FR2358359A1 - Procede de preparation en continu de la phosphine pure - Google Patents
Procede de preparation en continu de la phosphine pureInfo
- Publication number
- FR2358359A1 FR2358359A1 FR7721767A FR7721767A FR2358359A1 FR 2358359 A1 FR2358359 A1 FR 2358359A1 FR 7721767 A FR7721767 A FR 7721767A FR 7721767 A FR7721767 A FR 7721767A FR 2358359 A1 FR2358359 A1 FR 2358359A1
- Authority
- FR
- France
- Prior art keywords
- stage
- phosphorus
- alkali hydroxide
- phosphine
- continuous preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- XYFCBTPGUUZFHI-UHFFFAOYSA-N Phosphine Chemical compound P XYFCBTPGUUZFHI-UHFFFAOYSA-N 0.000 title abstract 6
- 238000000034 method Methods 0.000 title abstract 3
- 229910000073 phosphorus hydride Inorganic materials 0.000 title abstract 3
- 238000002360 preparation method Methods 0.000 title abstract 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 abstract 4
- 229910001854 alkali hydroxide Inorganic materials 0.000 abstract 3
- 150000008044 alkali metal hydroxides Chemical class 0.000 abstract 3
- 229910052698 phosphorus Inorganic materials 0.000 abstract 3
- 239000011574 phosphorus Substances 0.000 abstract 3
- 239000007795 chemical reaction product Substances 0.000 abstract 2
- 239000000243 solution Substances 0.000 abstract 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- 239000008346 aqueous phase Substances 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 1
- 229910052760 oxygen Inorganic materials 0.000 abstract 1
- 239000001301 oxygen Substances 0.000 abstract 1
- 238000003756 stirring Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/06—Hydrogen phosphides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2632316A DE2632316C3 (de) | 1976-07-17 | 1976-07-17 | Verfahren zur kontinuierlichen Herstellung von Phosphin |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| FR2358359A1 true FR2358359A1 (fr) | 1978-02-10 |
| FR2358359B1 FR2358359B1 (enExample) | 1982-02-26 |
Family
ID=5983317
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR7721767A Granted FR2358359A1 (fr) | 1976-07-17 | 1977-07-13 | Procede de preparation en continu de la phosphine pure |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US4143121A (enExample) |
| BE (1) | BE856843A (enExample) |
| CA (1) | CA1083777A (enExample) |
| CH (1) | CH631417A5 (enExample) |
| DD (1) | DD131009A5 (enExample) |
| DE (1) | DE2632316C3 (enExample) |
| DK (1) | DK146925C (enExample) |
| ES (1) | ES460465A1 (enExample) |
| FR (1) | FR2358359A1 (enExample) |
| GB (1) | GB1535711A (enExample) |
| IT (1) | IT1079733B (enExample) |
| NL (1) | NL182634C (enExample) |
| SE (1) | SE7708204L (enExample) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2840147A1 (de) * | 1978-09-15 | 1980-03-27 | Hoechst Ag | Verfahren zur kontinuierlichen herstellung von phosphan |
| US6685904B1 (en) * | 1998-04-16 | 2004-02-03 | Occicdental Chemical Corporation | Process for making phosphorus halides and oxyhalides |
| CN111453708B (zh) * | 2020-05-21 | 2024-07-23 | 天津中科拓新科技有限公司 | 一种电子级磷烷的合成与精制方法及装置 |
| CN114620695B (zh) * | 2022-02-23 | 2023-07-07 | 沧州华宇特种气体科技有限公司 | 一种制备磷化氢的系统及其制备方法 |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1181938A (fr) * | 1956-09-10 | 1959-06-19 | Fonte Electr | Procédé pour la préparation d'hypophosphites |
| US2977192A (en) * | 1958-08-26 | 1961-03-28 | Fmc Corp | Process for the production of phosphine and sodium hypophosphite |
| FR2139000A1 (enExample) * | 1971-05-24 | 1973-01-05 | Knapsack Ag | |
| FR2329588A1 (fr) * | 1975-11-03 | 1977-05-27 | Hoechst Ag | Procede de preparation de la phosphine |
-
1976
- 1976-07-17 DE DE2632316A patent/DE2632316C3/de not_active Expired
-
1977
- 1977-05-24 CH CH641177A patent/CH631417A5/de not_active IP Right Cessation
- 1977-06-20 NL NLAANVRAGE7706777,A patent/NL182634C/xx not_active IP Right Cessation
- 1977-07-01 IT IT50081/77A patent/IT1079733B/it active
- 1977-07-04 GB GB27882/77A patent/GB1535711A/en not_active Expired
- 1977-07-06 ES ES460465A patent/ES460465A1/es not_active Expired
- 1977-07-13 FR FR7721767A patent/FR2358359A1/fr active Granted
- 1977-07-13 US US05/815,161 patent/US4143121A/en not_active Expired - Lifetime
- 1977-07-14 SE SE7708204A patent/SE7708204L/xx unknown
- 1977-07-15 CA CA282,811A patent/CA1083777A/en not_active Expired
- 1977-07-15 DK DK322277A patent/DK146925C/da not_active IP Right Cessation
- 1977-07-15 BE BE179367A patent/BE856843A/xx not_active IP Right Cessation
- 1977-07-15 DD DD7700200097A patent/DD131009A5/xx not_active IP Right Cessation
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1181938A (fr) * | 1956-09-10 | 1959-06-19 | Fonte Electr | Procédé pour la préparation d'hypophosphites |
| US2977192A (en) * | 1958-08-26 | 1961-03-28 | Fmc Corp | Process for the production of phosphine and sodium hypophosphite |
| FR2139000A1 (enExample) * | 1971-05-24 | 1973-01-05 | Knapsack Ag | |
| FR2329588A1 (fr) * | 1975-11-03 | 1977-05-27 | Hoechst Ag | Procede de preparation de la phosphine |
Also Published As
| Publication number | Publication date |
|---|---|
| NL7706777A (nl) | 1978-01-19 |
| IT1079733B (it) | 1985-05-13 |
| DK322277A (da) | 1978-01-18 |
| NL182634B (nl) | 1987-11-16 |
| FR2358359B1 (enExample) | 1982-02-26 |
| GB1535711A (en) | 1978-12-13 |
| DE2632316A1 (de) | 1978-01-19 |
| DK146925B (da) | 1984-02-13 |
| US4143121A (en) | 1979-03-06 |
| DE2632316C3 (de) | 1981-12-24 |
| DK146925C (da) | 1984-07-23 |
| DD131009A5 (de) | 1978-05-24 |
| CH631417A5 (de) | 1982-08-13 |
| SE7708204L (sv) | 1978-01-18 |
| CA1083777A (en) | 1980-08-19 |
| BE856843A (fr) | 1978-01-16 |
| DE2632316B2 (de) | 1981-02-05 |
| ES460465A1 (es) | 1978-05-01 |
| NL182634C (nl) | 1988-04-18 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| ST | Notification of lapse |