ultrafiltrantes et membranes précurseurs susceptibles d'y être converties |
EP0037836A1 (fr) * | 1979-10-15 | 1981-10-21 | Asahi Kasei Kogyo Kabushiki Kaisha | Microfiltre a filament creux en resine de fluorure de polyvinylidene et son procede de production |
EP0037836A4 (fr) * | 1979-10-15 | 1982-01-26 | Asahi Chemical Ind | Microfiltre a filament creux en resine de fluorure de polyvinylidene et son procede de production. |
EP0040670A2 (fr) * | 1980-03-28 | 1981-12-02 | Pennwalt Corporation | Membrane poreuse en polymère de fluorure de vinylidène et procédé pour sa fabrication |
EP0040670A3 (en) * | 1980-03-28 | 1982-02-10 | Pennwalt Corporation | Porous vinylidene fluoride polymer membrane and process for its preparation |
FR2528361A1 (fr) * | 1982-03-16 | 1983-12-16 | Parker Pen Co | Instrument d'ecriture et son procede de fabrication |
EP0100552A3 (en) * | 1982-08-02 | 1985-05-02 | Mitsubishi Rayon Co. Ltd. | Hydrophilized membrane of porous hydrophobic material and process of producing same |
EP0100552A2 (fr) * | 1982-08-02 | 1984-02-15 | Mitsubishi Rayon Co., Ltd. | Membrane à base d'un matériau poreux hydrophobe rendue hydrophile et son procédé de fabrication |
EP0175322A2 (fr) * | 1984-09-17 | 1986-03-26 | Mitsubishi Rayon Co., Ltd. | Membrane rendue hydrophile à base d'un matériau poreux hydrophobe et son procédé de fabrication |
EP0175322A3 (en) * | 1984-09-17 | 1987-01-28 | Mitsubishi Rayon Co. Ltd. | Hydrophilized membrane of porous hydrophobic material and process for preparing the same |
EP0264333A2 (fr) * | 1986-10-17 | 1988-04-20 | Cytogen Corporation | Méthode de préparation de compositions de protéine, chélateur et ion métallique, convenant à l'injection |
EP0264333A3 (fr) * | 1986-10-17 | 1988-07-06 | Cytogen Corporation | Méthode de préparation de compositions de protéine, chélateur et ion métallique, convenant à l'injection |
EP0330072A2 (fr) * | 1988-02-26 | 1989-08-30 | SEPAREM S.p.A. | Membrane semi-perméable de séparation de fluides, son procédé de fabrication et son utilisation en microfiltration, distillation et pour des tissus spéciaux |
EP0330072A3 (fr) * | 1988-02-26 | 1990-03-14 | SEPAREM S.p.A. | Membrane semi-perméable de séparation de fluides, son procédé de fabrication et son utilisation en microfiltration, distillation et pour des tissus spéciaux |
EP0335805A2 (fr) * | 1988-04-01 | 1989-10-04 | Terumo Kabushiki Kaisha | Procédé de préparation de membrane poreuse et membrane poreuse préparée par un tel procédé |
EP0335805A3 (fr) * | 1988-04-01 | 1990-04-25 | Terumo Kabushiki Kaisha | Procédé de préparation de membrane poreuse et membrane poreuse préparée par un tel procédé |
US4965291A (en) * | 1988-04-01 | 1990-10-23 | Terumo Kabushiki Kaisha | Method of manufacturing porous membrane and porous membrane manufactured by the same method |
Also Published As
Publication number | Publication date |
---|---|
US4203848A (en) | 1980-05-20 |
CA1118560A (fr) | 1982-02-23 |
GB1594640A (en) | 1981-08-05 |
FR2391836B1 (fr) | 1983-10-07 |
JPS5416382A (en) | 1979-02-06 |
DE2822266C2 (fr) | 1987-05-07 |
DE2822266A1 (de) | 1978-12-07 |
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